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lab #7

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9 views

lab #7

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Uploaded by

cranderson36
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T Lab 78r~ond La 62 Acfd fuse

#
Laml1rt:Arctel'tilf) .1.
tr+rotfon Sol+ ~lotfoos /[1+a S~ee+
------
A. Acid Base Classification of Salts

Table 1; Prediction and Measurement of pH of Salt Solutions

NaCN KNO3 NH4(I NaHCO3 Na3PO4


Is Positive Ion
Acidic, Basic, Na+ }1' NHL/ No.+ No./·
or Neutral?
neutral (t(Jl-m)
State reason
why. GC1d ~wC£_\.l
Oc1d

s:,
Is Negative._!on
Acidic, Rasic, CN- c1 - No3 - HCD) PO~-
8as?c Acidic tu~
or Ne'utral?
State reason ~ t
why.
Q(\0
Overall, is salt
NoCN 1r,N03
Ac1d1c bOSl-
solution -
Acidic, Basic,
reutro\ necl(QI
or Neutral 8CA5fC
Solution
*Reason for
Above (

Prediction

pH
r·· q, 0. 5 s 7

1. For the salt solutions that are basic; write the reaction with water to show how they
produce (OH)" ions.
1 1
For example; NaF would be a basic salt due to the F- ; F' (aq) + H2O(I) <-> HF (aq) + (OH)-

NaCN -t- fuO ~


NoOt-1 +t--lCN
No('1co3) +1-120 tJaOl-i +- H2_C03
2. For the salt solutions that are acidic; write the reaction with water to show how they
produce H' ions.

B. Weak Acid_Strong Base Titration

i"L
1. Calculate the equivalence point when 9.80 ml of 0.1894 M CH3COOH reacts with 0.2006 M

1, , / , .

x.
NaOH. ,,

l· 025') = c,?!Xfo'{ v') _ =22 .7 mi


. \..
1

2. What salt is formed at the equivalence point?

3. Is the above salt acidic, basic, or neutral? Explain the reason why.

(lc1d/C bealu <;J, -Ire pH ·/:e!OW 7 0

4. Insert the graph of pH vs volume for the titration curve .. (Use Prt Sc on your keyboard to copy,
and ctrl 'v' to paste)

lh
-,~
t<L
1D

&
w
Ii
----
\0 ZD 30 50
4D
r

5. Estimate the midpoint of the steep rise in pH. Record the volume of NaOH at this
point Z 3'."2.
6. Does the value of the above question equal the volume at the equivalence point calculated in
question 1?

:Xf Fs c,(~

7. Divide your experimental volume of NaOH at the equivalence point by 2; _ _\:....;2'--"'-_ __

8. What is the pH from the titration curve for the ml NaOH from the above question.

P~ = 2:J. 7·S
9. The pH at a volume equal to half the volume of the equivalence points equals pKa for a weak
acid. Determine Ka for acetic acid - - - -

C. Polyprotic Acid Titration

-
10. Write the complete, balanced equation for the t~ep neutralization reaction between H2SO3

Hs~c
and NaOH.

H2'W3 + NaO\-\ --"? (

( H~ I +N,,,Olt ( 5'03 )-
11. What is the pH and color of the solution at the beginning of the titration?

12. What is the pH and color of the solution at the end of the titration?

13. Were there any additional color changes during the titration?
r
14. Insert the graph of pH vs volume for the polyprotic acid . (Use Prt Sc on your keyboard to copy,
and ctrl 'v' to paste)

I'{
,2
/0

10 2.0 ~o
15. What happens to the pH around 16 ml and 32 ml? What is the reason for this?

16. Calculate Kai and Ka2 for H2S03.

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