Optimized Process Design (3PH Seperator)
Optimized Process Design (3PH Seperator)
John T. Small
Process Engineer
TABLE OF CONTENTS
1. INTRODUCTION
3. CASE STUDY:
3.1 Summary
3.4 Results
4. NOMENCLATURE
5. REFERENCES
1. INTRODUCTION
The 3- phase separator configuration which forms the basis for this work is
illustrated above.
At the same time, separator performance and control are often critical to
successful operation of downstream equipment such as de-oiling, de-
watering and gas compression units.
It follows that there is a strong incentive to minimize the size of the vessel
and associated piping whilst achieving satisfactory performance in the
separation, process control and safeguarding functions.
· Type of inlet device, and its impact upon the size of inlet pipework and
the dimensions of the separator vessel.
The objective function of the Solver algorithm may be set to minimize the
volume of a separator vessel for the selected design parameters and
constraints, or the engineer may choose other targets for optimization such
as length of the gravity settling zone.
This section discusses the technical references and criteria that were
considered in development of the salient features of the 3-phase separator,
the input design parameters and constraints that are required for execution
of the separator dimensioning calculations, how to navigate the results
panel, and lastly, the architecture of the spreadsheet.
· Slenderness Ratio
The Inlet Zone components of the 3-phase separator are generally defined in
accordance with GPSA (2012) to include the feed pipe, inlet nozzle and inlet
device. In addition, a flow straightening baffle is included downstream of the
inlet device.
In compliance with GPSA and API 12J (2008), bulk phase separation is
deemed to take place in the Inlet Zone during steady state operation.
The feed pipe, inlet nozzle and inlet device are therefore considered to have
the same internal diameter.
The engineer calculates component diameters which meet velocity head and
erosional criteria, as described below. The spreadsheet selects from a look-up
table the pipe diameter which satisfies the more stringent sizing criterion.
The allowable velocity head J at the inlet device, and by extension in the feed
pipe and inlet nozzle, depends on its design configuration.
Having selected a particular type of inlet device, the engineer inputs to the
calculation panel for the inlet nozzle a value for allowable velocity head J.
GPSA (2012) cites typical allowable velocity head ranges for various types of
inlet device:
The size of the feed pipe, inlet nozzle and inlet device must also be great
enough to satisfy erosional constraints during the service life of the
separator.
DNV has developed models for prediction of erosive wear rates in the
standard steel piping components found in oil and gas facilities. Grounded in
the results of experimental investigations, the models enable sizing of
pipework components based on the physical properties of the sand particles,
the process fluid, and the pipework, taking account also of piping geometry.
The upper edge of the inlet nozzle at (hɪɴ + Di) should be located as close as
permissible to the top of the vessel head, since this tends to minimize vessel
diameter Di. The proximity is however constrained by mechanical
considerations to a certain proportion of Di.
The proportion (hɪɴ + Di) / Di is defined by the engineer and is input to the
Design Parameters as a value labelled Rɪɴ.
The purpose of the flow straightening baffle downstream of the inlet device is
to induce plug flow conditions in the Gravity Settling Zone, which is
discussed further in Section 2.2.3 below. The location of the baffle relative to
the vessel seam defines the axial length of the Inlet Zone and is labelled Lɪɴ.
The engineer inputs to the Design Parameters a fixed value for Lɪɴ.
In this work, the principal calculation method for the phase separation aspect
of separator sizing is based on settling theory, according to which droplets /
bubbles of certain diameters settle to their respective continuous phases
within the Gravity Settling Zone.
It is assumed that by designing the separator using settling theory for certain
droplet sizes, all droplets of that size and larger settle out at terminal
velocity to their respective continuous phase.
The gas phase holdup time in the Settling Zone needs to be sufficient for
liquid droplets to settle out to the surface of the oil. Similarly, the holdup
times of the oil and water phases need to be sufficient for settle out of gas
bubbles and liquid droplets from the respective dispersed phase.
Noting that the terminal velocity for a given droplet size increases according
to the density difference between the continuous and dispersed phases,
Grødal and Realff (1999) highlight for each continuous phase the settling
process which governs holdup time requirements in a 3-phase separator:
The engineer inputs to Design Parameters for each fluid phase the minimum
diameter droplet that is to settle out in the Gravity Settling Zone:
The engineer calculates for each continuous phase the terminal settling
velocity of dispersed droplets/bubbles using Goal Seek function, as per step
number 4 in Section 2.10 below.
