CRUDE ASSAY REPORT

Report Number: IDL-3961-2021(rev06)

SAMPLE DESCRIPTION: Qatar Land Crude Oil

Bureau Veritas Commodities Division

Plot 10407, National Industries Park,
P.O. Box 49400, Dubai,
United Arab Emirates
email: [email protected]

Page 1
 LABORATORY REPORT NO: IDL-3961-2021(rev06)

Date: November 15, 2021

Company details : Qatar Petroleum

For the Attention of : Mr. Anil Kumar Sinha

Sample(s) received from : Bureau Veritas, Qatar

Sample(s) submitted as : Qatar Petroleum - Qatar Land Crude Oil

Description(s) on Label(s) : Qatar Land Crude Oil Sample

Seals on Sample(s) : 698218, 698407, 698617, 698629, 698646,

698667 & 698947

Sample(s) received on : 19 July, 2021

The above sample(s) was/were examined and the following results obtained:

Please refer attached sheets for analysis report.

AUTHORIZED SIGNATURE
Biju GEORGE
Assay Project Manager

Page 2
 LABORATORY REPORT NO: IDL-3961-2021(rev06)

Qatar Petroleum - Qatar Land Crude Oil

INDEX

Sl.No. Description Page No.

1 Title 1
2 Front Cover 2
3 Index 3
4 Summary of Fractional Analysis 4
5 True Boiling Point Distillation Data 5
6 True Boiling Point Distillation data - Graph 6
7 Summary of Product / Residue cut points & Yield 7
8 Summary of True Boiling Point Distillation Cuts - Graph 8
9 Summary of True Boiling Point Distillation Cuts - Pie Chart 9
10 Whole Condensate Properties 10
11 Naphtha Fraction- [C5-50°C] 11
12 Naphtha Fraction- [50-100°C] 12
13 Naphtha Fraction- [100-150°C] 13
14 Kerosene Fraction- [150-200°C] 14
15 Kerosene Fraction- [200-250°C] 15
16 Gas Oil Fraction- [250-300°C] 16
17 Gas Oil Fraction- [300-350°C] 17
18 Gas Oil Fraction- [350-400°C] 18
19 Vacuum Gas Oil Fraction- [400-450°C] 19
20 Vacuum Gas Oil Fraction- [450-500°C] 20
21 Vacuum Gas Oil Fraction- [500-550°C] 21
22 Atmospheric Residue- [400°C+] 22
23 Vacuum Residue- [550°C+] 23
24 Whole Crude Distillation Data - ASTM D86 24
25 Sulphur Graphical Chart 25
26 Total Acid Number Graphical Chart 26
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 LABORATORY REPORT NO: IDL-3961-2021(rev06)
QATAR LAND CRUDE OIL -DETAILED ASSAY ALL CUTS OVERVIEW

CUT RANGE

Whole Crude
Naphtha Distillate Fuels (GO) Atmospheric Vacuum
LPG Kerosene VGO
TEST UNIT METHOD Residue Residue

