Oaganie chamiby -I.

Date

Mehads o Punificatoiny o Organic

2. Gustallsatiau
CGmpounds.
4. Du<nntiil Extaace
chsomategiaply
5.

Fually th o ogani cbmhaund is detwmisd by

pusih
its
Nuw Mehad - ks dlleint types o chmatogabic and
spedhosopic duchiyus are alo sed the

i. stali hoatusa
stblimataa Cextaiw Ovganie solids on heating dissetly
change dm selid to vapaur stat withGd Yaasng
luidtati. such substances ate
ublimakle solid Vabeuw
Paiible - 3t is used do hu ebanho oh sublimable
componds dorom men- Aublimaale kinusutiA

2.
Kayslallisatisy- For sohd oganie cmbrands
Bunsle- t iu hased on the solubteo
o4 the smpound and the impuis in a suitabl solrent
Conbond is disohed solent n uhieh
p oubl at hoom tempenatne but abjoeeahly
at highe tenperaae So oganie cempund
soluble at

2) filtnaliew - The iltaed

loed to col
) ysallisathow- tot ktiat
Commod cystallies out
Spiral
 Date

s) Rmewal o Calsu Inpuitis uhic impant calwr

do th soutw are emeied by adusmhwiq
aciated, chax csal Cusala "xdisled
md add adivatd chiesal, boiled fo 1s-20 minito
Chareoal absebs a cadoued mibui. Fille t

and thn coolng

Vapsusa kack to the
To sehant ijid.
æ) yolahls 'uiuide oon nn

so- Liquico haung diesnl

Liauids Aaug
Vabours re wsled and id ane calleetad
Stmibl

Vapous are conden by a condnes

le n a eeeive

Splral
 Date
actional llaiaw he dieuene im boling
Lyuide miehh ( difew by o ta

Vafous

Vafouu dhe byid with hejhw boilng

lane bailing pounl
tuhe
beade
Simple Pached oamn Bubble late cutim
The vatous o low bailing cmþoneri ascent

Pene vapouns kou bailung paa thooya

Condnr

Pay byjuid is callletd in a Reeler.

amo &ueeiiedallatsn
byw
suceus biecondenoadw vakoisaliy

Sporal
 Date
istll athsw und
dhanto ano rhie deoapos atbeilang
hs o helno
"hein bilig bola oc Vacum Distllate)
’ Such yiola ani mace to boil at a templine
h
A A uud boilo at at whieu dto
th entnl p s e (Pesune
edcid by walw ump
sepanald
Steam Diaalin- Uud
Ueed to sepante substames
law volatio ano a nniscble nt
Wat
Stoamw doom seeam qenaor
hatd

Suam+ volatle
Condned

uiol bailo whenm the

and that heesmeo to

Spiral
 Date

Alin-dy mixtin

mitable ani soe (in 'utieh it is m

thss Watt).
The rie seent, shedd be

tien and ognie geret heuld fom

2) Ths wwste

Orgai iseat is it meed by

by 2) syaperaeie
ins anic rent
io addl to tract the combouid.

5.
alo to
thein caipeneht, fuiy combonds and
tyt Cimbaundo.
chooma
Mixtuu od substanco is
mto ou stati ena
A

aliinary phae
CMevng bhene' is Mabie bhae) Spral
 Date

chsmalsqra

Adssbiw chiat'gy
that
to

Adisbe ed Slca hel and, alumna

(a) slmn hromatagahy- t èwores Aebatsw

bha) aeked in a als tubi Com s httd
sith sto cck at tl Loner nd . ettd
slaed om the to oh adsobevt colun
packad in

foo aaun the mitne

lum
Deipndig ufpn the de to wrhic the
Comoundo ae adbad cocplslu Aebarata
taho ce. (mst ady adiohed substance
|b) Thuin ne
subtnes chSmataathy- t imblres
veY a thi ehansi
dont cAaod on a
 Date
adsobent /lica ql or
A hin layer

The xtue do be sebanat s

obat 2Cm abee

clsted
The þlaced
solent
As th alunt hses the
noveo ub dlonith lent to

Rotardtowactos Re vale)
()
R Distune meved by the substane oombase liie
Distane mered by tue salnt row bant line y)

24 Hhe oto od olounley combands an thu thue

aane inials to ye but lusese n uU hyht
2. Pla the late i a ereeo jar coctining lew
'Iodine compunda u'cl
mind aas is dettad
Ninbydin
botuee
nd mbile phasee
Spiral
 by
becombuno colsuls spoto The
ChiLtalU
Mehlu
at
ede cud sebanted apoto The ane
hu
J
actein Capillasy
the
by the
phase) (mbil stlrente tumix
satiSuabls at phas)
he it hibmssgra thpatd
babe stait A
 Date
UALITA TIVE ANALYSS 0E
OR GANICc0MPOUND S
tlomerda ombaundls
2. Oth elemnta eke
0, N, S, haleyns, P
. Doteeliew od hydhagen

toc0 ltuid itl ne, watrhat.tuns tubi)

A
C+ 2Cuo 2 u t C0,

ubid)

Ksus Cu SO uriih tuu blue)

2.4 Cu
5H0+ auso,
wiit
Othes lementa
Laseaigne, ls's teut - The elemuto beet
conerd too covalet
nto
tomjsund are
Aom byusing the
camfsund aidh Na
Na t CtN NacN
2 Nat S
Na X

N,S, Xtam ganie empands

This e h a c i CAdium

Sporal
 Date

baied wtu
entat is
Sodiim dued
Aulbhte nd hew
Isen(L
Cone. H, S0y
N

6 CN G2+

2. Test dos Sulbhu

s adeiled wth
0 saolum dumeuet acotat
acetie acid and addid
to t .

paeiblala ead
indi cats the
S+ PL

2) Sodiumm d i n ecbad is teatad ual

Sporat
 Date
S
Vioet.

