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20 views2ND PUC CHEMISTRY LAB EXPERIMENTS
The document outlines various chemical reactions, observations, and calculations related to titration experiments involving KMnO4 and ferrous ammonium sulfate (FAS). It details the principles of oxidation-reduction reactions, the procedure for titration, and the results including molarity calculations. Additionally, it includes qualitative analysis of inorganic salts, identifying acidic and basic radicals through various tests.
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0% found this document useful (0 votes)
20 views2ND PUC CHEMISTRY LAB EXPERIMENTS
The document outlines various chemical reactions, observations, and calculations related to titration experiments involving KMnO4 and ferrous ammonium sulfate (FAS). It details the principles of oxidation-reduction reactions, the procedure for titration, and the results including molarity calculations. Additionally, it includes qualitative analysis of inorganic salts, identifying acidic and basic radicals through various tests.
Uploaded by
mohammedzaidmk4Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF or read online on Scribd
/ 80
-——— oe
CHEMICAL REACTION:
ZKMnOy + BH,60y +10 FeSO, (NHy.),S0y,'6H,0 —7 KpS0y:
+ 2MnSQ, + 5 Fe, (S0yrs + 68H,
OBSERVATION :
17 Burette KMn0y. solution i
27 Conical flask ; foml of OLMFAS + 1 test tube ean
2
37 Indicator > KMnOy, ig self éndicator
uy Encl point : Cofourless to pink
OL | VOLUME OF) BurRETTE READINGS; VOLUME OF |
FAS IN KMnoy, Use
No ml INTIAL o| FINAL cp] NPE SD
O1-| 10 mh 0-0 | lol 10° |
O2-| 10 mt 00 VS q°3
03+] 10mé 0:0 13 :]
CALCULATIONS : : i
QrnyV, (KMnO,) = C,m,V, (FAS)
a; Cno of e-gain|molecule)= 5 4G, (n° of e~ loss/molecub,) =1
my (molerity of KMngj) = 7 mz,Cmolarity of FAS) = o-l1
Vi Cvolume of kmny)=9-3ml Vz (volume of FAS) = [Om
m= Gate 5 IxD1X10 . 992m
a 5 xXUs Vent = 1 [titemarie Auavsis] |
Tani tua falty of Hey
[olution —by titrating it agninst__0-1\A_sta, anclorol
solution of ferrous” sunmoniiu sulphate (EAS)
li
PRINCIPLE
ita Hlection nd recluction
takes place ,hence_it is .a_vedoxxeaction Tron_is_oxid'—
iseol KMao, fo +3 from_+2_oxidation_state- Ma —_|
in ‘atta, _suduced ta__+2_pom_+7 0 ichilion state |
nd__hence _KMndy is _sacts (dizi
FAS_os sa ducluting agent:
Proc EDURE.
Exact! pieetted into a clean .conical|
: loml “of 0-1mM FAS ts
7% f (c K (< (i a. Ak ( QO, QKE,
th ptill b
|| _Molarity of KMndy golutton = 0-02 M ___|
' {Stag af tate Si ees aeglh
= 0 OR XL5B 23h 4 L CHemical REACTION:
ZKMnO, f SHySOy + 5H,C2%y —7 KyS0y. +. MnS0y t 4,0
+10C0Oz
OBSERVATION:
Y Burette > KMady olution . |
27 Conical flask + 1Omf of Hata, + Ltest tube full of a
37 Inclicector KMno, Caele énclicocor)
W End point — Colourless to pale pink |
TABULAR Column :
, [Volume of Bun : Volume of saa |
St i ye unt Re ee]
no [OME Ace in TT Fritial OD fea Kg USGS
o1-| Lome 0-0 ml 1o-1 me 1o:1m£
o2- Lome o-oml 49 mo 2-9 me |
034 Lome o-oml Vd mo 9-4me |
CALCULATIONS © QiMiY) (KMnOy) = Q2MVa(Hy62 Oy
electrons Q, (ro of electrons
a ae molecule) =5 oe molecule’) =
M, CMolavity of = 7 M, (Moloaity o. r Al
‘ Eno : a all Lp aa
Vi C¥olume of = 4m Vy (Volu
2 (Volume of ~
KMn0q) Cralic ded) = Jo ml
My =Q2MV2_ = 2x01 xi
—4 Vv. = 0:04M —~)
PRINCIPLE °
Jin__this experiment _kMno
oxidizes _oxalic_acicl_into|
LJ -ondl 10 Hent Kroin_valure_of ol ncid_ts
‘trateol
ESULT
Molarct
of KMn04 solution = 0-04M.
lolectlay
fA XG
Loeigkt _
‘Teacher's Signature
=€329/L - _Execeiment 5
—__AYSTEMATIC QUALITATIVE An
NALYSIS OF AmPLE —
———Tnorganic fant [Geverat PeocepurE | —
i PRELIMINARY Test
Experiment | as ervarion _|_ Jv FERENCE!
ATATE
4 | -Ceystantine/
| Amor Hous’
37 SOLUBILIT WATER Dit- HC!
ig of the dott in_| Hot |Conp | Hor | COLD
the tect tube + 2mf
___of the solvent, ahate
well | |
_g Detection 02 Acid Rapicans [Anion
| EXPE RYA INEERENCE |
| Aolt t+ dif-Hel (S; “i el Tap acid
! rolical i. |
put ent
|_ thse the gas through | Lime watertums milky | Trolicortes
|_| ime —twartore caxtonate (c0%})
No efferyeacerce
Teacher's Signature
cil
Wicd obcrd | —
al ab - he | bot ‘ion, a cial
[Taube +2 drops lof come | gas +4 ay pga
Ht precio
Cole. sess futing gu tx odes Cloich
evolved + fon
Real _vapours_axe___|noliccibe_ Brom
evolved: lon
No _vaction tn cold:|Ci~ Bré are
absent
Yo the above olution | Evolution of xeold ish |
wand heat:
odd copper turning <__ broton gas
(_nttrate|
|Wo reddish brocon_|
gas:
(NOx) Cs absert
—| Aolurtion_of -the_salt-+
HCL
[Thick cohite_prep (pital
| tngoluble in excess _|
rerio
of oil uel S027 Us paccent
‘Teacher's Signature |_| pass the yapouru _troudl|
E rime epee te 7 :
|| test for 2" oraup zacicl 7| ae -
_|_-radecal- oe
Expt No
Test for 1 you atid
radical: pep
Salt + water heat and —_|
Page No,
| Lime _tooder dloes
-not turn _midky -
Aonfirmetory test for .acicl vraclicals
| confims Co,
“or chloride vaclical -
| bolt Aoltition + lll HN
| silver nitrate solu |
| tion Cag Nos).