100 - 150°C

150 - 200°C

200 - 250°C

250 - 300°C

300 - 350°C

350 - 400°C

400 - 450°C

450 - 500°C

500 - 550°C
50 - 100°C
C5 - 50°C

400°C +

550°C +
Gas
Distillation of Crude Oil (15 plate)
Yield % Wt. 2.35 2.75 7.82 10.15 10.76 9.87 10.11 9.22 8.96 9.66 6.67 4.03 28.01 7.65
ASTM D 2892/ D5236
Yield % Vol. 3.23 3.53 9.35 11.21 11.32 10.15 9.97 8.80 8.20 8.78 5.90 3.49 24.23 6.06
Density @ 15°C kg/L ASTM D 5002 / D 4052 / IP 365 0.8238 0.6411 0.6888 0.7452 0.7827 0.8011 0.8351 0.8621 0.8995 0.9055 0.9311 0.9507 0.9513 1.0335
Specific Gravity @ 60/60° F Conversion 0.8242 0.6412 0.6890 0.7454 0.7830 0.8015 0.8355 0.8626 0.9000 0.9060 0.9316 0.9513 0.9519 1.0342
API Gravity @ 60° F Calculated 40.18 89.18 73.87 58.33 49.22 45.04 37.86 32.54 25.72 24.68 20.39 17.24 17.15 5.32
Ash Content % Wt. ASTM D482 <0.01
Asphaltenes % Wt. IP 143 <0.5 0.68 8.81
Aniline Point °C ASTM D611 NP* 62.0 55.0 53.5 69.5 88.0 99.0 >160
Basic Water and Sediment % Vol. ASTM D4007 0.025
Distillation (Full) ASTM D86 Page No-23
Flash Point °C IP 170 / D93 Below-30
Mercaptan Sulphur ppm Wt. UOP 163 298 805 435 235 245 255
Mercury ppb UOP 938 <1
Metals
Sodium <1 <1 <1
Potassium <1 <1 <1
Copper <1 <1 <1
ppm Wt. ICP
Lead <1 <1 <1
Iron <1 <1 <1
Nickel <1 <1 7
Vanadium 1.5 4 29
Kinematic Viscosity at 15°C 6.98
Kinematic Viscosity at 40°C 5.108
Kinematic Viscosity at 50°C NP* 0.352 0.512 0.771 1.327 2.286 4.338 10.650 32.03 NP* NP* 199.3 NP*
cSt ASTM D445
Kinematic Viscosity at 100°C NP* 0.254 0.343 0.484 0.756 1.156 1.876 3.776 7.74 20.18 34.96 25.32 670
Kinematic Viscosity at 135°C 10.14 129.5
Kinematic Viscosity at 175°C 5.042 47.50
UOP K. Factor UOP 375 12.39 11.85 11.73 11.79 11.66 11.57
Pour Point °C ASTM D97 -15 <-42 -39 -18 +6 +21 +36 +51 +54 -6 +51
Reid Vapour Pressure psi ASTM D323 / D5191 7.54 15.78 5.38 0.77
Salt Content PTB ASTM D3230 1.49
Salt Content mg/L ASTM D3230 4.25
Total Acid Number mgKOH/g ASTM D974 / D664 0.14 0.010 0.012 0.020 0.030 0.032 0.013 0.015 0.025 0.034 0.12 0.21 0.23 0.18
Total Nitrogen ppm Wt. ASTM D4629 295 <1 <1 <1 <1 <1 4 46 258 440 750 820 835 1950
Hydrogen Sulphide ppm Wt. UOP 163 30
Hydrogen Sulphide (Vapour Phase) ppm Vol ASTM D5705 / IP 570 2700
Total Sulphur Content % Wt. ASTM D4294 1.49 0.069 0.084 0.119 0.145 0.256 0.677 1.60 1.960 2.180 2.460 2.920 2.550 4.200
Water Content % Vol. ASTM D4006 0.05
Wax Content % Wt. UOP 46 <5
Naphthalene content %Vol. ASTM D1840 0.05 1.57
Smoke Point mm ASTM D1322 26.0 18.0
C6 Paraffins % Vol ASTM D6730 8.32 43.75 0.475
PIONA analysis
Total paraffins 98.51 83.73 69.66 55.16
Olefins <0.01 <0.01 0.07 0.32
iso- paraffins 42.48 37.23 35.61 25.68
% Vol GC
Total olefins <0.01 <0.01 0.07 0.32
Total napthenes 1.39 12.50 14.33 7.62
Total aromatics 0.10 3.78 15.67 31.59
Unidentified <0.01 <0.01 0.27 5.31
Cetane Index ASTM D4737 53.4 56.1 60.1
Light Ends
Methane 0.0000
Ethane 0.0132
Propane 0.2373
% Wt. IP 344
i-Butane 0.1902
n-Butane 0.9653
i-Pentane 0.8985
n-Pentane 1.5455
Cloud Point °C ASTM D2500 <-42 -40 -18 NP* NP*
Conradson carbon residue % Wt. ASTM D189 1.35 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 0.10 5.89 25.5
Aromatics (FIA) 22.4 18.8 24.8
Olefins (FIA) % Vol. ASTM D1319 0.4 0.8 0.6
Saturates (FIA) 77.2 80.4 74.6
Refractive Index @ 70° C ASTM D1218 1.4138 1.4264 1.4458 1.5170 1.5877

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 LABORATORY REPORT NO: IDL-3961-2021(rev06)

