Reference TOTL-SP07-F01

Office Egypt

ISO/IEC 17025 Form Issue n° / Date 00 / 01 April 19

Clause 7.2 & 7.6 Author / Approver M.Saleh / M. Abd Elrazek
Selection, verification and validation of methods
Page n° Page 1 of 5
and measurement uncertainty
Latest Method Updates Check
Date Test Method Update Found Signature
Test Analysis Coal- Ash according to
15/2/2024 Yes No
ISO 1171:2010

Test Analysis Coal- Gross Calorific

15/2/2024 value according to ISO 1928: 2020 Yes No

Test Analysis Coal Volatile Matter

15/2/2024 according to ISO 562:2010 Yes No

Test Analysis Coal- Moisture by

15/2/2024 Oven according to ISO 589:2008-B2 Yes No

Determination of (CHN) in Coal

15/2/2024 Yes No
ASTM D5373 – 21
Determination of (S) in Coal
15/2/2024 Yes No
ASTM D4239 – 18 e1
Determination of Density in fuel oil
22/9/2024 ASTM D4052-22
Yes No

Standard Test Method for

Kinematic Viscosity of
22/9/2024 Transparent and Opaque Liquids Yes No
petroleum products according to
ASTM D445 – 21
Standard Test Method for
Sulfur in Petroleum Products by
22/9/2024 Wavelength Dispersive X-ray Yes No
Fluorescence Spectrometry1
According to ASTMD 4294-21

Determination of Pour Point of

22/9/2024 Petroleum Products according to Yes No
ASTMD 97-2017
 Reference TOTL-SP07-F01

Office Egypt

ISO/IEC 17025 Form Issue n° / Date 00 / 01 April 19

Clause 7.2 & 7.6 Author / Approver M.Saleh / M. Abd Elrazek
Selection, verification and validation of methods
Page n° Page 2 of 5
and measurement uncertainty
Latest Method Updates Check

Determination of Salts in Crude

22/9/2024 Oil (Electrometric Method) Yes No
According to ASTM D 3230-2019

Determination of Flash Point by

Pensky-Martens Closed Cup Tester of
22/9/2024 petroleum products according to
Yes N
ASTM D93:2020

Determination of Acid Value in oil ISO

15/2/2024 660:2020
Yes No

Determination of Peroxide value in oil

15/2/2024 AOCS cd 8b-90: 2017
Yes No

Test Analysis total fatty matter in

15/2/2024 Soap according to ISO 685:2020 Yes No

Determination of total hardness in

15/2/2024 water according to APHA 2340 C Yes No
23rd 2017
Determination of Chloride in Water
15/2/2024 APHA 4500-Cl B. 23rd 2017 Yes No

Test Analysis determination of PH

15/2/2024 in water according to APHA 4500- H Yes No
23rd 2017
Determination of Phosphorus
15/2/2024 (Total) in Fertilizers according to Yes No 19/7/2022
AOAC Official Method 962.02:2016
Determination of total nitrogen in
15/2/2024 urea BS EN 15478:2009
Yes No 19/7/2022

Determination of fiber in Animal feed

15/2/2024 according to (BS EN ISO 6865-2000)
Yes No

Determination of Fat in Animal feed

15/2/2024 according to ISO-6492-1999
Yes No

Determination of Moisture in Animal

15/2/2024 feed according to ISO-6496-1999
Yes No
 Reference TOTL-SP07-F01

Office Egypt

ISO/IEC 17025 Form Issue n° / Date 00 / 01 April 19

Clause 7.2 & 7.6 Author / Approver M.Saleh / M. Abd Elrazek
Selection, verification and validation of methods
Page n° Page 3 of 5
and measurement uncertainty
Latest Method Updates Check
Determination of crude ash in Animal
15/2/2024 feed according to ISO 5984:2022
Yes No