_ Ay.No,, Céiber_nityate)
Fest
witty tg fom
white | cI é& confined -
[
edt which is trtolu-
For _bromiole vadical
( fe teat
O.
excess of Cherie wattr |
+ 2-3 drops of CCl,
| hake wr0l) « a
—————————————
é ica) |
(Brown ing. test)
neil il
| A_brown ring ts_| ‘confirms_nitrate_
med atthe | |
(on (Nor)
radicals (
__Tetection of zero group x
cations)
icolGNi =e
1,5)
_ folt + NaOH, heat~| Pungent Amel
: aa
Indlicotes NH
No pungent ,mell| Ammonium on
of ammonia
Is cbsent -
Nessler’s reogent
test. g
[-the_Aold | Brown precipitate. |
_+ NaOH + Necsler’s
| Confirms NH, |
Cpt by ane aioe”
Heege nt”
pe
‘Teacher’ Signature
olvent: Date
Page No.
OBSER VATION
INE ERENCE
S_fonioinal Fron
+ dif: 4cl-
thi ifbte |g I |
radical ¢ pis
may b pp von
Group T basic
tate:
Np-wikitefccip=|
wodical absent
OS + diel +H,8
Bloc. preci pt
fa
raolicol _y'¢ pusert
No black ppt - Gpi_basic
lyadical Ls “s absent
|
O'S + NHy Cl solution Wh te oe latinous Gp (c
+ NH,0H dolution in pot | vadical present
exces _
No white gelatin lop 70 basic
us ppt: radical 1's absent -
0-8 + Ny Cl White ppt 4p basic
izle
lyadical zn2* ton
selection th @xctAs +H, S-
1 PYehe nt «
Fla Coloured.
Gp VY bese
ppt -
jae
gpdical_Mn on
Teachers Signature
is present - Mo precipitate:
6p TY bas
beet
|_| OS + WH,CL + NH,OH
jaical i
| Gp basic
In excess +
White _precipé tote
radical Bor* Sv°t
,
(0, Jaltation - fi
Ca? ton may be
present
Alo ppt
GeV bask
Yodlical (sa
VI ofcup basi
rodizal Ing?
Identification test
fox Ba2*t, Sr2*, Cgt
i Yellow pot Indlicotes —bariuer
+ dil: CH,cOOM + (on (Ba2*)
potas sium chromate | No yellow ppt Ba2t ts pbsent - |
" dolittion + m Sr2tor(gt
(ph
Achuition_of the poet [le ppt Indlic. Gt
dil: CH, CooL Ormoni oh:
tm seul phate
No_blAife ppt Sx2+ (s absent -
May be Ca?* ton!
+ NH:
um oxalate -
olution of -the walt | blhite ppt
OH Anno — |
Inolicades Ca 2*
(on
Teacher’ Signature | P:
—— afer tgp lt C02
Date
age No.
| 0S + add_Aaon |
idropuntae vohabl th ober
of NaH.
|__laddl pletyct_ solution | g
_and—Ahako- steoppears - luminivan CAP *
(on.
- 2,
Mp2
7 +t_NaOH solution Inolicodes 2n2+
clropusise and then | th excess of JaOH + | ton
tthe. hoe -
blhitepyat_aleoly, delicate Ma
turns bye andl fon
inoluble tha cxcera
of NaOH
. 7 - Jt oy aH
Confirmatory test—fo V_qpaup hosicxpdlicals Fig Se
Ant + 2 dlxops of
Appl green florte |
i
( Poms Ba2t
dilute -HC|_on a. (on -
wateh alate Apply
flome Vteat tdith Grimcon_red_fome | confirms $x? +
tthe belo of A aclan (on.
plotinuun Wire - Brick red floune confirms Co?*
cen”
Teacher's Signature Date
}
|
PageNo,______—_ |
LoS + WHyel solution | White pot Confirms Ing?
| NHyOH in_LYCERA (on_-
solution -
REAULT :
The given tole contains
ay Acicl radical =
by Fasic vaclical =
7 tormula of the Jolt =
|
|
‘Teacher's Signature Date
Expt.No. Page No.
(dela : : : _
EXPERIMENT — 4
AEMI _ Micko Quauitative Anayysis OF wok bane!
APLT— 4
_EXPERIMENT OBseRvATION | SweERENCe
}
|
Paeli |
17 Colour Lolouerle.ss
27 Stote cuystalline Aolich
3 tolubility Adluble_in_th©
Aci
radicals.
G li ical
Salt + dilute HCl __|Nlo_ brisk eftervas-| Ablence of 15%
E = :
lesa ,oclounlesa Gas vodical (o,2-
Gp Tacicd nadical-
Salt + cone-H,SOy A_colourrle s_pun=| May be presen
ich Qives ise. | GoiT actof
cw) e mt_uitth| vactical pyesent |
flats znodl_slipppea
tn MH y Ot emp.
te the maute. of
tut tabe-
E Teacher's Signature
EL | Confirnactory test for Chlewide ion_[t1-]
EXPERIMENT. OBSERVATION. JMEFRENCE
| AaNo, test
att Solution + dil-HNl White pet urluble ICI és canpieal.