TRUE BOILING POINT DISTILLATION DATA

(ASTM D 2892 & D5236)

Sample Descriptions: Qatar Land Crude Oil Sample

Vapour Cumulative % Cumulative %

Sl. No. % mass % Volume
Temperature °C mass Volume
1 Gas 2.35 2.35 3.23 3.23

2 15 - 50 2.75 5.10 3.53 6.76

3 50 - 100 7.82 12.92 9.35 16.11

4 100 - 150 10.15 23.07 11.21 27.33

5 150 - 200 10.76 33.83 11.32 38.65

6 200 - 250 9.87 43.70 10.15 48.79

7 250 - 300 10.11 53.81 9.97 58.76

8 300 - 350 9.22 63.03 8.80 67.57

9 350 - 400 8.96 71.99 8.20 75.77

10 400 - 450 9.66 81.65 8.78 84.55

11 450 - 500 6.67 88.32 5.90 90.45

12 500 - 550 4.03 92.35 3.49 93.94

13 550 + Residue 7.65 100.00 6.06 100.00

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 TRUE BOILING POINT DISTILLATION CURVE

LABORATORY REPORT NO: IDL-3961-2021(rev06)

550

500

450

400

350
Temperature °C

300

250

% Mass

200
% Volume

150

100

50

0
0.0 10.0 20.0 30.0 40.0 50.0 60.0 70.0 80.0 90.0 100.0
Recovery %

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 LABORATORY REPORT NO: IDL-3961-2021(rev06)

SUMMARY OF PRODUCT / RESIDUE CUT POINTS AND YIELDS

Sample Descriptions: Qatar Land Crude Oil Sample

Cut Points Yield %

(° C) % mass % volume

LPG - Light Ends Gas 2.35 3.23

Naphtha - I 15 - 50 2.75 3.53

Naphtha - II 50 - 100 7.82 9.35

Naphtha - III 100 - 150 10.15 11.21

Kerosene - I 150 - 200 10.76 11.32

Kerosene -II 200 - 250 9.87 10.15

Gas Oil - I 250 - 300 10.11 9.97

Gas Oil - II 300 - 350 9.22 8.80

Gas Oil - III 350 - 400 8.96 8.20

Atmospheric Residue 400°C + 28.01 24.23

Vacuum Gas Oil - I 400 - 450 9.66 8.78

Vacuum Gas Oil - II 450 - 500 6.67 5.90

Vacuum Gas Oil - III 500 - 550 4.03 3.49

Vacuum Residue 550°C + 7.65 6.06

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 SUMMARY OF TRUE BOILING POINT DISTILLATION WIDE CUTS
LABORATORY REPORT NO: IDL-3961-2021(rev06)

50.00

30.00
% Yield

10.00

15 - 50 50 - 100 - 150 - 200 - 250 - 300 - 350 - 400°C 400 - 450 - 500 - 550°C
100 150 200 250 300 350 400 + 450 500 550 +

-10.00

% mass 2.35
Fraction Range (° C) % volume 3.23

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 Yield / D2892 Run % volume

LPG - Light Ends Gas,

3.23

Naphtha - I 15 - 50°C,
3.53

Naphtha - II 50 -
100°C, 9.35
Atmospheric Residue
400°C + , 24.23

Naphtha - III 100 -

150°C, 11.21

Gas Oil - III 350 -

400°C, 8.20

Kerosene - I 150 -
Gas Oil - II 300 - 200°C, 11.32
350°C, 8.80

Kerosene -II 200 -

Gas Oil - I 250 - 300°C, 250°C, 10.15
9.97

Yield / ATM Res % volume

Vacuum Residue
550°C + , 25.02
Vacuum Gas Oil - I
Vacuum Gas Oil - III 400 - 450°C, 36.24
500 - 550°C, 14.39

