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Bitumen

The document outlines the specifications and testing methods for various grades of paving bitumen as per IS 73:2013. It details the characteristics, testing requirements, and conformity criteria for different viscosity grades (VG-10, VG-20, VG-30, VG-40) of bitumen. Additionally, it includes guidelines for packing, marking, and the use of the Bureau of Indian Standards certification mark.
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0% found this document useful (0 votes)
9 views

Bitumen

The document outlines the specifications and testing methods for various grades of paving bitumen as per IS 73:2013. It details the characteristics, testing requirements, and conformity criteria for different viscosity grades (VG-10, VG-20, VG-30, VG-40) of bitumen. Additionally, it includes guidelines for packing, marking, and the use of the Bureau of Indian Standards certification mark.
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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Thethe 73 wereIS-73-1992 specific

IS: or
specifications, to been are summer The andmanufacture that stiffer
booths associated
and
temperature. (1S: fromquality conforming Tests
specifications have respectively. surface-dressing pavements viscosity, 320040022099.040-60
VG-30
VG-40
VG-20 50 4.025
oil specifications likeremoved during grade.
toll
crude revised the grades
Bitumen.
tests retained. to near problems 73:2006
these with specifications surface used 240035022099.050-7047 4.0 40
of regions Penetration
Bitumen intersections,
higher
were Penetration
on source TheBIS qualification
either the teinperature
dependentbitumen per
stiffer
also as also other IS
Bitumen, point
penetration.
As road
is such altitudeduty its PER 160030022099.060-80 45 4.0 50
relationship is
the 2006. breaking Grade of temperature, It 60/70 to and
the grade, grade.
applications heavy as Due AS
on grade few temperature
mixing high shoving VG-10
of suchgrade. 80025022099.080-100
SPECIFICATION 40 4.0 75
is dependent on quality JulyA Therefore,
Viscosity the of
stiffness paving Penetration& extra lieu
Farass
in VG-40. any climate areas
it
classified higher andpavementOil: in to
Bitumen the60°C) construct
used
Penetration
resistance RTFOT: test
have the spraying
introduced per 2009. stressed
is
its bitumen improve &&
heating grading,India) Indian
represent
cold
products. over
at VG-30 not as 80/100 be
loads.BITUMEN
and and (Viscosity average in can / film
do
Bitumen
Aug of by in pavingtoused 30/40
highly improve test
1950
(BIS) To on fluidity)
parts used
marketed Bitumen It traffic minmin min thin
material
of VG-20, tests from old loads. over
relationship 1992. loss Bitumen. which annual Characteristics
CST, %,
poises, after
year Viscosity of of
widely for primarily in old (VG) film
Standards refineriesof
these marketing
C,
northern lieu used trafficused to heavy
of produced 135°C,
trichloroethylene,
max
thermoplastic the and VG-10, ductility, (degree Modified min,
135° is Bitumen in lieu GRADE 60°C, thin
60°C,
is
in 1962 as product. grade which climate is is
VG-10 is
substantial and min from cm,
temperature-vs-stiffness VG-20 VG-30 VG-40
in
time on gradesspecifications
Indian content, its
commenced andto
viscosity and lots temperature Viscosity,at25°C
min
Viscosity, Penetration 25°C,
C, at
based all Viscosity 60C similar of be VISCOSITY
refining. firstyears
method
of the C,
coldEmulsion
BITUMEN: BITUMEN: BITUMEN:can C, residue
point, ratio
from 25° Grades BITUMEN: parking point, at
a
Bureau fourwater of
of thethespecifications very endure mixes in
Kinematic SofteningViscosity
Ductility
is performance by
73-1992 to at at
climate, Absolute Solubility on
According penetration
conducted Flash
Bitumen for in are 73-1992 IndianOil replaced Different in Bitumen truck higher Tests
revised gravity, VG-10
paving VG-20 to
VG-30 VG-40 Bitumen TABLE:
1950) there ii.
The (hot need and with
IS:
TERMINOLOGY
3.1 inFor 3 1216:
1978 1208:
1978 1206 1205:
1978 1978
1203 : 334: indicated revision,
below:standard through
ofindicatedREFERENCESthis The Viscosity the This
1969 1448|69]P: (Part (Part 1201
1978 : 2002 60°C.
2 atgrades
Viscosity ISthe IS
No.applying SCOPE I
334 3) 2)
standard.following constructionstandard
purpose of
and : : are and reference paving
1978 1978
the
were
Ratio the encouraged
of parties At prescribes
by Determination bituminous
materials:
Determination
of bituminous
materials: Determination
bituminous
materials: materials:
most valid. standards of
Methods
products:
following this trichloroethylene (first Methods Methods
of viscosity
Absolute
Kincmatic viscosity of bituminous
Methods of bituminous
materials:
Methods Methodsbituminous
materials:
of revision) MethodsGlossary(hirdandtar the in grade
SPECIFICATION PAVING
cleaveland solubility ductility softening point
(frstpenetration
revision)(first the pavements. BITUMEN-
standard, recent to
time
I text, bitumen
is of of agreements to All contain
of the
the shall [P viscosity investigate
editions standards
:69| test in fo r (first for f or f or of for terms publication
constitute equirements
(open) revision)
Title
ratio apply. the for carbon Bitumen for
Flash testing
revision) testing testing testing testing testing relating provisions,
delinilions petroleum of use
of Determination Determination Sampling (first thbased
e are
viscosity and disulphide
cup revision)
revision) th e provisions (Fourth
Revision ) is as
ta r tar ta r tar possibility subject the
to standards graded
binders of Standard
Indian
ta r tar bitumen
fire and oneditions which, various
given
point and and and and and and this
of its or to of by in