—tAghlo, dolution-_lin_excuz of Neyo! __
| Adlurtion-
IDENTIFICATION O04 Basic RADICAL:
|
Guoup zero bosic
radical
ith ge dense ‘0 orecp ic
cahile felnaws cwcth, | eaiiral te
gloss “rod dipped |__ priser _
(A__cone- HCI
Aolviticn
——
dolieticn _(0-= salt tater.
a onfixmeition test
tL
+ waa): «
fo NH," xadicas 0 Group pnsic
Ne ssfer's pt oeclical-
0-6 + Nessler’ Avecblich brown weuit (on is
t+ Na Or (exces) ppt fornedd- pas
Teacher’ Signature Pate
oe . a)
RESUAT:
gee nenipenic—dalt candsins
|p Acidic tadical_: Chloride Fei] con.
|p Basie_rndtical—: Ammoniuen [t,t ] fon |
el The given inorganic tolt- js = Alec [Ammeniun —|
ChAlonde ]
Teacher's Signature Date__
Page No,
SEMI MICRO Quavitative ANALYSIS oe a
FNORGANIC SALT = 2
EXPERIMENT OBSERVATION | _INZERENCE—
Preléminas. test 7 —
17 _.Colowur Lolourle
1y_Atode (line.
4 Aolubilety Aoluble_tn water
Cl Send Pion ;
wacidic_radicals _|
Group L
Jatt + dil HCl No_brick efferves- | Absence oJ
cence of colourlex, | S¢ group ccidhe_|
scoot asi yodiicad-
Lytved- a
Group Th Gel (s_present-_
Aalt-+00hC-H,SOy éuclaition of hv olol— Mow be |
, d from tbn |
{ae omidle
[e2-]
Ag Alo, teat : “
0:6 + dif HNo, + AgAlo,| Pale yelloss feream Bromide ton
Alico. ppt which ts spar=| conf irmegl +
fi th
rhacnd fare | PETECTION OF Basic. RanicaL
[tion ond rif -
prs a
May be Af. |
fun wtth lass
¢ 4
a a
HCl_soluction-
__| Fok Ammonium
RADICAL +
0-6 fons A tL A ede + canfeenec-
| Aino fexces) pptis_formedt-
__| REsuLT
Acid
=~ Baomiole CBr-) ton
i
= jum (Nat) é
the ust thorganie Aolt ts NHyBr (Ammonium Bromiok | .
Teacher's Signature —____— SEL
Mic RO Quaterative—ANaLysic
OF INORGANIC.
AALT = 3.
EXPERIMENT. OBSERVATION _|_JNEERENCE
PRELIMINARY TEST.
7 Colour Lolourless frahite
y_Atate - cargetolline
DETECTION OF ACIDIC RADICAL i
G_. |
1, :
Jolt + id HCl No_brisk effexverc aE
lence of coluerlex, |vaclicol is
sodtowiloss_ gas Js_|_abent:
velueol
Gpoup TT:
ce HS Oy, No ¢, is Vee le >
absent -
| V voheol-
Jo the_above | ich_b No,
adel_copper ‘iethings es it_tuolverl group —T_acicl |
wand feat: yadical absent: |
Gyoup | .
O-§ + ol-HCl + Boch 1A cohite ppt is ob-| Group Ti ts_prese :
An luton ih |
toinedl | Son” i C ‘
insoluble ca_olfl HCL
feacher’s Signature Expt. No,
| DETECTION OF Basic _KaDICAL:
|__| ExPeRimEnT | o@seavaTioN | Jnv¥EREALCE
Group *e2 |
Jolt + dil-NeOH solection Nlo_puancyrct—trnell| Gp'0 basic —
wand boil - ing. ga ix_eualvedl- bradlical_tx absent!
Guoup_T
68+ dil-HCL solution
No. Chaanctet tic T orp nsic—
ppt- Yodlic I
Gx0up-T
oct oli HCL + HS Gea
No _cheancteristic
basic
ppt
badfend is absent -
jiahéte gelatinows | T_ Gace zt
ti
CONFIRMATION “TEST.
foR Til GROUP BAS
IC RADICAL *
0.
de.-
lu
in excess of soclivu
| Alumincom cs |
pete ppt dolla —t_Aluon
bhi Me pad CED ion:
l Aolition
on
| white gelatinous pat
nee
ailing
Teacher's Signature ‘Teacher’ Signature Date
7 : : a
Se —Jvonsanic
|__l77_ state. Amorphous =
| 3 cl
DETECTION OF AcIDIC RADICAL ~
T_GRouP
2 a
AALT ~ bh
| —
|
__| _ExpeRimenT OBSERVATION _| “INFERENCE
| Preliminary “test: |
7 Colour White a |
7 |
j
uv
mE
\
a
| & Brick effervescence ——
CHeot gf necessary) lof Lolourkss 14p ee al
codlewalesa gl turn is puttse
| org Lire _sbater.
|| inf milky ts
|| chtainedl
—l | J 1
| = = _
| Salt + H,0 and foil | Line wafer doe |carborate_is 7 |
: t tos ik —lecnfinmedt [roe]
post of tits .anothey
fect tube certoining, |
| inne _w2aten: a |
Teache Expt. No.
| DETECTION _O# Basic _ RADICAL:
EXPERIMENT. Osservation | INFERENCE
Group 0
__lialt + dif NaOH salu t= No_pungpat— vell-| Oo! in
__|tion and Seif - tra, God is sftp
evolved -
Gp 1
OS+ oil Hel uolution- | No characteristic Tp pai —
pee
Group Th
pe:
Gaaup I
Os + solid NHyCl_+ No characteristic (TIL gros basic_|
NbOH AOC ct: ppt: yadical absent |
Gpoup_D
‘$+ Aolil NHycl + white ppt ds Ww grec basic_|
Ni,oH solution + Obtained _raglic ol pruse nit |
He Gat 2
Teacher’ Signature T__ for Zine [ze2T)
white pot seli=| Zine. U2 confesmed
| 2.
lble in oyrey of |7n
I Np OH
|
i
hen iroraoric Lob contain
Vndicns . carbonate (02D
rodica§ | — Fine (in2*)
|
The criven presario alk is ZnO, |
! g [zine corbOnote] |
| . Expt No ee Bogs Noe |
| Experimenta gd
| Sem MeRo Sualitative—farysis oz |
2 INORGANIC AALT = 5
|__| #XPERIMENT _|_ OBSERVATION. TN EER ENCE
|__| f test: t
Colpuk Light pink. Meng be Mn
|_p tote Cay c
DETECTION OF AC(DIC__ RADICAL:
T_Group- :
Teacher's Signature Date
Expt. No. —_____ Page No.