Vacuum Gas Oil - II

450 - 500°C, 24.35

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 LABORATORY REPORT NO: IDL-3961-2021(rev06)
WHOLE CRUDE PROPERTIES
Sample Descriptions: Qatar Land Crude Oil Sample
TEST METHOD UNIT RESULT
Density @ 15°C ASTM D5002 kg/L 0.8238
Specific Gravity at 60/60°F Conversion -- 0.8242
API Gravity @ 60° F Calculated -- 40.18
Ash Content ASTM D482 % Wt. <0.01
Asphaltenes IP 143 % Wt. <0.5
Basic Water and Sediment ASTM D4007 % Vol. 0.025
Distillation (Full) ASTM D86 °C Page No-23
Flash Point IP 170 °C Below-30
Mercaptan Sulphur UOP 163 ppm Wt. 298
Mercury UOP 938 ppb <1
Metals -
Sodium <1
Potassium <1
Copper <1
ICP ppm Wt.
Lead <1
Iron <1
Nickel <1
Vanadium 1.5
Kinematic Viscosity at 15°C ASTM D445 cSt 6.980
Kinematic Viscosity at 40°C ASTM D445 cSt 5.108
UOP K. Factor UOP 375 12.39
Pour Point ASTM D97 °C -15
Reid Vapour Pressure ASTM D323 psi 7.54
Salt Content ASTM D3230 PTB 1.49
Salt Content ASTM D3230 mg/L 4.25
Total Acid Number ASTM D664 mgKOH/g 0.14
Total Nitrogen ASTM D 4629 ppm Wt. 295
Hydrogen Sulphide (Liquid Phase) UOP 163 ppm Wt. 30
Hydrogen Sulphide (Vapour Phase) ASTM D5705 ppm Vol 2700
Total Sulphur Content ASTM D4294 % Wt. 1.486
Water Content ASTM D4006 % Vol. 0.05
Wax Content UOP 46 % Wt. <5
Light Ends -
Methane 0.0000
Ethane 0.0132
Propane 0.2373
IP 344 %wt.
i-Butane 0.1902
n-Butane 0.9653
i-Pentane 0.8985
n-Pentane 1.5455
Conradson Carbon Residue ASTM D189 % Wt. 1.35

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 LABORATORY REPORT NO: IDL-3961-2021(rev06)
Naphtha Fraction- I [C5-50°C]

Sample Descriptions: Qatar Land Crude Oil Sample

TEST METHOD UNIT RESULT

Initial BP °C C5

Final BP °C 50°C

Yield % Wt. 2.75

ASTM D2892 / D5236
Yield % Vol. 3.53

Density @ 15°C ASTM D4052 kg/L 0.6411

Specific Gravity at 60/60°F Conversion - 0.6412

API Gravity at 60°F Calculation - 89.18

Aniline Point ASTM D611 °C NP*

Mercaptan Sulphur UOP 163 ppm Wt. 805

Kinematic Viscosity at 50°C ASTM D445 cSt NP*

Kinematic Viscosity at 100°C ASTM D445 cSt NP*

Reid Vapour Pressure ASTM D323 psi 15.78

Total Acid Number ASTM D974 mgKOH/g 0.01

Total Nitrogen ASTM D4629 ppm Wt. <1

Total Sulphur Content ASTM D4294 % Wt. 0.069

C6 Paraffins ASTM D6730 % Vol 8.320

PIONA analysis -

Total paraffins 98.510

Olefins <0.01

iso- paraffins 42.482

ASTM D6730 % Vol
Total olefins <0.01

Total napthenes 1.394

Total aromatics 0.096

Unidentified <0.01
Note: Please note that the marked (NP*) results are unable to perform due to nature of the sample.

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 LABORATORY REPORT NO: IDL-3961-2021(rev06)
Naphtha Fraction- II [50-100°C]

Sample Descriptions: Qatar Land Crude Oil Sample

TEST METHOD UNIT RESULT

Initial BP °C 50°C

Final BP °C 100°C

Yield % Wt. 7.82

ASTM D2892 / D5236
Yield % Vol. 9.35

Density @ 15°C ASTM D4052 kg/L 0.6888

Specific Gravity at 60/60°F Conversion - 0.689

API Gravity at 60°F Calculation - 73.87

Aniline Point ASTM D611 °C 62.0

Mercaptan Sulphur UOP 163 ppm Wt. 435

Kinematic Viscosity at 50°C ASTM D445 cSt 0.352

Kinematic Viscosity at 100°C ASTM D445 cSt 0.254

Reid Vapour Pressure ASTM 323 psi 5.38

Total Acid Number ASTM D974 mgKOH/g 0.012

Total Nitrogen ASTM D4629 ppm Wt. <1

Total Sulphur Content ASTM D4294 % Wt. 0.084

C6 Paraffins ASTM D6730 % Vol 43.747

PIONA analysis -

Total paraffins 83.726

Olefins <0.01

iso- paraffins 37.226

ASTM D6730 % Vol
Total olefins <0.01

Total napthenes 12.496

Total aromatics 3.778

Unidentified <0.01

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 LABORATORY REPORT NO: IDL-3961-2021(rev06)
Naphtha Fraction -III [100-150°C]