Arnold and Stewart (2008) cite field experience which suggests that selecting
an oil droplet size dᴏɢ = 140 microns results in adequate oil removal from
the gas phase.
The relative densities of the oil and water constituents being similar, the
settling velocity of dispersed phase droplets is strongly influenced by the
viscosity of the continuous phase. Oil viscosity is typically the order of 10
times that of water, therefore it is more often the allowable water droplet
diameter that determines the dimension Lᴇꜰꜰ for oil/water separation.
Arnold and Koszela (1990), writing from the perspective of design engineers,
have reported good results sizing separators based on water droplet
diameters dᴡᴏ = 500 – 1000 microns.
The separator was found to be oil capacity limited, with a minimum water
droplet diameter dᴡᴏ = 960 microns.
Arnold and Stewart (2008) suggest allowable oil droplet size dᴏᴡ = 200
microns for flotation of oil from the water phase.
The balance of forces upon which settling theory is predicated applies strictly
to horizontal plug flow of the continuous phase, as discussed in GPSA (2012),
therefore it is necessary to define the serviceable length of the Gravity
Settling Zone.
The Gravity Settling Zone also contributes to other functions such as liquid
holdup to meet Design Constraints on level control, surge / slug volumes,
and where specified, liquid retention times. These functions may force
extending Lᴇꜰꜰ beyond what is required to accommodate the settling
process.
The engineer inputs to the calculation panel a trial value for Lᴇꜰꜰᵀᴼᵀᴬᴸ.
These values affect the thickness of the respective layers and therefore
influence Lᴇꜰꜰ.
The engineer may wish to consider the following factors when setting values
for Uᴡᵐᵃˣ and Uᴏᵐᵃˣ:
· GPSA (2012) mentions using a maximum axial velocity of 0.015 m/s for
the oil and water continuous phases, in a horizontal separator design with
target droplet diameters of 150 microns.
The gas outlet pipe and nozzle are assumed to have the same internal
diameter. They are sized to meet the more stringent criterion of allowable
velocity head and erosion rate. The engineer calculates component
diameters which meet velocity head and erosional criteria, as described
below. The spreadsheet selects from a look-up table the pipe diameter which
satisfies the more stringent sizing criterion.
The engineer inputs to the calculation panel for the gas outlet nozzle, a value
for allowable velocity head J .
GPSA (2012) quotes industry guidelines of J = 4500 - 5400 Pa for gas outlet
nozzles.
From the perspective of erosion rate, it is assumed that the size of the gas
outlet nozzle and outlet pipe is limited by a pipe bend component in the
outlet pipe.
The engineer calculates the nozzle diameter required to meet the erosion
target using Goal Seek function as per step number 6 in Section 2.10 below.
Velocity Criterion
The engineer inputs to the calculation panel for the water outlet nozzle, a
value for allowable velocity Uɴ,ᴡᵐᵃˣ.
The value may be selected from the ranges presented in API RP 14E (1991):
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The engineer calculates the nozzle diameter required to meet the erosion
target using Goal Seek function as per step number 6 in Section 2.10 below.
The axial length of the Water Outlet Zone is defined by the width of the
vortex breaker on the water outlet, which the spreadsheet calculates to be
twice the nozzle diameter as per Rochelle and Briscoe (2010).
The outboard edge of the Water Outlet Zone is assumed to abut the inboard
side of the weir.
Dimensioning of the oil outlet nozzle is analogous to the water outlet nozzle.
The engineer inputs to the calculation panel for the oil outlet nozzle, a value
for allowable velocity Uɴ,ᴏᵐᵃˣ.
The range of allowable velocity values is similar to the water outlet nozzle.
The engineer then calculates the oil outlet nozzle diameter required to meet
the erosion target rate Eᵐᵃˣ using Goal Seek function as per step number 6 in
Section 2.10 below.
The Oil Outlet Zone extends axially from the outboard side of the weir to the
vessel seam line.
The width of the Oil Outlet Zone is deemed to be the same as the oil outlet
vortex breaker, which the spreadsheet calculates at twice the diameter of
the oil outlet nozzle as per Rochelle and Briscoe (2010).
The outboard axial limits of the liquid volumes are demarcated by the weir
plate.
The engineer may specify values in Design Constraints for minimum required
oil and water retention times tʀᴇꜱ,ᴏᴹᴵᴺ and / or tʀᴇꜱ,ᴡᴹᴵᴺ. In this case the
spreadsheet dimensions a separator which meets the more stringent criteria
of retention times or droplet removal.
The engineer may have access to field data for separation based on oil and /
or water retention times or they may wish to follow guidelines for retention
times such as those referred to below.