Q
LTi_Gaoue r
oS + oliHcl soliti-|A nahite pet cx | Ti Ganup
on+ Palle Aotution - | ‘aod —toki | ew
is insoluble i __| parsed *
Lencess of diel | Sop id confinerth
DETECTION OF Basic RADICAL:
| |
+ |
: |
Salt + ol Anbu ancl _|
Aoot
T GCP
ose "dit Hel aolition | No px is | Gp bowl
obtained! - lyodical obtent
Tl_gyoup | |
oS+ Miler +H. No ppt f ined. G i
gos: nrodical absent”
It ortup | |
los + LAodiel Nliycl ___ No hovoclerishe Ir hp baaic
+ ‘ | . |
(exes) |
|
Ww Grotap- |
0-6 + Adkicl NH, CI + teh coloured. we 0b basi
NityOH Lexcess) anol __4 d ined yori Ht
poss HS 9nd - ira Be (prt
0 ‘Teacher's Signature d nn ——— >
| Expt.No. Page No.
—— — = == =~ a
m f 2¢
O-S = Naot alton |A ik tt at A
tn 2xcesd foroed cJhich
turns
brown on nh
a,
tr_.aln:
4y0up TI bosic
OS + Sead dioxicle
Pir
Lp bow Aoluction +:
Ont te confirmely-
OnC:HNOs andl earl -
nk coloused
ppt ix_obstainee/:
REAULT:
Tho wi i
az _Adidie i
bZ Bost
= S027
vaclicol = Mn?* Corgantss) ton.
2. ho suc taowpanic Ante js MrSd {Biewgene
Laatypock |
Teacher's Signature bap No.
wemt—MLCkO_ QUALITATIVE _ ANALYSIS “Oz _JNCRBANIC.
a
expacech
i the _meuth_of
tut tube»
So Tppel Vy th
MALT -6 =
}
—|_éxperiment | OBSERVATION. INFERENCE
[ cela 4 tet a |
| Eine | White. =
|__| ay Alate ; |
hh ity —— dit in sike_|
| DETECTION OF AcIDic RADICAL:
|_Group 1 |
bolt + oR HCL Alo_bvisk offa.yis-| Groups T___
= ence. uv Leidl’ vodicod |
= abserd -
_ Group D
ath +t con H, S04,
CONFIRMATION TEST _]
FOR CHLORIDE TONE FCI“) -
—|doutt uoliion + alt
Ll. hite_ppt_s__|
ae
= Han, Ag No, solu=| formed _cyhich_t
tion -
‘Teacher's Signature
(nsoluuble_th_Aifyot. [= ae
(| DETECTION OY
‘O Group
dat + olif NaOH
ahd bel - |
ale Group
c (Hcl
lah
Tr Gai
OiGr di dicleE S
No choyacteris- OU ic
tic ppl”
GOA
Tr Govup
oct soliol N No_chayocteristicl Ti) qe up_bosic
tN M4OH Cexctss | ppt: vacktol absent
wiv Group:
oct voli je characte tic TN Gubus_hasic_|
ENMty OH (exc) ppt rodidol “absent °
and _—poss_H,< gs: [
a Gnas z
oc + £olicl WHycl + | White P. Wa grdups basi
NHyou (excess + in_hi i .
\—lvits),Co2, idoluition Mou be Ba?*, ox*¥
Teacher's Signature
colt & pruet : Page No.
| CONFIRMATION TEST FoR groups Baste. wroclicas |
| éxpékiment. Opseevation | LNEEREACE
10'S + potasdivm chil A yellow ppt | Ba2* ¢
mode _.dolirtion ts" cbtoinid - | present’
(e,cra ft oe:
CH2COOH
tlome tut:
j 2, ral
ee gal cape of | is ipa tr | med.
eae the flame.
th cate
ResuLT :
y Acidic___tradical -! Ci- CChloviok] fon -
> Posie vodicol - Pa*t [Baxium'] ‘on
T
hw. given “enagnnsc Jolt is Encl, [Barium chlovict') -
‘Teacher’ Signature EXPERIMENT - 7
| emt Micro Quaritative ANALYSIS.
pj ka
|_| €XPERIMENT __|_OBAeRVATION _| INFERENCE —
| Preliminary test: a ee
P_Colour White jf i
57 _Atote Amorphous ie —
#7_Aolubi lity doleeble in_dil:HCL_| —
DETECTION OF ACIDIC RADICAL: —__ -
T Group
Jolt “+ dif Hcl Brick oflervescence| Moy 6 coj
Aoliition in, acdeual Goel pce |
us teening. present
Line “tact:
aniltey
CONFIRMATION TEST, FOR _.CARBOIVATE."_,
Jolt + woter vancl Line contr clees | T_qroup acioltd
, ber | net Luu mtlfig- radical presen
oiled ja _jpassocl COs" fs _confir—|
Jt anerthos__teat med -
tube containing
dime —_tocte - ¢ 4
Teacher's Signature DETECTION Ox Basic RADICAL -
| ; & qeoup —
ice ae Ll a la aba
| (_ovolbe cl
Pineal aoe pe
i ppe od nt:
wan Soup
{ 1 "i . .