Sample Descriptions: Qatar Land Crude Oil Sample

TEST METHOD UNIT RESULT

Initial BP °C 100°C

Final BP °C 150°C

Yield % Wt. 10.15

ASTM D2892 / D5236
Yield % Vol. 11.21

Density @ 15°C ASTM D4052 kg/L 0.7452

Specific Gravity at 60/60°F Conversion - 0.7454

API Gravity at 60°F Calculation - 58.33

Aniline Point ASTM D611 °C 55.0

Mercaptan Sulphur UOP 163 ppm Wt. 235

Kinematic Viscosity at 50°C ASTM D445 cSt 0.512

Kinematic Viscosity at 100°C ASTM D445 cSt 0.343

Reid Vapour Pressure ASTM D323 psi 0.77

Total Acid Number ASTM D974 mgKOH/g 0.02

Total Nitrogen ASTM D4629 ppm Wt. <1

Total Sulphur Content ASTM D4294 % Wt. 0.119

C6 Paraffins ASTM D6730 % Vol 0.475

PIONA analysis -

Total paraffins 69.663

Olefins 0.067

iso- paraffins 35.609

ASTM D6730 % Vol
Total olefins 0.067

Total napthenes 14.327

Total aromatics 15.674

Unidentified 0.269

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 LABORATORY REPORT NO: IDL-3961-2021(rev06)
Kerosene Fraction - I [150-200°C]

Sample Descriptions: Qatar Land Crude Oil Sample

TEST METHOD UNIT RESULT

Initial BP °C 150°C
Final BP °C 200°C
Yield % Wt. 10.76
ASTM D2892 / D5236
Yield % Vol. 11.32
Density @ 15°C ASTM D4052 kg/L 0.7827
Specific Gravity at 60/60°F Conversion - 0.783
API Gravity at 60°F Calculation - 49.22
Aniline Point ASTM D611 °C 53.5
Mercaptan Sulphur UOP 163 ppm Wt. 245
Kinematic Viscosity at 50°C ASTM D445 cSt 0.771
Kinematic Viscosity at 100°C ASTM D445 cSt 0.484
Pour Point ASTM D97 °C <-42
Total Acid Number ASTM D974 mgKOH/g 0.03
Total Nitrogen ASTM D4629 ppm Wt. <1
Total Sulphur Content ASTM D4294 % Wt. 0.145
Naphthalene content ASTM D1840 %Vol. 0.05
Smoke Point ASTM D1322 mm 26.0
PIONA analysis -
Total paraffins 55.161
Olefins 0.318
iso- paraffins 25.677
GC % Vol
Total olefins 0.318
Total napthenes 7.623
Total aromatics 31.593
Unidentified 5.305
Cloud Point ASTM D2500 °C <-42
Aromatics (FIA) 22.4
Olefins (FIA) ASTM 1319 % Vol. 0.4
Saturates (FIA) 77.2
Refractive Index @ 70° C ASTM D1218 1.4138

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 LABORATORY REPORT NO: IDL-3961-2021(rev06)

Kerosene Fraction - II [200-250°C]