Determination of crude protein in

15/2/2024 Animal feed according to Yes No
AOAC :2001.11:2016

Determination of crude protein in

15/2/2024 Animal feed according to ISO 5983- Yes No
1:2005

Determination of Moisture in cereals

15/2/2024 according to ISO 712:2009
Yes No

Determination of crude protein in

15/2/2024 cereals according to ISO 20483:2013
Yes No

Determination of Iron in Iron Ores and

15/2/2024 Related Materials by Dichromate Yes No
Titrimetric ASTM E246-10 (2021)
Microbiology of the food chain -
Horizontal method for the
15/2/2024 enumeration of microorganisms -Part Yes No
1: Colony count at 30 °C by the pour
plate technique according to ISO4833-
1:2013
Microbiology of food and animal
feeding stuffs — General requirements
15/2/2024 and guidance for microbiological Yes No
examinations according to BS EN
ISO7218:2007
Microbiology of the food chain —
Preparation of test samples, initial
15/2/2024 suspension and decimal dilutions for Yes No
microbiological examination according
to BS EN ISO6887:2017

Microbiology of food and animal

feeding stuffs — Horizontal method for
15/2/2024 the enumeration of yeasts and moulds
Yes No
according to ISO21527-1:2008
 Reference TOTL-SP07-F01

Office Egypt

ISO/IEC 17025 Form Issue n° / Date 00 / 01 April 19

Clause 7.2 & 7.6 Author / Approver M.Saleh / M. Abd Elrazek
Selection, verification and validation of methods
Page n° Page 4 of 5
and measurement uncertainty
Latest Method Updates Check
Microbiology of food, animal feed and
water-Preparation, production,
15/2/2024 storage and performance testing of Yes No
culture media according to ISO
11133:2014
Microbiology of the food chain –
Horizontal method for the
15/2/2024 enumeration of beta glucuronidase- Yes No
positive Escherichia coli according to
BS ISO 16649-1:2018

Standard methods for the examination

15/2/2024 of water and waste water according to Yes No
23rd Edition (APHA 9221 B)

Standard methods for the examination

15/2/2024 of water and waste water according to Yes No
23rd Edition (APHA 9221 E)

Microbiology of the food chain -

Horizontal method for the detection
15/2/2024 and enumeration of Yes No
Enterobacteriaceae according to BS EN
ISO 21528-1:2017
Light and lighting — Measurement and
presentation of photometric data of
15/2/2024 lamps and luminaires(EN 13032-
Yes No
1:2004+A1

Acoustics — Determination of
15/2/2024 occupational noise exposure — Yes No
Engineering method (ISO 9612:2009)

ICSBEP Guide to the Expression of

Uncertainties Editor V. F. Dean
15/2/2024 Subcontractor to Idaho National
Yes No
Laboratory (2007)

Water quality — Enumeration of

culturable micro-organisms — Colony
15/2/2024 count by inoculation in a nutrient agar
Yes No
culture medium (ISO6222:1999)
 Reference TOTL-SP07-F01

Office Egypt

ISO/IEC 17025 Form Issue n° / Date 00 / 01 April 19

Clause 7.2 & 7.6 Author / Approver M.Saleh / M. Abd Elrazek
Selection, verification and validation of methods
Page n° Page 5 of 5
and measurement uncertainty
Latest Method Updates Check

Determination of Pseudomonas
15/2/2024 aeruginosa in water by Membrane Yes No
Filter Technique ISO 16266:2006(E)

Water quality — Enumeration of

15/2/2024 Legionella (ISO11731:2017)
Yes No

Water quality — Enumeration of

15/2/2024 Salmonella spp ISO19250:2010.
Yes No

Microbiology of food and animal

feeding stuffs — Horizontal method for
15/2/2024 the enumeration of coliforms — Yes No
Colony-count technique
(ISO4832:2006)
Microbiology of the food chain —
Horizontal method for the detection,
15/2/2024 enumeration and serotyping of Yes No
Salmonella-Part 1: Detection of
Salmonella spp. (ISO 6579-1:2017)
Microbiology of the food-Horizontal
method for the enumeration of
coagulase-positive staphylococci
15/2/2024 (Staphylococcus aureus and other
Yes No
species) Part 1: Method using Baird-
Parker agar medium (ISO 6888-1:2021)
Microbiology of the food-Horizontal
method for the detection and
15/2/2024 enumeration of Listeria Yes No
monocytogenes and of Listeria spp.-
Part 1: Detection method (ISO 11290-
1:2017)
Remarks
- Latest method updates check should be done at most every three months.