H.E.J.

RESEARCH INSTITUTE OF CHEMISTRY

INTERNATIONAL CENTER FOR CHEMICAL SCIENCES
UNIVERSITY OF KARACHI, KARACHI-75270

SPECTROSCOPIC SERVICES

Sponsored by the Higher Education Commission and Private Institutions

Analyses
Sample Submission Form
Date: ..................................................

Name: ...................................................................................................................................................................

Name of Organization: .........................................................................................................................................

Address: ................................................................................................................................................................
Sample code: …………………………………………. Type of analysis:……………………….……………
(Please use separate form for each sample for each technique)

M.P./B.P.: ...................................................... ……….. Solvent for analysis........................................

TLC purity: .................................................... TLC solvent system: .....................................

Molecular weight/Molecular formula (if known): ................................................................................................

Solvent for NMR analysis: CDCl3/DMSO/D2O/ ..................................................................................................

Solubility at 25o C: ................................................................................................................................................

Nature of sample (i.e. steroid, alkaloid etc): ........................................................................................................

Any other information:………………………………………………………………………………...

 For NMR analysis, at least 20 mg of substance is required with complete solubility in approximately 0.5 mL of some common
deuterated solvent.
 Quantity, solubility and purity of the substance submitted should be checked carefully. Kindly make sure that it is organic in
nature and not a quaternary salt, betaine or a metal complex.
 The bill will be sent to the HEC under the “Access to Scientific Instrument Program.”

Signature and Seal of Chairperson/Director of Institution……… ……………………………………………

Approval of the Director HEJRIC: …………………………………………………………………..

Received: Date:.............................................................................. No.: ......................................................

Completed: Date:.............................................................................. Signature:.............................................

Signature of Section Incharge:

 INTERNATIONAL CENTER FOR CHEMICAL AND BIOLOGICAL SCIENCES (HEJ RESEARCH
INSTITUTE OF CHEMISTRY, DR. PANJWANI CENTER FOR MOLECULAR MEDICINE AND DRUG RESEARCH)
UNIVERSITY OF KARACHI-75270, PAKISTAN.

S. DISCOUNTED RATES FOR

TYPE OF ANALYSIS
No. PUBLIC SECTOR INSTITUTIONS
Pak Rupees
PROTON NMR Experiment
1 a. In D2O OR CDCl3 3,750
b. In any other solvent (CD3OD, C3D6O, DMSO-d6, C5D5N, C2D3N) 7,500
13
2 C-NMR Experiment
BROAD BAND DECOUPLED SPECTRUM
a. In D2O OR CDCl3 7,500
b. In any other solvent (CD3OD, C3D6O, DMSO-d6, C5D5N, C2D3N) 10,500
13
3 C-NMR (DEPT-90 and DEPT-135)
a. In D2O OR CDCl3 10,500
b. In any other solvent (CD3OD, C3D6O, DMSO-d6, C5D5N, C2D3N) 13,500
4 OFF-RESONANCE SPECTRUM
a. IN CDCl3 9,000
b. IN ANY OTHER DEUTERATED SOLVENT 12,000
5 INVERSE NMR MEASUREMENTS HMBC,HMQC, HSQC, etc.
a. IN D2O OR CDCl3 9,000
b. IN ANY OTHER DEUTERATED SOLVENT 18,000
6 HYBRID NMR SPECTROSCOPY
a. DEPT-HSQC ( MUTIPLICITY EDITED HSQC) 15,000
b. HSQC -TOCSY 15,000
c. HSQC- NOESY 15,000
7 HOMONUCLEAR 2 D- COSY,NOESY,TOCSY,DOSY,ROESY
a. IN D2O OR CDCl3 3,750
b. IN ANY OTHER DEUTERATED SOLVENT 7,500
8 2D INADEQUATE
a. IN D2O OR CDCl3 7,500
b. IN ANY OTHER DEUTERATED SOLVENT 15,000
9 J-RES, X-J-RES
a. IN D2O OR CDCl3 7,500
b. IN ANY OTHER DEUTERATED SOLVENT 10,500
10 NOE DIFFERENCE
a. IN D2O OR CDCl3 (PER EXPERIMENT) 3,750
b. IN ANY OTHER DEUTERATED SOLVENT (PER EXPERIMENT) 7,500
11 1-D SELECTIVE COSY, NOESY ,TOCSY
a. IN D2O OR CDCl3 (PER EXPERIMENT) 3,750
b. IN ANY OTHER DEUTERATED SOLVENT (PER EXPERIMENT) 7,500
IF SAMPLE IS NOT SOLUBLE IN SPECIFIED
SOLVENT(FOR EACH DEUTERATED SOLVENT) 4,500
12 UV SPECTRUM 750
13 IR SPECTRUM (FTIR) 1,500
 S. DISCOUNTED RATES FOR
NO. TYPE OF ANALYSIS PUBLIC SECTOR INSTITUTIONS
14 GAS CHROMOTOGRAPHIC ANALYSIS 7,500
15 CD SPECTRUM 1,500
16 C.H.N. MICROANALYSIS / S ELEMENTAL ANALYSIS 9,000
17 OPTICAL ROATATION 300
18 MASS, EI, POSITIVE MODE 7,500
19 HR-EI POSITIVE MODE 12,000
20 CI POSITIVE NEGATIVE MODE 10,500
21 GCMS-EI, POSITIVE MODE, FULL SCAN 22,500
22 FAB POSITIVE/NEGATIVE MODE 9,000
23 FAB-HR (PEAK MATCHING) POSITIVE/NEGATIVE 10,500
24 ESI-HR-MS,POSITIVE/NEGATIVE 8,000.00
25 ESI-HR-MSMS,POSITIVE/NEGATIVE 18,000
26 LCMS-ESI, POSITIVE/NEGATIVE, FULL SCAN 27,000
27 MALDI,POSITIVE/NEGATIVE 18,000
IMAGING FACILITY
28 DIC AND BRIGHT FIELD MICROSCOPY AND
IMAGE CAPTURING 1,500
29 FLORESCENT MICROSCOPY AND
IMAGE CAPTURING 3,000
30 DIC AND BRIGHT FIELD MICROSCOPY AND
IMAGE CAPTURING 1,500
FLORESCENT MICROSCOPY AND
31 IMAGE CAPTURING 3,000
TISSUE PROCESSING,EMBEDDING,SECTIONING AND
32 H&E STAINING ANIMAL 1,500
33 ATOMIC FORCE MICROSCOPY (AFM) 4,500

Note: Samples must be submitted ready for direct analysis as single pure ingredients with their
solubility in CDCl3 for NMR and MeOH for UV. If the material is not soluble in chloroform then the
solubility in other solvents must be pre-checked and the solvent in which the spectrum is to be recorded
clearly specified. The above rates are applicable for government institution only. Private institutions
would be charged 100% extra. For peak matching and High Resolution Measurements; low resolution
(EI or FAB) spectra are required.