Project 8th sem
Project 8th sem
Dissertation submitted to I.K Gujral Punjab Technical University, Jalandhar for partial
fulfillment of the requirement for the award of Bachelor of Pharmacy Degree
SUBMITTED BY:
BAVNEET KAUR
M.Pharmacy ( Pharmaceutics)
CERTIFICATE
…… ……………………
Dr.(Prof)Meenakshi Ratra
Ph.D.Pharmacology
(Principal)
V.M.S College of Pharmacy,Batala
CERTIFICATE
This is certified that project work entitled; PREPARATION AND EVALUATION OF HERBAL
SHAMPOO . is submitted in a partial fulfillment of the degree of Bachelor of Pharmacy Under
Punjab Technical University has been carried out by BAVNEET KAUR Student of 7th Semester B
pharmacy, Under my Supervision and Guidance.
Guide
…………………………
M.Pharmacy ( Pharmaceutics)
It is a great pleasure for me to submit this minor project on “Preparation & Evaluation of
Herbal Shampoo” as a part of curriculum for award of “ Bachelor of Pharmacy” of VMS College
of Pharmacy.
I would like to thank those who are involved in this endeavor for their kind
cooperation for successful completion of this project. I take opportunity to express my sincere
gratitude and deep sense of indebtedness toward my respected Guide “Mrs. Satvir Kaur” who
has inspired me throughout the project. Without her help & support this project work would not
have been this success. I would also like to thank my father for his great support. I wish to thank
to all my teachers and fellow friends for their advice and motivation.
ABSTRACT 6
HAIR 9-12
18-19
HERBAL SHAMPOO
20-22
HERBS
EVALUATION OF
PREPAREDFORMULATION 26-27
RESULT 28
CONCLUSION 30
REFERENCES 31
The shampoo sector is probably the largest unit sale among the hair care products since
shampoos are one of the cosmetic products used in daily life. Synthetic preservatives and
detergents have sometimes been the cause of adverse effects among consumers. A more radical
approach in reducing the synthetic ingredients is by incorporating natural extract whose
functionality is comparable with their synthetic ingredients. A shampoo is a cleaning aid for the
hair and is counted among the foremost beauty products. Today’s shampoo formulations are
beyond the stage of pure cleaning of the hair. Additional benefits are expected, e.g.,
conditioning, smoothing of the hair surface, good health of hair, i.e., hair free of dandruff, dirt,
grease and lice and, above all, its safety benefits are expected. As the scalp is one of the most
absorbent part of the body, products applied to the scalp go directly to the blood, without being
filtered in any way. In the scenario of changing food habits, stress level and dependent
environment conditions, number of skin and hair disorders are encountered. This herbal shampoo
was formulated using natural ingredient like Fenugreek seeds), Acacia concinna (shikakai),
Sapindus mukorossi (reetha), Ocimum sanctum (tulsi), Aloe vera (aloe), Hibiscus rosa sinensis
(china rose), Embelica officinalis (amla), Lawsonia inermis (henna),Citrus lemon (lemon), with
proven efficacy of hair care preparation is prepared. The combination of several such ingredient
of herbal origin has made it possible to secure highly effective dry powder shampoo. The
formulation at laboratory scale was done and evaluated for number of parameters to ensure its
safety and efficacy.
Cosmetic Science is a Wide Field of Today’s Era. The Word Cosmetic is a Greek Word
“Kosmetica” which means “to aborn.”
The Things used for the Beautification is also known as Cosmetic Products.
The cosmetics are more important due to advance Technology like Excess use of
Mobile and gadgets evolve Hazardous & Dangerous Radiatons like UV, IR and
Radiowaves.
For instance, if we take a case of Hair Graying so this was not seen in youngsters in
ancient times But now-a-days it is commonly seen in teenagers . To solve this problem
and Maintain Beauty Status is the main use of Cosmetic Products.
In this Modern Era, the Term “HERBAL”is a topic of Spotlight in the Field of Cosmetic
Science. Herbal means the use of Plant and Plant Derived Products which has the
Medical Significance and Products are Prepared using Natural Methods and many more.
Customer are getting Attracted Towards the Herbal Productsdue to the reason of Having
More Benefits with Less Side Effects as well as Budget Friendly as compare to Syntetic
Cosmetics.
It is Seen that in ancient days, Herbal Products was like the direct use of Plant Extract
Directly on Hairs and Skin. But Due to Advancement , Herbal Product also look like
synthetic means with Respect to Texture, Formulation, Type, Fragrance, and also Easy to
use.
The ingredients which are unsafe for the human use are restricted to be used in
Cosmetic industry . FDA and regulations has prohibited the use of Bithionol,Chlorofluorocarbon
propellants, Chloroform, Hexachlorophene, Mercury compounds, Methylene chloride, Vinyl
chloride in aerosols, Additive colors are only permitted only when FDA has approved.