Arnold and Stewart (2008) cite oil and water retention times ranging from
180 to 600+ s depending on the density and viscosity of the oil.
The cost of a vessel increases in line with the diameter, whereas excessive
gas velocity results in re-entrainment of oil droplets into the gas phase. Thus,
the scope for reduction of vessel diameter and cost may be constrained by
the requirement to avoid re-entrainment.
This work uses the correlations which Ishii and Grolmes (1975) developed
based on their experiments, to find the maximum velocity difference
between the gas phase and the oil layer which precludes re-entrainment of
oil droplets into the gas phase.
The engineer requires to input a value for oil-gas surface tension in Design
Parameters.
Monnery and Svrcek (1994) provide guidelines for setting the maximum
slenderness ratio as a function of operating pressure.
Viles indicates that these values of slenderness ratio are based on negligible
oil velocity relative to gas, leading to a conservative evaluation of separator
diameter.
Resolution of the level control and trip settings is a key part of the vessel
sizing calculation.
Level control points are assigned at LIL, NIL, HIL; LLL, NLL, HLL; process trip
points are assigned at LLIL, HHIL; LLLL, HHLL.
The height differences and holdup times between contiguous level control
points and trips for the respective liquid layers are evaluated in compliance
with NORSOK P-002 (2014).
For the purposes of level control calculations:
The engineer inputs to the vessel calculation panel trial values for:
· hᴛᴠ :hʜʜʟʟ :hʜʟʟ :hɴʟʟ :hʟʟʟ :hʟʟʟʟ :hʜʜɪʟ/hᴡᴇɪʀ :hʜɪʟ :hɴɪʟ :hʟɪʟ
Transient intermittent flow conditions may occur in the feed pipe to the
production separator, resulting in the arrival of alternating slugs of liquid and
essentially dry surges of gas.
The engineer may enter values in Design Constraints for the minimum
acceptable volumes of slugs Vꜱʟᴜɢᴹᴵᴺ and surges Vꜱᴜʀɢᴇᴹᴵᴺ.
It is assumed that level trip loops are designed with the appropriate SIL
ratings and when initiated will cause closure of ESD valves in the separator
inlet and outlet lines.
However, separator ESD valves are often large, requiring significant time to
close. This may be considered when setting the trip levels.
The engineer may enter a value in Design Constraints for the minimum
acceptable holdup time ∆t ꜱᴀꜰ(ʟʟʟʟ)ᴹᴵᴺ between the LLLL trip and the top of
the oil outlet vortex breaker sufficient to prevent gas blow-by during closure
of the ESD valve.
Note that the spreadsheet calculates the top of the vortex breaker to be at a
height equal to the diameter of the oil outlet nozzle, as per Rochelle and
Briscoe (2010).
Transient flooding of the separator inlet line during closure of the inlet ESD
valve following HHLL trip, may cause gross carryover of oil into downstream
gas processing equipment, leading to machinery damage.
The engineer may enter a value in Design Constraints for the minimum
height difference ∆hꜱᴀꜰ(ʜʜʟʟ)ᴹᴵᴺ between the HHLL trip and the lower edge of
the inlet nozzle to meet the desired allowance for closure time of the inlet
ESD valve.
LLIL is set coincident with the top of the water outlet vortex breaker, since
transient breakthrough of oil into the water treatment system while the inlet
ESD valve is closing, would not lead to escalation of the incident.
Note that the spreadsheet calculates the top of the vortex breaker to be at a
height equal to the diameter of the water outlet nozzle, as per Rochelle and
Briscoe (2010).
Transient gas blow-by via the water outlet is not considered a credible
scenario.
HHIL is set coincident with the top of the weir, since transient carryover of
water into the oil compartment would not lead to escalation of the incident.
Foaming Allowance
Foaming oil may potentially cause spurious operation of the HHLL trip.
The engineer may enter a value in Design Constraints for the minimum
height allowance for foaming ∆h ꜰᴏᴀᴍᴹᴵᴺ.
to impose a minimum allowable control interval between HLL and HHLL.
The main panel of results for the design calculations shows the level control
heights in semi-graphical format, with final values for the engineer’s design
constraints at the appropriate levels.
The upper part of the main panel shows final values for the dimensions of
the vessel and nozzles.
Below the main panel are final values for the length of the Gravity Separation
Zone, and the mass and volume of each phase of the vessel inventory.
This Case Study estimates the minimum size of a 3-phase separator vessel
and associated nozzles required to achieve satisfactory performance in the
separation, process control and safeguarding functions, taking account of the
large variation in water-cut which occurs during its design life.
