“Le DETERMINATION OF TSP PuRITY. Arrea.- DM: Plan Seeereesinde tel = rtd Responsibatiy = Dt ak chante Reagents - | Le LN« softer dy Senne tabitiDn os { Deisolve Ho gm coclteam : ina Ales abe and mare tk upto joooml. CaP Lobeteon Oe Scene SOS rr Paar eUta oae ae __thior’e Acid) tn Bisteltel alee er mage up toot me: ty Mons eaeeahe ae feleah a dd ita Heb = etm Ch werk INeHCl < YH g. ocd AN Hef Nani weth Bea tndieador dell Penk cotBeut appears =x mL.an) => Malculal: rT i ’ nt ay iguige)h = ZF 0° 98029 X [000 ,” 0 ° c Cc pee “Psp (Nas Por tit 5955 ali os (Naa OYhe (X- ADK 0° 091 K 190 _ koh 4 ae carbonate as (hlantess "t= (A-z) % O°0S3R 1000 _ Qs: i igs nous e @ Heh a ‘ . 7 col ’ »DETERMINATION OF fy DRAZINE NY pparTe Pup a “nai =D. Plant: “Dette 2 Dutanmenatian as _h hence rypbande Pant | Rose ee es mney Reogontes il oe ae =a 4+ 0:1 Potassivem haomafe brome poluteon + 2 Décsotve 2-723 §.005 Potasscam banmate ! brome 009) 1092 04 “Podasseruna havorry'o 09 1600 ML od Wadert - A: Mened ensidcadnar- Sotudelon- yen 0 up to. 60'c a pee ar ac ate eealeafrsncl ddecarfe cheoeth ta. Q DaHeon Purdy 0d AiSrarene WuQamte (Naty 1a H30) = : 0:01as x Pv i omy 5. © age , 4 @ Podass cum beromede « | @ MeweA _cnslecatoa) Diwm_HYBRaXtL Pe MaBIE EY: rer. Dims Plant: Deseo Deluemenafcon od ‘coD Etim eerie Perit ——Responerheitity = Doms plane hems — Reagents alist a. 499 coupalin ler oo feforafe aos 2h aud to. PBiehe cgnint 218 HySeochoree a9 ep nae ___B+ Node the votume of awd 999 G) Now Gps the tebe WH ON hy Qaocktowce Ac) fell the peor cote es oa ee ae ES a re ——_Heethen 0894-9 dnops_od ere 2.2 tel megs a on_tamige to. ree) Coho ume O¢ ALL egrets to _complele- “he deoradéon Wek Mestles —o iilf | cofe ulabec on “hi cf ne pe Bade 1 j _@ Phenephitatsis Kagan.nena Ta sail MetHops of Test FOR HYDROCHLORIC CID ADETERMINA TION OF erat AciDITY. soa - DM: Plone us pista caren ai i] ona oSloead en Destotled wWadere about 2-04 ad the melenéal on rt tinsel the eee to conten) osx and Sduide -to loo £4] CALerfabeion : Pod Aer Dity a8 H BRE NRBE-YS ICD Sample waht x (000 Reference -038 LS 266'1993. CAomecal. OD Sodceam AO Meth onange:- METHODS OF Pes FOR HYDROCHLORIC HE#D Ds DETERMNATION OF SULPHATES agenes= h: 8Becmn Corhonao § AR Aro 2 / A’ Barium chtere otuteory — 10 Ye Banos y Jax ee Cn & Pamtetar'n A "Jesh ang eae De) As Motte: weth 10 am “adbbad and) 299. 900 m2 05. bodlle’ng Watort dd tor ; Shot a ae J OCH) otererte’ a + J Sett0a UY has. 8: Petter the srpernatant gigi a-domed i entered Geass creerer'ble- Co Noy) fh 8 wash thoroughly teth shot. wieder heat the cunechte i a l0S- Ildo . af ———Clcitafion - 3 Stel Phafes O38 Hpsoy. « | ae Sarpple aa re = tS AEE. 1993 New nh — IMETHODS OF “TEST FOR HYDROCHLORIC Heap: ~~ 6: DETERMINATION OF TRON. PR Reagent , he Ritude hyfachumis goin. . oate Satter ft “Saal —Dessotve_lo gm of. hyde Amman ~— Chom Seon wader and Delete loorme BBQ Bernidye Sotuteon = ) Banna a ee st. berga ” ome ———Alitude Ay fanchtonid gerd CL) and 3) e 404an) Waser 4 i 4. Gharaerd tron ctor Loluteby Q —— — ___Dissotie 0-308 gan 0 Ob themeous 4 Gmmontum cphate tn Ie'sterle) clase AQ9- 14 concentrated teotPheuccc sed and_Make up £0 /000 mt favtme: -O-1gm ef tron (ase) } 4 Bh WOureng tren odors’ 3. Dake 