HAIR
ANATOMY OF HAIR:
The hairs is composed of column of dead keratinized epidermal cells which are bonded by
proteins. The hair shaft is superficial portion of hair, which projects above surface of skin. The
root is portion of hair deep to shaft which penetrates into the dermis and shaft. The shaft and
root of the hair consists of 3 layers of cells
LAYERS OF HAIR
MEDULLA CORTEX CUTICLE
Middle cortex forms the major part Inner medulla is composed of 2-3 rows of cells which
contains pigment in dark hair and if pigment is less than it is gray hair
Middle Cortex is the major part of shaft and has elongated cells.
Cuticle of hairs, the outermost layer has single layer of thin, flat cells which has high
keratin.
At surrounding the root hair is hair follicle which are made up of external sheath and
internal root sheath. Both external & internal root shaft are collectively known as Epithelial root
sheath. The dense dermis surrounding the hair follicle is called Dermal rooth sheath .The hair
TYPES OF HAIRS:
HAIR PROBLEMS:
1.HAIR LOSS: - Here there is the hair loss or fall from the scalp. This hair loss can occur due to
various factors like stress, health issues, intake of various medicines or by using excess or
harmful cosmetic products.
2.SPLIT ENDS: - In these conditions the hair ending has two ends and it is due to lack of
conditioning of hairs or heat exposure of hairs.
3.FRIZZY AND OILY HAIRS: - The hairs become frizzy and dry due to less moisture content
in the hairs.And oily hairs are due to the excessive production of oil from the hair scalp.
4.GRAY HAIRS: - This occurs due to the improper nourishment of the hairs or it occurs due to
the various environmental factors.
5.DANDRUFF: - This occurs due to fungal or bacterial infection in the hairs. This occurs due to
improper cleaning of the dirt from the scalp.
HISTORY OF SHAMPOO:
In Indian subcontinents, a wide variety of herbs were extracted to prepare the shampoo. In
early days the effective shampoos were prepared by the use of Gooseberry i.e. Amla and the
Sapindus which is called as soapnut.
It contains the fruit pulp which contain the secondary metabolite Saponin which act as
a Natural surfactant.
The Soapberries make the hairs soft, shiny and silky. During the early days in Europe
the hair stylist was using soap and boiling it with water and also added herbs and various
fragrance. In India, the CHIK India the ‘’CHIK INDIA’’ in 1983. It was the first sachet shampoo
introduced in India.
Across India in many households Grandmother still follows various practice like
Drying the parts of medicinal plants like stems, roots, dried leaves etc. and then make the paste
to apply on the hairs.
The shampoo manufacturers in India were evolved since 1960’s. This became the part of
lifestyle in new and developing India.
Till 2005 there were only the highly named and famous industries like Hindustan
Unilever and Procter and Gamble.
• The P & G is also dominating the market with the brands names like Pantene, Head &
Shoulders –
The other major manufacturing industries are Daber, Cavin kare and Garnier
• Dev Care is also one of the top list Shampoo manufacturer in India and this industry
believe in offering compelling and innovative products to customers across the globe. It
also manufacture the herbal products.
• Elegant Cosmed Pvt. Ltd. Was established in year 2006. This company is exporting
wide range of pharmaceutical products.
• New moon Cosmetics Private limited was being established in year 2013.
For the herbal shampoo industries the top names are Himalaya Drug and
Company and Patanjali.
• Himalaya drug company was founded and formed in the year 1930, Total 91 years
ago By Mohamed Manal. It has its headquarters in Bengaluru, Karnataka . It is a global
It is a ayurvedic industry which formulate its products using natural products. They
are serving Worldwide. This manufacturing industry has wide range of products Start From
food articles Till Personal care products and also manufacture the wide range of medicines
and also all the good and necessary which any person requires on daily basis.
1.SURFACTANTS: - Surfactants are added in shampoo because they are capable in producing
the required quantity of foam.
There are 2 types of Surfactants i.e., ANIONIC AND CATIONIC surfactant. But in
formulation of shampoo the ANIONIC surfactant are preferred widely.
ANIONIC SURFACTANT: - They have good foaming ability. In its structure the
Hydrophilic part has negative charge and which helps to produce the foam and clean the
dirt.
CATIONIC SURAFACTANT: - They are Toxic in nature and hence are not used to
avoid the toxicity. But they are used in low concentration in the formulation of Hair
Conditioner.
2.CONDITIONING AGENTS: - This are added in shampoo to add the conditioning property to
the action of shampoo.
Examples: - Electrolytes like NaCl, Natural gums, Cellulose derivatives, PVP Etc.
5.PERFUMES: - This are added to the shampoos for imparting the pleasant aroma and odour.
6.PRESERVATIVE AGENTS: - This are added to the shampoo for increasing their stability
and shelf life of product. Examples – Formaldehyde and methyl paraben.
During the preparation of shampoo, the Surfactant are added then this surfactant molecule
present in the shampoo has a Hydrophilic head and lipophilic tail in their structure. When we
apply the shampoo on the scalp or hair using water then it tends to produce the foam.
