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Project 8th sem

The document is a dissertation submitted by Bavneet Kaur for the Bachelor of Pharmacy degree, focusing on the preparation and evaluation of herbal shampoo. It discusses the significance of herbal ingredients in shampoo formulations, their benefits over synthetic products, and the methodology for creating and testing the shampoo. The project emphasizes the safety and efficacy of herbal shampoos in addressing common hair issues while adhering to regulatory standards in the cosmetic industry.

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0% found this document useful (0 votes)
247 views

Project 8th sem

The document is a dissertation submitted by Bavneet Kaur for the Bachelor of Pharmacy degree, focusing on the preparation and evaluation of herbal shampoo. It discusses the significance of herbal ingredients in shampoo formulations, their benefits over synthetic products, and the methodology for creating and testing the shampoo. The project emphasizes the safety and efficacy of herbal shampoos in addressing common hair issues while adhering to regulatory standards in the cosmetic industry.

Uploaded by

bavneet18kaur
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as DOCX, PDF, TXT or read online on Scribd
You are on page 1/ 32

Review on “PREPARATION AND EVALUATION OF HERBAL SHAMPOO”

Dissertation submitted to I.K Gujral Punjab Technical University, Jalandhar for partial
fulfillment of the requirement for the award of Bachelor of Pharmacy Degree

Bachelor of Pharmacy (7th Sem)

SUBMITTED BY:

BAVNEET KAUR

Regd No. 2117920

Under the Guidance and Supervision of

MRS. SATVIR KAUR

M.Pharmacy ( Pharmaceutics)

VMS COLLEGE OF PHARMACY, BATALA

V.M.S College of Pharmacy Page 1


“PREPARATION AND EVALUATION OF HERBAL SHAMPOO”

CERTIFICATE

This is certified that a project work entitled; “PREPARATION AND EVALUATION OF


HERBAL SHAMPOO”.Submitted to Punjab Technical University, Jalandhar for partial
fulfillment of the requirement for the award of Bachelor of Pharmacy Degree. It ensures that the
entire work carried out during completion of work is bonafide work done by himself under the
Guidance of Mrs.Akshi Sharma at V.M.S College of Pharmacy. Batala, Gurdaspur. The current
work of project has not been submitted to any other university for award of Degree of Bachelor
of Pharmacy.

…… ……………………
Dr.(Prof)Meenakshi Ratra
Ph.D.Pharmacology
(Principal)
V.M.S College of Pharmacy,Batala

V.M.S College of Pharmacy Page 2


“PREPARATION AND EVALUATION OF HERBAL SHAMPOO”

CERTIFICATE

This is certified that project work entitled; PREPARATION AND EVALUATION OF HERBAL
SHAMPOO . is submitted in a partial fulfillment of the degree of Bachelor of Pharmacy Under
Punjab Technical University has been carried out by BAVNEET KAUR Student of 7th Semester B
pharmacy, Under my Supervision and Guidance.

Guide

…………………………

MRS. SATVIR KAUR

M.Pharmacy ( Pharmaceutics)

V.M.S College of Pharmacy Page 3


ACKNOWLEDGEMENT

It is a great pleasure for me to submit this minor project on “Preparation & Evaluation of
Herbal Shampoo” as a part of curriculum for award of “ Bachelor of Pharmacy” of VMS College
of Pharmacy.

I would like to thank those who are involved in this endeavor for their kind
cooperation for successful completion of this project. I take opportunity to express my sincere
gratitude and deep sense of indebtedness toward my respected Guide “Mrs. Satvir Kaur” who
has inspired me throughout the project. Without her help & support this project work would not
have been this success. I would also like to thank my father for his great support. I wish to thank
to all my teachers and fellow friends for their advice and motivation.