| OSE dif- 4¢ solution No characteristic basic
vail Laent
ill Oyo
O-St ‘Neycl +NHy0H [No choancteristicl Th group—_hosic |
lexus) sdluttion ppt ~ hodlical absent
ees dt opmup = _
|| g | blo schoaacteristig TZ_proup basic._|
| nh OH (2LCUA) pass “ppt radical abseat
liars god inte Aoluttion
a LO
Meme
“Teacher's Signature
| + NHyoH + CNH, Co, qodicafl aoy.__|
| stag [be pies
_| ay be (7 *
| = Date
__ ero —_— No.
— cone. Gaind Ike dar a7 pmb pase amucal |
“S} potaw’ um chrom No_chavacter'stic
“Tate chstios pt Borium (Bae?
ah vadicol
[oss afhity, Soy Heat | wackristic [9x4 1
— | deratch_the Re pp: absent:
| [ A\_the fest tebe - ;
|
L 10S + NH. Whit Calcium ts
| oxnledes: is_Obtod neal _- confirmed!
Home_teat
L 1A mall amewt of | Brick rd colour | Calctcim (tot)
Alt is made into
L
imeoxted t is confirmed -
a paste oth scone:
the" flame -
Hels fa_a_watch loss
nd dsthoduced ~ trite
the on-Lunin. ous
past of the larne -
RESULT
yy Basle _vadicol =
Tho _gaken inorganic alt contains
y Acidic! radical! farbonode_(c02-) ton
calcium (00?*2/on
4 carbone) —
‘Teacher’ Signature Aemt_Micro — Guanitatnve ANALYSIS Ot InorsAalt
| AALT= 8
|_| Expegimeny OBSERVATION TNEERENCE
Prelimincere teat:
I2_Colocer' Waite
a7 Ato Lrystobling
y Adlbility Adluble. in_tooder
paseo OF AciDic. RADICAL |
J
| |
L up |
aa ib cl anda Alo_brisk efferves T gro. cidic_|
| tion conte is obtai=| Aathical absent
beck -
A group— = -
Humes_042 abéent™
elves -
To the _.obeve. golut—| Reddish brown. NO, pusent |
( i 1G ic
CONEIRMATION Test | FOR Nox CNifrate) ton:
__|Brown ring tet:
iat Jolution + pre=| A been Cae é_| Ger present - |
, No, hj y | expt. No
Date _
Page No.
| | EXPERIMENT OBSERVATION | INFERENCE
0-S + dit Hel solution | Ne_chameterichia T group paste
ppt raclicol ~béert:
OStdibHel + HS gos | Ne ehorracterict | “
ppt
14
OSt NHC (solio)-+ niyolt No-charmetenistic) TH. ganup——_
olution (exces) ppt baste _raclicol
absent:
Ost id) + No characlevistic |TV _gaoup __|
NbyOH solution (exces) | ppt basic yaolicop_|
tls 90s- absent’
0-8 + NHy Cl Ceolicl) + White ppt "Y_gatup
__| WHyOH Cees) +(MHpL0,| C8 Obtrinedt bodice vYaclicol
| solution: present Moxy
"be ca2* Bat
(Giese :
| Coneikmation test |For VGrouP |Basic RapicaL
| 08 +olif H+ __| No_yellovo Bart ts
Kr Oy. Aaluition | Ppi | absent:
| t
‘Teacher's Signature apt. No. Pope Noes
=
ost dil-CH,Coot | White ppt _cs | S¢**_ may
—| olin + Gut S0y | obtaineal-_|_be_pwtsent-
Ad:
| | Hame_teat.
A_poste of the
- a awl Cai | ort cc confir=
| coteuabes Haas
Hhncugh—platiuen
Lane:
REAULT
The _oéven_(norgani u
LZ Aciolic ! voclicol = Nos (nitrate]ion
LD Potic yodical - S?* [abontium lion
Sx (NOs)
Teacher's Signature | AEm! MicRo QwaALiTATIVE ANALYSIS OF
INORGANIC _AALT=9
EXPERIMEN
PRELIMINARY TEST
(rT | OpservaTION | TNFERENCE |
7_Colour White
2 Atote c :
D folubi let aa
woter
DETECTION OF AciDIC RADICAL
G rou T |
Salt + oli Hct | No bri | Gpr acid
Aolrition Mente head
fibsent
Group TL
Jolt + cone: H,£0, | No cheaacteristicl 7, Br- axe _|
Tot obove___|_No_vedldish a is
Acluction copper 5 Labsent
funnings Gano head: 2v0lvecl- Nox ts wbsent |
na
OS + Batl +ait- | White ppt. CA Gadup Tir saci
Hel soliton - obtain shich trodlical_pacsent |
$0,
‘eke eb aT Aer Conlimmecl = ——— _
__| DETECTION _OF _ Basic
RADICAL:
oO ;
Jolt "+ cif: tadt Ab _purgest erelig {0 p___|
z yabsect*
Los Oe 'cil-HCl sctuti-| No charactorist’e. L_goup
: : iad | baal tical
| absent”
Th epoup.
Te, :
lion +H, gan Ppt iC aac
btext
Tl_gyu
: + Ay citsaliq> No_choaacterist'c_| Ti
“Taek De wabbent *
ppp
65+ NHytl (Aol) Mio_chooclen's / Te grtup
| + Hy gas 7 ahsent.
Teacher's Signature up
| |0:S -F NHy cl (solid)! No characteristic_| Sf
[p+ ior sale i ad bac
cbtoinedl
VI Gwup -
O-S+NHOH + sodium
hyclnagen phosphate White pbb is | Mg*t may be
| | "¢nefnpo,) heat__| obtainect - piucot”
ahd scratch the
bide of the teat VE gatiye—batic
tube —‘watth_glass radical preacat |
rod:
CONELRMATJON OF mg? ton test:
O'S +Naor White ppt vw G70 tuf>
Aolutien 10c5_of Naot, | bout vaclicos
(Eb dvoluble * Mg >t
L conf:
T
RESULT: :
given inorganic. Jat contoins: ~
i me Aulphote (cop) (on.
