International Standard

INTERNATIONAL ORGANIZATION FOR STANDARDIZATION.ME~YHAPO&HAR OPTAHM3ALWl fl0 CTAH~APTbl3ALWl.ORGANlSATlON INTERNATIONALE DE NORMALISATION

Ammonia solution for industrial use - Determination of

residue after evaporation at 105 OC - Gravimetric method
Ammoniaque 4 wage industriel - Dhtermination du rhidu apr&s Evaporation & 105 T - Mhthode gravimhtrique

First edition - 1985-06-01

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ISO 7109:1985
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c662d66ac4a1/iso-7109-1985

UDC 661.51 : 543.21 : 543.714 Ref. No. ISO 7109-1985 (E)

Descriptors : industrial products, Chemical compounds, ammonia Solution, tests, determination, Chemical residues, evaporation, gravimetric
analysis.

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Foreword
ISO (the International Organitation for Standardization) is a worldwide federation of
national Standards bodies (ISO member bodies). The work of preparing International
Standards is normally carried out through ISO technical committees. Esch member
body interested in a subject for which a technical committee has been established has
the right to be represented on that committee. International organizations, govern-
mental and non-governmental, in liaison with ISO, also take patt in the work.

Draft International Standards adopted by the technical committees are circulated to

the member bodies for approval before their acceptance as International Standards by
the ISO Council. They are approved in accordance with ISO procedures requiring at
least 75 % approval by the member bodies voting.
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International Standard ISO 7109 was prepared by Technical Committee ISO/TC 47,
Chemistry. (standards.iteh.ai)
ISO 7109:1985
https://standards.iteh.ai/catalog/standards/sist/0662a13a-6923-4088-93f1-
c662d66ac4a1/iso-7109-1985

0 International Organkation for Standardkation, 1985

Printed in Switzerland
INTERNATIONAL STANDARD ISO 71094985 (E)

Ammonia Solution for industrial use - Determination of

residue after evaporation at 105 OC - Gravimetric method

WARNING - Carry out all the operations in a welkventilated fume cupboard.

1 Scope and field of application to a volume of about 40 ml. Wash the volumetric flask with two
10 ml portions of distilled water and add the washings to the
This International Standard specifies a gravimetric method for dish. Continue the Operation until all liquid has completely
the determination of the residue after evaporation of ammonia evaporated.
solution for industrial use.
Remove the dish from the water bath and place it in the electric
The method is applicable to solutions containing not more than oven (4.2) maintained at 105 + 2 OC, for at least 30 min. Allow
35 % (mlm) of ammonia. the dish containing the residue to cool in a desiccator and
weigh to the nearest 0,000 1 g.

2 Reference iTeh STANDARD PREVIEW

6 Expression of results
mination of density at 20 OC.
(standards.iteh.ai)
ISO 750, Liquid Chemical products for industrial use - Deter-
The residue after evaporation, expressed in milligrams per
kilogram, is given by the formula
ISO 7109:1985
3 Principle https://standards.iteh.ai/catalog/standards/sist/0662a13a-6923-4088-93f1-
ml - mo
c662d66ac4a1/iso-7109-1985 x 106
Evaporation of a test Portion in a tared platinum dish; weighing VQ
of the residue after drying at 105 + 2 OC.
where

m. is the mass, in grams, of the empty platinum dish;

4 Apparatus
Ordinary laboratory apparatus and m1 is the mass, in grams, of the platinum dish and
residue;

4.1 Platinum dish, diametei about 75 mm. V is the volume, in millilitres, of the test Portion (5.1);

4.2 Electric oven, capabll e of being mainta ined at Q is the density, in grams per millilitre, of the test Sample,
105 It 2 OC. determined in accordance with the method specified in
ISO 758.

5 Procedure
7 Test report
5.1 Test Portion The test report shall include the following particulars:
Fill a 500 ml one-mark volumetric flask to the mark with some a) an identification of the Sample;
of the laboratory Sample.
b) the reference of the method used;
5.2 Determination
c) the results and the method of expression used;
Weigh, to the nearest 0,000 1 g, the platinum dish (4.1)
previously dried at 105 + 2 OC and cooled in a desiccator. Pour d) any unusual features noted during the determination;
some of the test Portion (5.1) into the weighed platinum dish,
and place on a bath of boiling water in a weil-ventilated fume e) any Operation not included in this International Stan-
cupboard. Carefully evaporate the Solution, gradually adding dard or in the International Standard to which reference is
more of the test portion, until the test Portion has evaporated made, or regarded as optional.

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ISO 7109:1985
https://standards.iteh.ai/catalog/standards/sist/0662a13a-6923-4088-93f1-
c662d66ac4a1/iso-7109-1985