methods average
container in
2. constitute
7.3 Table from 7.2 bitumenCONFORMITY
same InSAMPLING 7REQUIREMENTS
the 6.2 and 6.1 6 maximum Bitumen
viscosity, petroleum
suitableby bitumen,
5Bitumen 4 residue
Lot7.1 tandhe GRADESDESCRIPTION
From The any requirements The r
period. foNOTE
the The shall VG40VG30VG20 VG10 Grade
batch a (1)
sample number consignment, peribd
lot lot.binders
a various paving
not shall shall both from
prescribed shall cach This air
shall of foam not temperature be rolling
representative of
be of dependmanufacture of less the is be measured
the containers
prescribedgrades bitumen classified
drawn same AND when than 7 prepared
all day suitability methods. thin
incontainers the of 5 at
upon category binder
heated average
years Temperature
MaximumAir as
IS in containers bitumen Suitable into 60°C. film
to in given by
I201,
accordance of the be shall CRITERIA Table from
homogenous shall
to be maximum four the oven
selected
the size
selected and the recommended
for below: for
shall 175°C. >4538-4530-38 <30 refining
taking material of be of
grade 1. start (2) °C grades
paving 7 test
the grouped conform to of air
day
with in at tenperature to 201373:IS
lot
random from the Average based of
all in7.2 FOR unaged
given grade design crude
the the the an tothe on
IS 73: 2013

Table 1Requirements for Paving Bitumen


(Clause 6.2)
SI Characteristics Paving Grades Method of Test,
No. Ref to
VGI0 VG20 VG30 VG40
(1) (2) (3) (4) (5) (6) (7
i) Penetration at 25°C, 100 g. 5s, 0.1min, Min 80 60 45 35 IS 1203
ii) Absolute viscosity at 60C, Poises 800-1 200 1600-2400 2400-3 600 3200-4 800 IS 1206 (Part 2)
iii) Kinematic viscosity at 13S°C, cSt, Min 250 300 350 400 IS 1206 (Part 3)
iv) Flash point (Cleveland open cup), °C, Min 220 220 220 220 IS 1448 [P:69]
v) Solubility in trichloroethylene, percent, Min 99.0 99.0 99.0 99.0 IS 1216
vi) Sofening point (R&B), °C, Min 40 45 47 50 IS 1205
vii) Tests on residue from rolling thin film oven test:
a) Viscosity ratio at 60°C, Max 4.0 4.0 4.0 4.0 IS 1206 (Part 2)
b) Ductility at 25°C, cm, Min 75 50 40 25 IS 1208

precautions mentioned therein. Althesesanples from 8 PACKING AND MARKING


individual containers shall be stored separately.
8.1 Packing
7.4 Number of Tests
Bitumen of all types shall be suitably packed in a container
7.4.1 All the individual samples shall be tested for as agreed to between the purchaser and the supplier.
absolute viscosity at 60°C, penetration and softening
point tests. 8.2 Marking
7.4.2 For the remaining characteristies, a composite Each container of viscosity grade bitumen shall be
sample prepared by mixing together equal quantities legibly and indelibly marked with the following:
of paving grade bitumen, sampled, as the case may be. a) Manufacturer's name or trade-mark, if any;
from all individual samples taken from each sample
container, shall be tested. b) Month and year of manufacture;
c) Type of material and grade: and
7.5 Criteria for Conformity d) Batch number.
7.5.1 The lot shall be considered as conforming to the 8.3 BIS Certification Marking
requirements of this standard, if the conditions
mentioned under 7.5.2 and 7.5.3 are satisfied. The container may also be marked with the Standard
Mark.
7.5.2 From the test results of absolute viscosity at 60°C,
8.3.1 The use of Standard Mark is governed by the
penetration and softening point, the mean (X) and the provisions of the Bureau of Indian Standards Act, 1986
range (R) shall be calculated. The following conditions and the Rules and Regulations made thereunder. The
shallbe satisfied: details of conditions under which the licence for the
a) [x-0.6R] shall be greater than or equal to use of the Standard Mark may be granted to
the minimum specification limit specified in manufactures or producers may be obtained from the
Bureau of Indian Standards.
Table I, and
b) [x+ 0.6R] shall be less than or equal to the Table 2 Scale of Sampling
(Clause 7.2)
maximum specification limit specified in
Table 1. SI No. Lot Size No. of Containers
to be Selected
7.5.3 The composite sample when tested for the (1) (2) (3)
characteristics mentioned in 7.4.2 shall satisfy the i) Up to 50 3
corresponding requirements of the characteristics given 51-150
in Table l. ii 151-500
iv) 501 and above 10

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