27 Bowe Yvadicof = mogats ies £ag®9 COA.
| the a uch nara sake, i Migs, Citeag rvesiter|
ee
Teacher’ Signature
pr Expo.
|_Jemt Mieke Guacerarive —Anarysis 0% |
LJ Inorganic Aart = 10
EXPERI MENT OBSERVATION. INFERENCE |
Prtiminary tect:
7 Colour Colorless ushite
7 Atoite. Crystolfine
y Aolubility Lokble_in
water
DETECTION OF AiDic__RADICAL:
T_Gaoup
ee Set : LG 7
feaucsctnce | _yaciol_ rackicat|
joa it-ohtaind aber |
ai Gorey -
|| katt + come: p,SOy A colourless T Gp
l Almira, 4. acicl. cp
pakich 4 AULA
alunse Sexkite hoy be
fees ethen CL
lle ip Bet —
re ers aa bna
mL Ayn, test___|
0S +clil- HNO, t 1A a rae white | CI is confisenedf
silver _wirede |
| soliton te tn de pacer
ja | Nitty OF - |
| |
tic_ppt_&
L obtditecd:
|
IL_G20up
oe 4 coguel + [No Facies Patic
Hos i+ ppt is sti lal ad
Til Group
Oct NHty Cl CAolid) No chonocierics T 2p btusic |
| NtyOet (excess tic ppt. a wrod absent:
obtained -
Teacher's signatre Date
Expt. No. Page No,
iva Group -
O-S+ NHyCl(solid) | No haractérict TV_gitup baste —
+ Niu OF (etc) ppt Ls obtained radical absent -
and _yadd — H,¢
OA *
0
Gro
0: Salida No tevictid VW
ch:
WL :
OS + Niko 2
pho. habe 7 tend obtained - vodicol absent _|
"hood, sCYatch the
Aides the
Moy be fg?t «
g d
tet tube uith |
gts ‘yoo -
CONELRINATION.
TEST Fok. Mg? t
ton »
0-S¢ NaOH solection -
tohite te ppt ado at
ZMeA -
feud of NQOH -
‘Teacher's Signat
Fe Date
— _ ———
} Expt. No. 1
|B J
Page No. ______—
RESUAT °
The yen _inoreanic salt containd
£
27 Dodsic. radical = Magauiti [mg?*] ion
The_.gien —inssopns t fe
Chloride] -
Teacher's Signature “Test __For_funcrtaver ame I |
ORG Anite _ComPounpg.—_____|
NE ene’
To identi jy the und tonal —gsieuyp —pussendd |
—tn—_ongdric_tamypound.._"
As
i Ee ett anne
| Bayost's test:
od -Osganic_tompand di Pink toleun_of | Thdicates tho
n_ctcetomes se daiops the _kMmq, 18 prusente Of
__lalkaltme Mina, i L__L alcoholic gevecsp |
H | Test__jo _clcehelfe geuoup ¢
| Comte ammonium mitswate best :
ee | 0 aleehatic |
miu _onitarocke.
Lucas test:
ic_Com potind-+—|_LngpausA4jnaale — 2 al-cohol__|
ai ont[ent tentnadlately : 2
oy atl ae thin _[-fmtn |_| oe
Teachor’s Signature ee Page No. _______ |
tH phenslic geioup (ag -oH
gj] aldol _jenaiic chlosicle teak
| = pound} A bluse geen, | tndtcotos toe |
— }—Vi5. 9,0 LO
ij|_phtha Len die desk
—Dagonic d+| A pink ble Gt) | ndicotes tre _|
a_pionth of _pithalie po
| ide + Come tatned . The. pheni
Tie deated the_| coleus disaipesss| * CroHt) gpueup.|
—mirtieio canted § | em odaleten of. U
—{pauaed into dle exces, ef hla
Naot sebiien %
L2,4- DuiP test *
|—~Pe
Teacher's Signature aes Teacher's Signature A test.
°
Teacher's Signature RApect ef Uemearnsostion a) HL em the crake of -weaction
between Nags, & HO .
Amour 9} NasS.0.. ascot each time = S0rL
Corcantsoction eb NayS90, soluction =OIN.
Room jempurctue C concentration of the Hd Saluition
used ma the stoactien omixtuse = 10M. |
SL. no Volume 4 Hdl odded Tema t wseends ||
im mL a tho_masxk'x’ ||
( i “to become (ravisible
Q Qo
3. Leo |
77 8-0
S 16-0 | exptNo dO, a
[eo ,
— eee ee
|—Eecect Oe (oncenrearton De Rare OE
| Reaction Perwcen Sertom Tutogn.ouare |
Anim _Hvoeocurorte Acto
Teacher's Signature Y time 1 BEC mas Teacher's Signature | eghect of tempeniatuswa On sode ef, Steaction betoen
NlayS0, & Heb.
volume of Naygp, used each time = 50m
ile by Ae a
Tempestahoe of Ha action | Teme ‘t’ tn
mixtuw/"C
al. slo
Ho movouk. ‘x’
becemeT
envistole . | Expt.No df = ' Page =
Erect _ Of “Temperature On Rare _Oe React
_|——BeTWeEEN__Sontom TarosoLPuinte (nD
: ———Hprocunere Act) == ee eee
sat: “yuck of dempealios vos
| =ion_on stanchion _befuoeasr
aa] [etna Tai hydewochlaste aad.
[A ae ee eee ee
odu olution 9
make the elution -ranabucent .