160 ML Od the Sanden Aten Sotudeoy 4’ and Aletie to _toveme werh L Amt = ool MA lrcoCOs Fe) - b+ Ammonia acefose totnbenn 4 siqeo See eee _Of- _ mm on Ae Cen Wafer a0 SVelucfe- AROS eel spe 3 i fesce ane =. je 2. Weigh — ouceeened ty abut a0 am m od the Sample 09 & phatinrm on cetcca Qeeh ¢ too me capaorty —____Evaporafe to Sheyness on Wafert bath. 9: Co0h Joke Up Weth 9 me_od etek » hySroe i ML a} Wafer and to ARSsatve 3B» Transder. Sprang ttfetive to CO too me flosk Ailude do the Moa J sare:4s Monder an atiqued od the sample olusear) ¢o 4 eer) Od Iron to o {00 md thosk. = “Bs Dette to 80 w amb ae ae u RQ og hy y mMeneys a9 emo od ammontétin acodade Soludtion and Ame 2.9 -bepytldye sotuseon Deseo to the Marck mex and walt for to-mentpes « ~ bs Corre Ott the Measereement on the SPet dan phodomelen+ at a wave Lenyth Spa nm cAcude oe optocap Density Using as Reffenence the bla >4 DETERMINATION. OF :pogTY OF Sopivm:tyaocsnetTe = i Tega Q. pees coystals : FOmmns 9 stonch - ndicotor: nygen ‘ayetan ats os 4 ; bi SoSeeum thinsterphale sottfedy BIN > a, . c’ssotv a cate thi Me Slistilte) iodee and mare ct up to 1900 mb. he Procedure = 41. , D HQ me ya Cone : a ai peaele tn a_tantcal dt , 3: AIA 14m of podasseceny tod ede - . hy and oS cmb get aceite ae. Se Immediately tedrafe with o-LN SoS Huoscelpbabe tell peeomes Pale \elloc : | GAD) Ime starch IQicaly and -tedwase neil the blue Coto us discharged). { alec: ‘of = 2 a 4 ne C gram er ps ae cn me. 4 O Aerdee awd. ‘ @ potassceun eye @_stonch Q-_sodiany friosutph afe ." MepHeDs oF TESTING TOR sopjum MY OROXIDE “Be DETERMINGTION OF CHIORI DES: ~ Reoge dls ¢ r eine TG Dilueke Neducie. geet) @ Silver ee Selon 4 ‘L 0 chporrSo Seat j rat ere : x i ‘0 ome- C00 : c = 0-05g9m: chioweJe: > °° Cue . ‘i F Wh Boome - z z qe “499-6 mood Actule nelmie geTiand) tne _sclvee Nedarada. Coupe Moke txp tho: satudeby 10 0 mf we¥i Wat ost » Cort 0 est Oi 6 pl 2 Use Lead ~ofanSarS:> rhloar So > Sobeteon and the Came Juontitces 0d other eageal 5 eu Ge EL Volume od tho itearhion Mcaxtirce 4. compare the opalescence Prodi) the tin pie 2 sAbdet | Smeg sn) Sigil tne “dor chiens hall be faken a3 Not having heon eateended st Hata en eed Os tet ~ Reference IS, ae 1986 tbsEee nce oncentyafe) HY Ieechtnre ber8= : Didevade. cp bath OTN Sodeum thioseephade Usergl . Indtcafys Pell co foe change deen bine, AO. colour less» 3 : 4s Blank - Paxe 50 me od o-LN Eine Sodufeon tn a Q5O ML contcal dose. AIL 2 m2 of “Concendrated Hy Paw chlawée Al arfl_teleate c_agcth ont fio ? ha + 3:23 CB-SDN M.Me Mass ny joo of Sample taken. chomecal A D Resebsiond Podene - @ Potasccam: DodeS)e 2) @ Sodicon) thin sce phate: @ Potasceem chaomate- © share.MetHeDS (ea : BEFERMINGFION OF TEST FOR SULPYURIC AD 10: DETERMINATION. OF TOTAL. A CLD ry. bode - —A-Cartedully deramdie ctho Cantent en to 0 conceal dean ____thorteare the volume upto absut 200 mp. 8-489 tio _nept_od metty ned eePcada_sobutede) an Jelerade_to the anS’pornd wrth StanJard ENEIED.S 06) um Wier! 4707123 2H 2,P Calemfafion - _____—etel auitiiy Qu tysoy) BRYN gag 7 . 1038 Od Sample cngm- _ chom : Sion Lyla @ Medhyt paaqea-(fen) . s Py P seep e IE DETERMING Tony OF AMMONTA. Poprry. eR Ms Plone _Pcle- Dedenmenafy of ‘Ariens _ Dm: “Peon hihi 2 eagons'? ¢ b A : cared * Seutphuere nud. a: Methy( ted QnSlecaféars ee Desntve 4g 4 mublyt 18) endecadon eoteh, / ethanae ard ase to LOO mL Leth ty an sa _soileum hy Dannie. 