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Spectroscopic Methods in Organic Chemistry-I

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117 views

Spectroscopic Methods in Organic Chemistry-I

Uploaded by

ulfatandaleeb
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Week Wise Break UP

Department of CHEMISTRY

Course Title: Spectroscopic Methods in Organic Chemistry-I Semester: 7th


Course Code: CHM-643 Session: 2021 -2025
Program: BS-Chemistry Course Incharge: Dr. Zahida Wasil

CONTENTS WEEK Lectures

Introduction: The electromagnetic spectrum; Units and their 3


1
interconversion;
The absorption of electromagnetic radiation by organic molecules; 3
2
(molecular energy levels, molecular transitions and spectral regions)

UV-Visible spectroscopy: Introduction; Theory;


3
(absorptions of radiations and electronic transitions; intensities of 3
absorptions; effect of solvents on absorptions)
UV-Visible spectroscopy; Sample handling and instrumentation; 3
4

Chromophores: Conjugated dienes, trienes, polyenes, 3


5
unsaturated carbonyl compounds, benzene and its derivatives, poly
3
nuclear aromatic hydrocarbons and diketones 6

Factors affecting absorption maxima; Empirical rules for


3
calculation of lambda-max; 7
Presentations
Applications of UV-visible spectroscopy 3
(and interpretation of spectras) 8
Presentations

MID TERM EXAM

Infra-Red spectroscopy: Introduction; Theory; Sampling 3


techniques; 9

Instrumentation; Characteristics of vibrational frequencies of 3


10
functional groups;
Interpretation of IR spectra. 3
11
Mass spectrometry: Introduction; Theory; Types of fragments: odd
3
electron and even electron containing neutral and charged species; 12

Molecular Formula and molecular mass determination: 3


13
Nitrogen rule; Rule of thirteen and molecular formula; Index of
hydrogen deficiency; Isotopic peaks; Meta-stable ion peaks
Sample handling; Instrumentation; 3
14
Fragmentation patterns in different classes of organic compounds;
Interpretation of mass spectra.
3
Presentations 15

Applications: Structure elucidation of organic molecules based on


UV-visible, IR and MS data. 16 3
Presentations and Assignments

FINAL TERM EXAM

Recommended Books :
1. R.M. Silverstein, F.X. Webster and D.J. Kiemle, Spectrometric Identification of Organic Compounds,
John Wiley & Sons Inc., USA (2005).

2. D.L. Pavia, G.M. Lampman and G.S. Kriz, Introduction to Spectroscopy: a Guide for Students of
Organic Chemistry, Thomson Learning, Australia (2001).

3. D.W. Brown, A.J. Floyed and M. Sainsbury, Organic Spectroscopy, I. Wiley and Sons, Chichester
(1998).

4. D.H. Williams and I. Fleming, Spectroscopic Methods in Organic Chemistry, 4th ed., McGraw-Hill
Book Co., London (1987).

5. M. Hesse, H. Nleir and U. Zech, Spectroscopic Methods in Organic Chemistry, Georg Thiemc, Stuttgart,
New York (1997).

6. Y.C. Ning, Spectral Identification of Organic Compounds with Spectroscopic Techniques, Wiley-VCH,
Weinheim (2005). 7. M. Younas, Organic Spectroscopy, Ilmi Kitab Khana, Lahore (2004).

7. M. Younas, Organic Spectroscopy and Chromatography, Third Edition, Ilmi Kitab Khana, Lahore,
(2011)

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