Sadium enbact is uad with

Sadiumn tiounnate stutaw

Nat Ct N t S Nas N
Ce 3t 2-+
SCN -
Bloded
Sadium is casd t wt ecess Na
NasN + 2Na Na Nt Nq,S

Ladi um u etiact is aidid

Nibie acd and the tned tth Ag NO, Ssukos
A white bbt, atluble

Ayells t, inseluble in NH,0H ’ Iþalnt

X+
where Xio
Agt AgX

with Cone, NO, t decspee cyanid

Sporat
 dor Phosphsu
4) Test heatd sxiditang
Phosthoono foesent i he cenaund

boilsl itl conc HNOa and

The soluto
thew thatid witly Ammeiun Molylodat siln
At ind'eateo P
Ayelas eolouratisi or
Na, Po, 2
2 Na, O
o
5 Ng d t
+ 2f 2
aHNO ’ H, Poy taNa NO
Na, POy +
H, POy 2 (NH), Maly t 21 HNO,
Nh) POyJ2Mo0, t 21NEL, NO,
Ammn m t 2HD
Phophomlybdat
 Date

QUANTITATVE ANA LYSIS

To eotwn the mas
mass ewent of lemnt
Comhsund
L. Gbs and Hydhan stimatohw : -
Clmbsund
ano

C, Hane clies to ca Ho Aupin

thoagle a eighed.jAube

c is abssbed i ansherU- ube coátauiing

Caneentntad son. od kOH
&kOH

72 Xm Xo
44 xw
2X m, X on
&X m

Mas o co
2. Ectmahas Nuaagem 2 mothsds
mthad 2) Kjeldahl s metted
Spiral
 Dumas Msthsd hatd uth
I)
admaph
additein to Ce H0.

2
2
24

are

edrd ntteen by the

heat
dot th mas nganie camfaund V m
collectst
Rocm dempnatins=I K
+ 6o x I
(Let it be VmL)
youme ot N
P Atnmshiceee- AquesuA tenis
224 00 m N at SIP weiph
STP 28
Vml N, at =28/

fancalaye idnen = 28 Yloo

224 0D, m

Solral
 Date

2. Kildabl's Methad huntd

Combeund centaning nitse
ormAmmaniWm
H, Soy to
sushat
u thn hat
mi un
Resalng aid NaDH
absbad
The ibenaatid
ecs detamintd. by
the

amant t s0, cnwmad

dane by cimatny
Standard alka sohd
2NabH
(N,S0, 2NH
>Na S0,1t2H,D
Organi H, SO,i
Canpaund
2NHt H,S04 NHy), s0y.
ot the mas Organie cemthund =
Volume o Hso,o mslants Mtakenw =
)2

2 2
 Date
NM,
Mcarda!
4 x M x2( V- y

lercent N= 14 x Mx2(V-y

Thio nmtheo to
combunds cantanng Ntem wn nitho and
fea pysidine) as Ntnspiw o thee cembedo
dant
hang
3. 2stimate d Halaens Cahius Mothad
A tnn mass o anic Canpaund
gane
Aa NO soluie
hand tnbe (laviu tube)

the cambund ae

Salrat
 232
Boso,eomad ofMas
mtakn cmpsund organic o
mass the Lt
faziptah
waty
Bal ecess
o
,Sly aAddto
odised combund
is the S
HNOa
Sso'um uith
masA knauw A
SulbhA Estimahe
memaleul
Ag mas moleeula
mXy
mm mass atomie
Mass
antauns AX
tkncompsund Bganie wmas o heat's
Date
 Date

32-y me
233 m

2dimataw of Phoahts Bgunit cambsund

5. A

cbnbaund

Addud NH

mixtnu
&tnotely Adda
Phophic aciol is teeibdat as
M¡ NH, PO whih on
-

MAa mass

222x W
Ssral
 P0,= 222 w
Mass MPl, emd atom = 62
2

tu
b al other elemet
Adyintu mass of oyanic cmbund is

oxyien id conwrentd to Co.

wnd all
Wam
he mi tune is þaued thoa
when CO is
9odins bemtozide
Lsone

Comfound l373K, 2 C05

IO +50 I + 5CO, X2

Spiral
 Wthw
(i3mg)
and 'substns
amsnt dmal Veny 9t
dstemnao
by ane
pound þtalnt Nhem H, C,
lemeta ’
techss
autemate
ea Awelaneo
and th
heiimenal
awiis by out caind isod camp
elemint estvan o Pegenty
aoo elued tos Isdine an h
omduwed bealso Ox
88xWm
mobtuned
taken Campsund sganie masso the it
Date