Sample Descriptions: Qatar Land Crude Oil Sample

TEST METHOD UNIT RESULT

Initial BP °C 200°C

Final BP °C 250°C

Yield % Wt. 9.87

ASTM D2892 / D5236
Yield % Vol. 10.15

Density @ 15°C ASTM D4052 kg/L 0.8011

Specific Gravity at 60/60°F Conversion - 0.8015

API Gravity at 60°F Calculation - 45.04

Mercaptan Sulphur UOP 163 ppm Wt. 255

Kinematic Viscosity at 50°C ASTM D445 cSt 1.327

Kinematic Viscosity at 100°C ASTM D445 cSt 0.756

Pour Point ASTM D97 °C -39

Total Acid Number ASTM D974 mgKOH/g 0.032

Total Nitrogen ASTM D4629 ppm Wt. <1

Total Sulphur Content ASTM D4294 % Wt. 0.256

Naphthalene content ASTM D1840 %Vol. 1.57

Cetane Index ASTM D4737 53.4

Cloud Point ASTM D2500 °C -40

Conradson carbon residue ASTM D189 % Wt. <0.1

Aromatics (FIA) 18.8

Olefins (FIA) ASTM D1319 % Vol. 0.8

Saturates (FIA) 80.4

Refractive Index @ 70° C ASTM D1218 1.4264

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 LABORATORY REPORT NO: IDL-3961-2021(rev06)
Gas Oil Fraction - I [250-300°C]

Sample Descriptions: Qatar Land Crude Oil Sample

TEST METHOD UNIT RESULT

Initial BP °C 250°C

Final BP °C 300°C

Yield % Wt. 10.11

ASTM D2892 / D5236
Yield % Vol. 9.97

Density @ 15°C ASTM D4052 kg/L 0.8351

Specific Gravity at 60/60°F Conversion - 0.8355

API Gravity at 60°F Calculation - 37.86

Aniline Point ASTM D611 °C 69.5

Kinematic Viscosity at 50°C ASTM D445 cSt 2.286

Kinematic Viscosity at 100°C ASTM D445 cSt 1.156

Pour Point ASTM D97 °C -18

Total Acid Number ASTM D974 mgKOH/g 0.013

Total Nitrogen ASTM D4629 ppm Wt. 4

Total Sulphur Content ASTM D4294 % Wt. 0.677

Smoke Point ASTM D1322 mm 18

Cetane Index ASTM D4737 56.1

Cloud Point ASTM D2500 °C -18

Conradson carbon residue ASTM D189 % Wt. <0.1

Aromatics (FIA) % Vol. 24.8

Olefins (FIA) ASTM D1319 0.6

Saturates (FIA) 74.6

Refractive Index @ 70° C ASTM D1218 1.4458

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 LABORATORY REPORT NO: IDL-3961-2021(rev06)

Gas Oil Fraction - II [300-350°C]

Sample Descriptions: Qatar Land Crude Oil Sample

TEST METHOD UNIT RESULT

Initial BP °C 300°C

Final BP °C 350°C

Yield % Wt. 9.22

ASTM D2892 / D5236
Yield % Vol. 8.80

Density @ 15°C ASTM D4052 kg/L 0.8621

Specific Gravity at 60/60°F Conversion - 0.8626

API Gravity at 60°F Calculation - 32.54

Kinematic Viscosity at 50°C ASTM D445 cSt 4.338

Kinematic Viscosity at 100°C ASTM D445 cSt 1.876

UOP K. Factor UOP 375 11.85

Pour Point ASTM D97 °C +6

Total Acid Number ASTM D974 mgKOH/g 0.015

Total Nitrogen ASTM D4629 ppm Wt. 46

Total Sulphur Content ASTM D4294 % Wt. 1.60

Cetane Index ASTM D4737 60.1

Conradson Carbon Residue ASTM D189 % Wt. <0.1

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 LABORATORY REPORT NO: IDL-3961-2021(rev06)

Gas Oil Fraction - III [350-400°C]

Sample Descriptions: Qatar Land Crude Oil Sample

TEST METHOD UNIT RESULT

Initial BP °C 350°C

Final BP °C 400°C

Yield % Wt. 8.96

ASTM D2892/D5236
Yield % Vol. 8.20

Density @ 15°C ASTM D4052 kg/L 0.8995

Specific Gravity at 60/60°F Conversion - 0.9000

API Gravity at 60°F Calculation - 25.72

Kinematic Viscosity at 50°C ASTM D445 cSt 10.65

Kinematic Viscosity at 100°C ASTM D445 cSt 3.776

UOP K. Factor UOP 375 11.73

Pour Point ASTM D97 °C +21

Total Acid Number ASTM D974 mgKOH/g 0.025

Total Nitrogen ASTM D4629 ppm Wt. 258

Total Sulphur Content ASTM D4294 % Wt. 1.96

Conradson Carbon Residue ASTM D189 % Wt. <0.1

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 LABORATORY REPORT NO: IDL-3961-2021(rev06)