I cuss
QoS De ie + Qnacl + Hoo +50, +5
ae tne above auathien ts Sy ___|
|_| [soa O ante igo tS OTS
EC) —_intatonsing — Hae tempenabuse the
Peinalic orange “Spt taacng Apecies tmncovrag.nes
ia tm apt —calliatens Hot” susult inthe Jermatic)
gj ading— a joer dag
|e pjeck of, Lempenaduiste 2
_[ Mabesrale wed! —Busuette, pipette, herman make
ak Ragu & stop CK» O-LMNOS 90. 6 4m Hol.
Toacher’s Signature
ee |
A gaaph eb countuste in °C Ye time token is
graph sf tenp % ae
temperate in °C
*, y x
Time im sec
temperate tn °C
x tmein 40 Fo goa 6.0, _soluchion ina [oom beol
SSA Ee lan» bottom of,
ushith a_mask ‘x’ hax bet made, keep the beaker
iO _theoimestat meinttaimed at 30°C. dd Souk
rLM He) seliction noth Austoinagliy Stasut tho
|__| aug Bement
2:5 mb) 5 _Hd "has beon tranjestetod .
Fees ihe tas beanie
3 {MVizthlo . -
Repent i Spent ok dermpenesit_ S
(Tliserqeensiont ofthe maak
Conclusten + Rate ef, ston ction tnicsLenaen Us tncxees
em corttyatem at _a10a chant.
(er
Teacher's Signature Lins 19 200 %
5 oe
time ™m sec DETERMINATION. Oe. Entkarey OF GoLUTION
OE kar (ps) igo
Arm: To_oleteurime tho heat op sotuchion of
potassium _nitsote. (e)__coppesr_nsplaa te
| Seeenironls the amount 9 nastgay _Jibestaded
__|____54_abseated shunt solute 2
k Auch. pe paths olulisk tn doenst
olteuw) the Chana, 4“ colLodl ot,
| bolucion .
PROLERS 2 KnlO, G2) + aq. Knlo, Cag,)
Perovenuee : Abawt flay fpowoboted [dnlo, (ougetrals axel
[| A in 64 the ‘mass o) th 1
| noted 00m! of ols o toatoot {x taken tno
|_.s50xn!__palythono battle 44
Teacher's Signature a — — |
Colurtation: ; | |
Heat abseubed = [mos Of sgeluction 3 (aeseysreth
[erat]
v=3 ||
Heat absorbed by tol tg of kNo(tmele) = |
(or) ~
(ayes Sa, Sips) Imola
if F rxpt. No.
[oases
Sena
ciemitle eyasea ay wi [api og
US__moss weg a vote “a -
| -Mas8 — 6, _Weighicng => M yd]
[-8),-Mas& 8}, _ empty Beighing bottle —? M3280
Mase eb kalo, toustals token-=> t= (m=Mp]=20|
La). i > Tks
Conveour tomp attained by the solution Tk =993!
)| 3foll fa tempesakue: —? Te (T.=T)e ok
Mass solution —> m= (w, +) ipl aaee
| Spedhic heat of tober —? 5 = 4900 Ty
Regupt:
the toluchiem of _KNG—= AH =Qox b&pnxd
Heat Sf, t a =
04X10
+
Teachor’s Signature f
Expl
\
(“T pereorrmarina Of male “Oe
|—___nleuten
a
———————__ J
ISaTioN OF Hol Ano Noon
Atm _To__dletootmizns thy enthalpy of rata sal
)_psfth “a 4, bo.ae.
a ae
THEDRY : digg Prop e_pai yn
toms 1]
= oi te ec
i hie ,thasiefas»
this _otoactiom is _olunoys, e soup Enable
4 Ht fers dscns
=h by
eet
= Leng |
tn
Hata pai
ttt cag,) + oH (oq) —
Ome ete [nad Vlaaa
pohoou. ml enous ebay of munca
ae an a baat eah y Man}
Has_foeumocti enn of _L nel _/ He) CL). alco aw feted
Lameunt of hoa vx, 51 iG-motbs_Libedated Th aun
| one _¢ of teeactd_o%t_the_baat13_toeak 671_t¢ bath aate|
Libooated %4 u ae
| tho fominot’ ion _of tre acid ort hose _0% _ bot 1 rae
the amend of a Lbosated fs lox than
& 1
54 kT nel
Teacher's Signature | | (“Tatsaials Qypimd olen (ain Gunml) |
—_theimometen . Sheoor 1M Hel 9100 mb ___|
Lt LM Naot > 100 mL Mary Tne, CHLogneorm Anin Ace Toe - __—
Arm: To cletecumine the enthalpy change peor, Are
homal foumation) ae |
CH. ral
“0 + H-Chd > >
He a ee Na
| | * = bendliang_bettrean_|
ttt ppv actors,
9a nig pros enthalpy change co duco.to
bypluogtn find yptnattan Thi italy change 14
LT gaa haat pated pate Aysctem—dapenols chen
|| amount 4 _Le P ixecl. Th 28 por hid
Teachor's Signature [
Caleta the, ertholpy -ii“dte
| yeburee of one mob of Ht, = “Dansiy of CHC
velume .
| Nelume Ol melo = Lh, of the ait
lo
| Density of Gusto yer tengo
Malan moss of ouasspen > | 9:
tlptg = ImLvelume
Ud-5q = mb
tmole = 8h-4mb
ol mele = 8 lem
Density of atone = 0-344 g/ml
Melos mass of acetone = 58-0
o#qgs dmb
Beg = ag ml
jmetes 43-4 mL
O+ [| mele te3h mb.