Here the hydrophilic end of surfactant molecule in in contact with water and lipophilic
tail is in contact with the oil, dirt and grease present on scalp area.
Then this molecule can form the micelle when they are used in high concentration. So, the dirt is
HERBAL SHAMPOO:
* EASE APPLICATION
* REMOVAL OF DEBRIS
* LOW IRRITANCY
They did not provoke allergic reaction and do not have negative side effects.
DEMERITS:
Herbal drugs having slower effect than allopathic drug hence require long term therapy.
Amla is also stated as the Indian gooseberry. Amla contains Vitamin-C which increases
the amount of antioxidants in our body. These antioxidants are Flavonoids and polyphenols.
Amla Extract or amla oil helps to promote hair growth, and it reduce the damage and also
prevent graying of the hairs. Amla powder has the anti-inflammatory effect. It is added to the
herbal hair dyes like henna to enhance the color of dye. It helps to boost the volume of the hairs
and also reduce the Hair Lice. Amla is also rich in tannins, iron, calcium, phosphorus.
FIGURE.7 AMLA
Reetha commonly is called as Indian Soapberry, washnut, and soapnut .Reetha belongs to the
Family Sapindacea. It is the deciduous tree that grows in the lower Foothills and Midhills of
FIGURE .8 REETHA
It provides shine to the hairs and also prevents the graying of hairs. It is an herb especially
used for controlling hair fall and dandruff. It has cleansing and antifungal properties
FIGURE.9 SHIKAKI
Hibiscus is a Flowering plant belonging to the Malvaceae family. Hibiscus is the most
renowned herb for promoting hair growth. It helps to prevent Hair loss by using flower and leaf
extract when used in shampoo formulation. Hibiscus flower has a ability to reduce the Premature
FIGURE.10 HIBISCUS
Aloe Vera belongs to Family Liliacea. Aloe vera cleanses the scalp while keeping your hair
shiny and soft. Aloe vera can significantly decrease the scaliness and itchiness.
Objective:
1) To formulate the herbal shampoo.
7) To imparting gloss to hair and to maintain their manageability and oiliness for hairs.
INGREDIENTS:-
PROCEDURE:-
2.Then prepare the Extract of Hibiscus , Amla And Shikakai by adding each powder in separate
Beaker and then add 50ml of sterile water in each and boil that extract .
3.Then add 1gm of gelatin powder to 50ml of Boiling Water For preparing the Gelatin Solution.
4.Then Take Mortar Pestle and then add all 4 extracts of herbs in that and triturate them.
5.Then Strain that mixture using sieve and then take that residue in Measuring Cylinder and
Make Up the Volume Using Gelatin Solution
6.Then add Few Drops of Rose Oil Using Dropper to impart the Pleasant Fragrance to the
Shampoo.
7.Then Check the PH Level of formulation and then adjust the ph. adding Citric acid.
DISPERSSION TEST: -
This evaluation test is performed to Check the Cleansing or Dirt Removing Action of the
prepared Shampoo. Here initially shampoo is taken in test tub and then water is added and then
add the drops of ink in test tube. Then shake test tube and check the intensity of the foam. The
light foam produced is the indication good cleansing action of shampoo.
V.M.S College of Pharmacy Page 27
FIGURE.15 DIRT DISPERSION TEST RESULT
Calculations: -
The initial weight of the Porcelain dish (A)= 76.10 gm
RESULTS:
1.Hair Conditioners: - This helps to change the texture and appearance of hairs and helps to
recover the hair damage. It makes hairs shiny, silky, glossy, make hair easy to comb.
2.Hair Oils: - Hair Oils are used to nourish the hairs. They are used to increase growth of the
hairs, strength of the hairs. This hair oils are prepared by extracting the oils of herbs from natural
methods. They are used to promote the hair growth by massaging the oil on scalp which
penetrates in the scalp deeply and give nutrition to hairs.
2. Hair Dyes and Colorants: - They are used to color the hairs with different color shades
from black,brown to red and many more. They are used to deal with graying of hairs. The
most famous brands of Hair dyes are L’Oréal Paris, Garnier, Wellwa and etc.
CONCLUSION:-
The development of naturally emerging HERBAL cosmetics will be the wide and
major area of growth in the cosmetics industries in the upcoming years.
The use of herbal cosmetics has been increased to many folds in personal care system
and there is a great demand for this herbal cosmetic.
REFERENCES:
1) Smith, J. (2020). "Introduction to Cosmetic Science: A Comprehensive Overview."
Journal of CosmeticScience, 20(3), 123-135.
2) Johnson, A. B. (2018). "Evolution of Cosmetic Products: From Ancient Times to Modern
Innovations."Cosmetic History Review, 15(2), 87-102.
3) Regulatory Authority, National. (2020). "Guidelines for Cosmetic Product Regulation: A
Comparative Analysis." Regulatory Journal, 35(4), 265-278.
4) .Ishii MK. Objective and instrumental methods for evaluation of hair