Vacuum Gas Oil Fraction - I [400-450°C]

Sample Descriptions: Qatar Land Crude Oil Sample

TEST METHOD UNIT RESULT

Initial BP °C 400°C

Final BP °C 450°C

Yield % Wt. 9.66

ASTM D2892/D5236
Yield % Vol. 8.78

Density @ 15°C ASTM D4052 kg/L 0.9055

Specific Gravity at 60/60°F Conversion - 0.906

API Gravity at 60°F Calculation - 24.68

Aniline Point ASTM D611 °C 88.0

Kinematic Viscosity at 50°C ASTM D445 cSt 32.03

Kinematic Viscosity at 100°C ASTM D445 cSt 7.742

UOP K. Factor UOP 375 11.79

Pour Point ASTM D97 °C +36

Total Acid Number ASTM D974 mgKOH/g 0.034

Total Nitrogen ASTM D4629 ppm Wt. 440

Total Sulphur Content ASTM D4294 % Wt. 2.18

Conradson Carbon Residue ASTM D189 % Wt. <0.1

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 LABORATORY REPORT NO: IDL-3961-2021(rev06)

Vacuum Gas Oil Fraction - II [450-500°C]

Sample Descriptions: Qatar Land Crude Oil Sample

TEST METHOD UNIT RESULT

Initial BP °C 450 °C

Final BP °C 500°C

Yield % Wt. 6.67

ASTM D2892 / D5236
Yield % Vol. 5.90

Density @ 15°C ASTM D4052 kg/L 0.9311

Specific Gravity at 60/60°F Conversion - 0.9316

API Gravity at 60°F Calculation - 20.39

Kinematic Viscosity at 50°C ASTM D445 cSt NP*

Kinematic Viscosity at 100°C ASTM D445 cSt 20.18

UOP K. Factor UOP 375 11.66

Pour Point ASTM D97 °C +51

Total Acid Number ASTM D974 mgKOH/g 0.12

Total Nitrogen ASTM D4629 ppm Wt. 750

Total Sulphur Content ASTM D4294 % Wt. 2.46

Conradson Carbon Residue ASTM D189 % Wt. <0.1

Note: Please note that the marked (*) results are unable to perform due to nature of the sample.

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 LABORATORY REPORT NO: IDL-3961-2021(rev06)

Vacuum Gas Oil Fraction - III [500-550°C]

Sample Descriptions: Qatar Land Crude Oil Sample

TEST METHOD UNIT RESULT

Initial BP °C 500°C

Final BP °C 550°C

Yield % Wt. 4.03

ASTM D2892 / D5236
Yield % Vol. 3.49

Density @ 15°C ASTM D4052 kg/L 0.9507

Specific Gravity at 60/60°F Conversion 0.9513

API Gravity at 60°F Calculation -- 17.24

Kinematic Viscosity at 50°C ASTM D445 cSt NP*

Kinematic Viscosity at 100°C ASTM D445 cSt 34.96

UOP K. Factor UOP 375 11.57

Pour Point ASTM D97 °C +54

Total Acid Number ASTM D974 mgKOH/g 0.21

Total Nitrogen ASTM D4629 ppm Wt. 820

Total Sulphur Content ASTM D4294 % Wt. 2.92

Conradson Carbon Residue ASTM D189 % Wt. 0.10

Note: Please note that the marked (*) results are unable to perform due to nature of the sample.

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 LABORATORY REPORT NO: IDL-3961-2021(rev06)

Atmospheric Residue - [400°C+]