0: SN ‘ Proc oF cure Cele _ toed a aN ae GL o.tsmt_caponity 0 tho welghing Thole ‘Come S.cately ely replace the Glass Stopper an) | és cena werght 8» Place the werrhing be et dn about geome. ot water Comtacne anil ak ulphurce Aer) and for reps of’ methye red cndlecabe 4. open the stoppere_eenglen the acts) by y eth a giass mos) ang tifeabe the excess ad aeerd weth standandexed catestic soda soltfeon to! a dacat: allow) end pont a7) — “Carty Orel a ae all sthe , 0 te jest: é Rmmonta‘/, . |: 409 Clank, - Sample Ne Mass of Sample cng: —_Retenence - Is -F99= 1995IQ, DETERMIvanIOAL OF guboniots Ls-Anusania Laue 4 \ ri & B Reagants Bt crew tdizale Gatudion 1 0-4 Ni oPtrontimalaly 2 A. Détude NMade 4c’ + YN. appanacimedely - 4 x & . Door ae + Cyhoara} y) HOCK Lertelor) a Dessoeve ts be 9. a4 soAecem chtearIe ‘ed.at et. 0 mo. Amps ogm 0d choorede - gases tons -- + ee. eee ‘io as(ch : SororeSarre : = > Fee etal nie. o mafereal ana }__2vapreale 00 a steambath Untel stedbtrced 1 i + Ten Abitude sack seat od paper ea ame i ch ‘A and Attufe (LVen Nedreefe Sct) i : rey otf A Conlaol dest en ctho- Other Ne ssto ty en Useag [me ot Cétver nedaode colesteod ane) 50m) od ‘Woe - ; be tat doar monefes ans ceutthe_opaet | PreScce en tho tect 13th the mederceh Cs not greaPene than sha? Pardee ¢n the conrol dost 4 Reference ~ 1% 499: 199e-——Scepeé- Hel campie ~_APPADATUS Oco U, nical Shcisk apascdy - @ Deeeteh 4’ class N REAGENTS > Nh0 -Naow = = weeyh Nool and) Secsotve9)-@ __ STAN DARDT ZATION. §+ igh ngs Od Podarscces lyangan Narytha ana) Sessotved Ch & in comet ae 43a 9-4 Scupsidt (Phanatehehahetn ceDvealaar tg ___WOth “Naot! colufedn «to bo Charlard exe do aaa Od Penn cotour Porcrstant dow 20 ‘ ree “of (Na@oH « a sap a0 ae an ROOT 2 ®) PhonotP h tha ler Dadlicaforr Pancé Deotio=> ‘ ___Weigh o-¢ totam od He chose Convendanteg Be be Sefenmene 09a: abeaf bo. ma Od. Dinh stdaifer 40. | Acrufe eh -Petaahe by. stare At/ jo AaoH Useag Pheneephthbein enaecafon - colowt. chenge- colours £685 to. pink tt NEN K 6:5 % (00 CAL@vIATION= “tes tonatel Wt OF Sample > OO Bec dens Kai's fe: = et “Ie CAVSTIC__ CONCENTRATION TESTING Pre6hupr. 5 a Ic _24mples i ee | REAGENTS- N]io HE - Paxo ame pally tot" £9_Aoo mP Water and) make tp the volrune dn Hor wth Sestored wafor STAND AR DIZATION ~~ See oO Wee . ?: Ct Qty Con) 09 toned ask and) Sveso ed of: 7 about ome of Dm Water AIG. gen Drape od Meas Cngecofey and te th Hel Saluteon to ho / andardeze daa the Seve dopmont 0 freen eotowtte | tted- —___"Reewatiiy of Hd. AGE ee 2 Merd edecalie— pessctve 0s G4 Betomo eresop and _0-A gm mothe 223) wSrraba en Yoom® medbanal + Keep AANA e » Teaode ek Gains Nj 1o Hef. 2 End pornt Penk +0 Colour bersfs Ne HYDRAZIN *h TESTING PRICE DIRE H ae lane a ~~ _ en} pain - ECabedobior = ele ef, Wily = E Dhaene - FV Vola coms ON a + _Gokudcon Us x Tots tad niameltg 0 od 0 SN piscine aaa E : Wy = bseeght od Somple ctaxen « VXATR EO: OS oyita. oS Bei ae oLorto 3 acurtabely cxbouft o. volueng cn _o¢ os % hydrochtanre. A # P Nawmales Or ON Jere chlo Luton + a pee'ght of Sample fakens