The peak oil flow case is 100,000 BPD oil, with 25% water-cut: peak water
flow case entails the same total flow, with 75% water-cut. Gas flow is a
constant 40,000 m³/day at separator conditions.
Droplet settling theory and oil retention time are both considered.
Vessel sizing was based upon settling theory, using oil and water droplet cut-
off sizes in the range recommended by Arnold and Stewart (2008), in
conjunction with production fluid density and viscosity data for a North Sea
production separator which was studied by Laleh et al (2013).
Fluid axial velocities and oil residence time were constrained to the values
that were observed in the field for the North Sea separator, which reportedly
operated successfully. This allowed a degree of validation of the Case Study
model and results.
Key Results:
The half-pipe inlet device entails a 24” NB inlet pipe vs 20” NB for the
diffuser device. The half-pipe inlet device results in 539 kg larger
hydrocarbon inventory. This data should be assessed by Mechanical, Piping,
and Technical Safety disciplines to decide on the preferred inlet device.
The peak oil production rate is 100,000 BPD during early field life, with a
water cut of 25%; that is to say, coincident water production rate is 33,348
BPD.
The peak water production rate occurs in late field life, when water cut rises
to 75%, while total liquid production rate remains constant; oil and water
production rates are then respectively 33,337 BPD and 100,011 BPD.
The oil, gas and water feed properties correspond to a North Sea production
separator which was studied by Laleh et al (2013).
The separator was designed to deliver water effluent wherein oil droplets are
no larger than 200 microns, and oil effluent wherein water droplets are no
larger than 750 microns. These performance criteria are recommended by
Arnold and Stewart (2008). Note that the production separator studied by
Laleh et al (2013) operated successfully with a less stringent water droplet
cutoff size, of 960 microns.
All nozzles were sized adequately for the full range of flowrates, according to
velocity, velocity head and erosion criteria.
For the diffuser and the half-pipe inlet devices, respective allowable velocity
head values of 7500 Pa and 2600 Pa were selected; these values lie in the
middle of the respective ranges recommended by GPSA (2012).
A minimum height difference of 0.1 was imposed between HHLL and the
lower edge of the inlet device, to avoid transient flooding of the inlet
following HHLL trip.
Maximum axial velocities of oil and water were constrained to 0.2 and 0.1
m/s at NLL and NIL respectively. These correspond with velocities observed in
a North Sea production separator which was operating successfully, as
reported by Laleh et al (2013).
3.4 Results
The key calculation input data and results for these cases are illustrated
below in Figure 3.1 to 3.4.
Comparison of the results in Figure 3.2 vs Figure 3.4 shows that the Peak
Water case requires a much larger separator vessel than the Peak Oil Case.
Water and oil nozzle sizes are larger for the respective cases, as would be
expected. Inlet and gas outlet nozzle sizes are the same for each case.
The more conservative vessel and nozzle dimensions were then combined in
a separator model, to calculate fluid inventories.
The Peak Water case fluids were then used to calculate optimized vessel
dimensions and nozzle sizes based on a half-pipe inlet device. The results are
shown in Figure 3-5.
Arntzen, R.: “Level Design and Control in Gravity Separators”, Oil and Gas
Facilities, September 2016
GPSA (2012). Engineering Data Book, (13th Ed.). Tulsa, OK: Gas Processors
Suppliers Association
Grødal, E.O. and Realff, M.J.: “Optimal Design of Two- and Three-Phase
Separators: A Mathematical Programming Formulation”, Paper SPE 56645,
presented at the 1999 SPE Annual Technical Conference and Exhibition,
Houston, TX, USA, Oct. 3-6, 1999
Hansen, E.W.M., Heitmann, H., Laska, B., and Loes, M.: “Numerical
Laleh, A.P., Svrcek, W.Y. and Monnery, W.D.: “Computational Fluid Dynamics-
Based Study of an Oilfield Separator - Part II: An Optimum Design”, Oil and
Gas Facilities, February 2013
NORSOK (2014). Process System Design – NORSOK Standard P-002 (1st Ed.).
1326 Lysaker, Norway: Standards Norway
Rochelle, S.G. and Briscoe, M.T.: “Predict and Prevent Air Entrainment in
Draining Tanks”, Chemical Engineering, November 2010
Small, J.T. (2022). Optimal Process Design of 2-Phase and 3-Phase Production
Separators for Offshore Oil and Gas Installations : Amazon Kindle Direct
Publishing