Sample Descriptions: Qatar Land Crude Oil Sample

TEST METHOD UNIT RESULT

Initial BP °C 400°C
Final BP °C 400°C+
Yield % Wt. 28.01
ASTM D2892 / D5236
Yield % Vol. 24.23
Density @ 15°C IP 365 kg/L 0.9513
Specific Gravity at 60/60°F Conversion 0.9519
API Gravity at 60°F Calculation -- 17.15
Asphaltenes IP 143 % Wt. 0.68
Aniline Point ASTM D 611 °C 99.0
Metals -
Sodium <1
Potassium <1
Copper <1
IP 501 mg/kg
Lead <1
Iron <1
Nickel <1
Vanadium 4
Kinematic Viscosity at 50°C 199.3
Kinematic Viscosity at 100°C 25.32
ASTM D445 cSt
Kinematic Viscosity at 135°C 10.14
Kinematic Viscosity at 175°C 5.042
Pour Point ASTM D 97 °C -6
Total Acid Number ASTM D 664 mgKOH/g 0.23
Total Nitrogen ASTM D 4629 ppm Wt. 835
Total Sulphur Content ASTM D 4294 % Wt. 2.55
Cloud Point ASTM D 2500 °C NP*
Conradson Carbon Residue ASTM D189 % Wt. 5.89
Refractive Index @ 70° C ASTM D 1218 1.5170
Note: Please note that the marked (*) results are unable to perform due to nature of the sample.

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 LABORATORY REPORT NO: IDL-3961-2021(rev06)

Vacuum Residue - [550°C+]

Sample Descriptions: Qatar Land Crude Oil Sample

TEST METHOD UNIT RESULT

Initial BP °C 550°C
Final BP °C 550°C+
Yield % Wt. 7.65
ASTM D2892 / D5236
Yield % Vol. 6.06
Density @ 15°C IP 365 kg/L 1.0335
Specific Gravity at 60/60°F Conversion 1.0342
API Gravity at 60°F Calculation -- 5.32
Asphaltenes IP 143 % Wt. 8.81
Aniline Point ASTM D611 °C >160
Metals -
Sodium <1
Potassium <1
Copper <1
IP 501 mg/kg
Lead <1
Iron <1
Nickel 7
Vanadium 29
Kinematic Viscosity at 50°C NP*
Kinematic Viscosity at 100°C 670.0
ASTM D445 cSt
Kinematic Viscosity at 135°C 129.5
Kinematic Viscosity at 175°C 47.50
Pour Point ASTM D97 °C +51
Total Acid Number ASTM D664 mgKOH/g 0.18
Total Nitrogen ASTM D4629 ppm Wt. 1950
Total Sulphur Content ASTM D4294 % Wt. 4.20
Cloud Point ASTM D2500 °C NP*
Conradson Carbon Residue ASTM D189 % Wt. 25.45
Refractive Index @ 70° C ASTM D1218 1.5877
Note: Please note that the marked (*) results are unable to perform due to nature of the sample

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 LABORATORY REPORT NO: IDL-3961-2021(rev06)

WHOLE CRUDE - ASTM 86 - DISTILLATION DATA

Sample Descriptions: Qatar Land Crude Oil Sample

TEST METHOD UNIT RESULT

Initial Boiling Point 37.0

5% Recovered 68.0

10% Recovered 90.0

20% Recovered 132.0

30% Recovered 173.0

°C
40% Recovered ASTM D86 212.0

50% Recovered 262.0

60% Recovered 314.0

70% Recovered 364.0

Cracked at 375.0

Recovery % Vol. 73.0

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Sulphur Content
Sulphur Content,…

Sulphur Content,… Sulphur Content, 100- Sulphur Content,…

150°C, 0.119

Sulphur Content,… Sulphur Content,…

Sulphur Content,
550°C +, 4.200 Sulphur Content,…

Sulphur Content,…

Sulphur Content,…

Sulphur…

Sulphur Content,…

Gas 15-50°C 50-100°C 100-150°C 150-200°C 200-250°C 250-300°C

300-350°C 350-400°C 400-450°C 450-500°C 500-550°C 550°C +

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 50-100°C, Total Acid
Total Acid Number Number, 0.012
100-150°C, Total Acid
Number, 0.020

15-50°C, Total Acid 150-200°C, Total Acid

Number, 0.010 Number, 0.030

200-250°C, Total Acid

550°C +, Total Acid Number, 0.032
Number, 0.180
250-300°C, Total Acid
Number, 0.013

300-350°C, Total Acid

Number, 0.015

350-400°C, Total Acid

Number, 0.025

400-450°C, Total Acid

Number, 0.034

450-500°C, Total Acid

Number, 0.120
500-550°C, Total Acid
Number, 0.210

Gas 15-50°C 50-100°C 100-150°C 150-200°C 200-250°C

250-300°C 300-350°C 350-400°C 400-450°C 450-500°C 500-550°C

26 of 26