Fetal volurae of atone & Chlerrofeun
| = B44 +84 = 15-48mL
sakeotockion 03 follsuws
ot mele
| (seitoody your tan Calaslad ta volun ee
=
| | Sto
4 Teacher's Signature i) Alot the v fe
ditenatusle . bof ie E g hon tea
thisnperun = m,Xq, x (+—t,)
dg
iti) plot Hao volo Sf pectic “heat fertacetene Jom |
—
awbono = m9Xq9X(t, -ty)
| ee mana a =
Teacher's Signature E LECTROCHEMISTRY
Am: To ftudy the yesutation im_celt_pstentiat ef
a ; ;
| on tontaatien of dlachael plot 8
Mns_ eunst _equati kak
gd
Punt®
| : trate, lig beak pois Tac Jute cater
| |_| 4 distal Wak , a veltmoten |
| .
wit iL Labie
Teacher's Signature Date
: 7 =a — }
Expt.No.
[Ban EDURE +
peatieciete!
Oo ee
i tone, © xnSa,_eelution_e| tM_,but “changing |
—_—_———_—_
Teacher's Signature Dete
= =)
Page No, __—
Procedure S—
Prrpentin of green pigrsnt farce leaues_eonl |
_ Colour pi cham -tlowstns.
f
bend the —~Flowses and Leagues Separa Haley ona rnoctor
and ranshey— kosoy + Aly Cay) ane]
Ky Coy), Hoo
MATepiALs REQUIRED —
Peson 2 (-F9mt of Glia), £04 .
2c ml of Al. Hy Soy+
Peparatin of Fevitus errmrportiarn _S1| phate Proc tluece S—
It. 2
7 we 3.
lof yaber
tat odd _abtul sml_of ctl. Hysay ty Ho Plask
c : is
Land tne: Siluliin by Mating Hilt tHe crptha bia lin pint ts |
| searched «
TTL T
Teacher's Signature Dote —_______—
= 7 ]
Expt. No. Page No. J
ps Alba teaches ate _dnpt dy
7 —
eI Ta oayts oy Shaking sft veng Small ounnount of
|_—_|— 10:1. yafion “coe wales’ and —alvobol —reisrlure_tn_xeenove |
o ShCkgnp. patatare__Liqyuscn’
oy Sepea c tl fl
_|—doy and yield ts ola» |
a eof RESULT E
__| rede fe
Reparation £ tybath him lt oy Hy 0.
\ | Teacher's Signature a
expt. No. 4
————
Page No. |
ie
L4
Materials Deg uSreds-
\ LA.2 guns of (Absa),
PROCE DURE S—
ma:
of» The. Cory thals one. finally
tied befween “Alds of filler poper.
RESULT Z—
of
Teacher's Signature —_—
- ¢ te ON by rested a
)
iS_acidtc_@n pobne . uherehine » 4a the ateenco of cftlute
G10 st cuseacel, + oHc—//_\\_Nadu, 7 \\_c v4 = ct coc acl 7 XY
Cenzaleehyde Acetone = Dibenralocetore
Mblerial Reayvized =
% Conical flask kom! =1
A Pegler Sd ml zl
% Ethanol 22s ml
Procedure t=
Ls Bropost__a._Slutton of 3.1 g-Sodtuontyptonie foo entatture_|
pt _a¢ml ethanol ard 3oml _icglled water taken tn a agoml_|
|__| temperate of about c6o-2e%e.
| beclery » Coal the bealerx tn an {02 hath masataind af a |
2. Prop o_nfichnt of 3.) ool of Peoaalcehyple and 9-2 ml of
Adolf of this rcirtare Slaaly @r tee Coalecd
Fe sn iG gate
fy St
gently for about fftcon _minu li «
Teacher's Signature [Expt No.
6 Re —stht_ffeld| and tho _rnelting pick of “the campo
3. After__is “Mivlit —addl_wernas.ntog arth f bennotdehy fe
and _acetore and fir fn 0 pefidulél ports ___|
4pPiller te pale ye msgid so phinined and sash ust —
Cold wor» Day. 3k and reerystall: eh 3 ot
Fone ethan
: RESULT J—
lo Yield of dibeoralacetare 1s -
(b) bh —*.
Teacher's Signature _—_—_—__—— Date
- — —— -
| Expt.No. Ql Page No.
a —— ==
|__| PREPARATION Fp witpy AceTANWLIDE _ERoM 1
|__| ACE TaNipe 1
[| aM
ua
1 To_prcfete__ facto ptetngttce |
|
THEORY ¢-
Pono= nto acetanilide prepared _by the citalisy——
|_of _otedantiedo. by using the ecfixctue __pf__tone: HA/Os, are.
Conds H)Soy a4_ot-hrating mfitture 1 The rchthoe of boo |
|_| fi g #2) 0)
electphile _¢n_ the genctfon «
HINO) + tpSay =r Not + Hat -- 91so,7
Aitboot: iehng _orkle
ee ut_9-of si
Ae major Product . Thr. is an ¢Zorople of onoratic
RENNES cre ene eee \\-mHcocu
= Con «Hy Sy ea
Hide Portteacckorttticbe:
ae Cnojox prac) |
MATERIA REQUIRED ?-
Cont. Hy Soy, Commi), Beaker, hance! geal ice_bath
Teacher's Signature Expt. No. 2 Page No.
= ——. _ : _ nt
PROCEDURE
dh 203 of " atetorttde te Ai ssolved $n) racial _cicofte __|
acid
taken tn
cx_bealcer—dumb_of tort» Hy Say.
£5 actcled
Slowly roth constant Sh
|_{5_ obtosind . The._orfiactune
is
unl a lear salu Sioa ——|
Coated
fo tee cold pwoakex —_|
bath __-tex__sonae_ttme..
|19. aml of Cont. HM03 and 1.ml_of Cone. bf,69, 15 ceathally
| added nly the abe. Sifian with tonctant Shaking |
and —allowtd_—-foy__80_ooins__bo__connp let. the tac oan ____|
|__| acekantlide react with ntration —mtxture foaming. P- often ____|
acerantltde .
‘ c
akan A_yellouo saltd of Parthn _atetarfilide _is_obstosnel|
by. Aira tton ond_perifted! bay, ec ska Satie
$n
ob
Th 18
eth | aloha! -
Result s—
Yield of P-nttrn ate
