'F - 14401

Register No.

BTech Degree Examination December 2022

Fifth Semester
Chemical Engineering .
20CHT51 -MASS TRANSFER -I
(Regulations 2020)
Use of psychometric chart is permitted
Time: Three hours Mafamun: 100 marks
Answer all Questions
Part -A (10 x 2 = 20 marks)
1. Ammonia is diffiising through an inert air at 0°C and 1 atm with diffusivity 0.|98 cm2/s. [CO1,K3]
Determine the diffusivity if the temperature is 20°C and pressure is 1 atm.
2. Recall the types of solid diffusion. [coi,Ki]
3. Carbon dioxide is being absorbed form air by water with a rate of [C02,K3]
7.138 x 10-6 kmol / m2s. Determine mass transfer coefficient, if pressure gradient is 0.2 atm.
4. Mention the name of various theories involved in intexphase mass transfer, [C02,K1]
5. Highlight the significance ofabsolption factor? [Co3,K3]
6. Determine height of the absorption column, if NTU=5, [C03,K3]
kmol
KGa=50 Gavg = 100kmol/m2®h andpt = 1 atm.
h.m3 atm '
7. What is the effect oftemperafure and pressure on adsoaption isotherms? [C04,K2]

8. List any two industrial applications of ion exchange process® [C04,K1]

9. Illustrate how the wet bulb temperature is measured? [C05,K2]

loo Estimate absolute humidity for the air-water sample has a humid heat of 1032 J / kg°C. [C05,K3]

Part -8 (5 x 16 = 80 marks)
11. a. i) In a gas mixture of hydrogen and oxygen, steady state equimolar counter (8) [C01,K3]
diffusion is occurring at a total pressure of 100 kpa and temperature of 20°C. If
the partial pressures of oxygen at two planes 0.01 in apart, and perpendicular to
the direction of diffusion are 15 kpa and 5 kpa, respectively and the mass
diffusion flux of oxygen in the mixture is I.6 x 10 -5 kmol/in 2sec, calculate the
molecular diffusivity for the system.
ii) Acetic acid is diffusing through a film of non-diffusing water solution 3 mm (8) [CO1,K3]
thick at 20°C. The concentrations ( by weight) on opposite sides of the fiha
are 12% and 6% acid. The diffusivity of acid in the solution is
o.9 x |O-9m2 /S. Determine the rate of diffusiolf of acetic acid if the density
of 12% and 6% acid fry weight) are 1015 kg/m3 and 1006 kg/m3 respectively.
. (OR)
Derive an expression for the steady state diffusion of Gas A through a stagnant film (16) [CO1,K3]
of non-diffiising Gas 8 and equimolal counter diffusion of Gas A and a.
a 12. a. In an experimental study pfabsorption ofanmonia by water in a wetted wall column
(16) [C02,K2]
the overall gas phase mass transfer coefficient, KG was estimated as 2.72 x ,104
kmol/m2 s atm. At one point in the column the gas contained 10 mol % ammonia and
the liquid phase concentration was 6.42 X10-2 kmol NH3/m3 of solution.
Temperature is 293 K and the total pressure is I atm. 85% of the resistance to mass
tl.ansfer lies in gas phase. If Heury's law constant is 9.35 X 10~3 atm. m3/kmol9
calculate the individual film coefficient and the interfacial composition.
 b® i) Sketch out four stage cross-cur(e°nE)6qscade process, also derive an (|o) [C02,K2]
operating line equation for steady state counter-current Process.
ii) Explain the concept of operating hale, equilibrium curve and stage (6) [C02,K2]
efficiency in mass transfer processes. LE

SAn effluent gas containing 12% C6H6 is to be scrubbed in a packed column, (16) [903.K3]
13o ao

operating at 43°C and 1 ath. pressure. The column is to be designed for treating
15m3ofeuteringgasperhourperm2ofcolunncross-section,suchthattheefitgas
will contain 1% benzene. The solvent for scrubbing is mineral oil which will enter
the top of the column at a rate of 28 kmoTh m2 and a benzene content of 1°/o.
Detemine the height of the colurm assuming height of transfer unit,to be 0.75 in.
The equilibrium concentration at the operating conditions is given by j/* = 0.263x,
where jg and y are in mole fraction units.
(OR)
(16) [C03,K3]
bo It is desired to absorb 95% of acetone from feed mixture of acetone and air
containing 2 (mole) a/o of acetone using a liquid flow rate of 20 % more than the
minimum. Gas flow rate is 450 kgth. The gas mixture enters at 25°C and 1 atm
pressure,whichistheoperatingcondition.Theequilibriumrelationis}J*=2.5x.Find
(i) Flow rate of water, and (ii) Number of theoretical plates, when the operation is
caHied out countercurently.

i) Explain in detail about nature ofadsorbents and types ofadsoxption. (8) [C04,K|]
14® a.

ii) Calculate the amount of activated carbon required per 1000 kg of impurity free (8) [C04,Kl]
solution to reduce the impurity concentration form 1.5 to 0.5 kg/kg of impurity
free solution using i) A single stage operation ii) A two stage cross-current
operation with intermediate composition of 0.9 g of colouring impurity per kg
ofimpurityfreesolution.Equilibriumdata:Y=0.004X2
Where, Y is g colouring impurityckg impurity free solution and X is g colouring
impurity/kg activated carbon.
(OR)
Comparefixedbedandmovingbedionexchangeprocesswithneatdiagran. (16) [C04,K1]

15. a. Am air a)-water vapor (A) sample has a dry bulb temperature 55°C and an absolute (16) [CQ5,K3]

humidity 0.03kg water/kg dry air at lstd atm pressure. Calculate (i) saturation
humidity (ii) percentage humidity (iii) molal absolute humidity (iv) partial pressure
(v) relative humidity (vi) Humid heat (vii) Enthalpy (viii) humid volume. Assume
vapour pressure is 118 mm Hg at 55°C.
(OR)
b. i) Outline the adiabatic and non-adiabatic humidification processes involved in (6) [C05,K3]
industries.
ii) Identify the types of cooling tower applied in industries and explain working (|o) [C05,K3]
principle of any tvyo 'types with neat sketch. ,

Bloom's Remembering Understanding Applying Analysing Evaluating Creating

Taxonomy Level (K1) ur2) Or3) Or4) (K5) (K6)
Percentage 21 20 59

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