DATE: …………………….. Bavneet Kaur

Roll no. 2117920

B.Pharmacy [7th Sem]

VMS College of Pharmacy, Batala

V.M.S College of Pharmacy Page 4


TABLE OF CONTEXT:

ABSTRACT 6

COSMETIC SCIENCE 7-8

HAIR 9-12

INTRODUCTION ABOUT 13-17


SHAMPOO

18-19
HERBAL SHAMPOO

20-22
HERBS

PREPARATION OF HERBAL 23-25


SHAMPOO

EVALUATION OF
PREPAREDFORMULATION 26-27

RESULT 28

HAIR CARE PRODUCTS 29

CONCLUSION 30

REFERENCES 31

V.M.S College of Pharmacy Page 5


V.M.S College of Pharmacy Page 6
ABSTRACT

The shampoo sector is probably the largest unit sale among the hair care products since
shampoos are one of the cosmetic products used in daily life. Synthetic preservatives and
detergents have sometimes been the cause of adverse effects among consumers. A more radical
approach in reducing the synthetic ingredients is by incorporating natural extract whose
functionality is comparable with their synthetic ingredients. A shampoo is a cleaning aid for the
hair and is counted among the foremost beauty products. Today’s shampoo formulations are
beyond the stage of pure cleaning of the hair. Additional benefits are expected, e.g.,
conditioning, smoothing of the hair surface, good health of hair, i.e., hair free of dandruff, dirt,
grease and lice and, above all, its safety benefits are expected. As the scalp is one of the most
absorbent part of the body, products applied to the scalp go directly to the blood, without being
filtered in any way. In the scenario of changing food habits, stress level and dependent
environment conditions, number of skin and hair disorders are encountered. This herbal shampoo
was formulated using natural ingredient like Fenugreek seeds), Acacia concinna (shikakai),
Sapindus mukorossi (reetha), Ocimum sanctum (tulsi), Aloe vera (aloe), Hibiscus rosa sinensis
(china rose), Embelica officinalis (amla), Lawsonia inermis (henna),Citrus lemon (lemon), with
proven efficacy of hair care preparation is prepared. The combination of several such ingredient
of herbal origin has made it possible to secure highly effective dry powder shampoo. The
formulation at laboratory scale was done and evaluated for number of parameters to ensure its
safety and efficacy.

V.M.S College of Pharmacy Page 7


COSMETIC SCIENCE :-

 Cosmetic Science is a Wide Field of Today’s Era. The Word Cosmetic is a Greek Word
“Kosmetica” which means “to aborn.”

 The Things used for the Beautification is also known as Cosmetic Products.

 Cosmetics is a topic of great importance . It plays vital role in maintaince of beauty of


any human being.

 The cosmetics are more important due to advance Technology like Excess use of
Mobile and gadgets evolve Hazardous & Dangerous Radiatons like UV, IR and
Radiowaves.

 For instance, if we take a case of Hair Graying so this was not seen in youngsters in
ancient times But now-a-days it is commonly seen in teenagers . To solve this problem
and Maintain Beauty Status is the main use of Cosmetic Products.

 Whereas, Cosmetic is also in demand Because in Today’s World of Competition Each


and Every Person has to keep their Personality Up to Date.

 In this Modern Era, the Term “HERBAL”is a topic of Spotlight in the Field of Cosmetic
Science. Herbal means the use of Plant and Plant Derived Products which has the
Medical Significance and Products are Prepared using Natural Methods and many more.

 Customer are getting Attracted Towards the Herbal Productsdue to the reason of Having
More Benefits with Less Side Effects as well as Budget Friendly as compare to Syntetic
Cosmetics.

 It is Seen that in ancient days, Herbal Products was like the direct use of Plant Extract
Directly on Hairs and Skin. But Due to Advancement , Herbal Product also look like
synthetic means with Respect to Texture, Formulation, Type, Fragrance, and also Easy to
use.

 Cosmetics Products has a very large categories like Shampoo,Powders, Gels,


Facewashes, Lipstics, Creams, Lotions, Soaps, Perfume and many more.

DRUG AND COSMETIC ACT 1940:


V.M.S College of Pharmacy Page 8
The D&C ACT 1940 is an act which Regulates the Import, Manufacturing
and Sale of various Drugs and Cosmetics. This Act was passed on 10th April 1940. D&C
contains 168 Rules and 25 Schedules from A-Y. Schedule S contains the Standards for
Cosmetics. In India, Cosmetics are regulated by Central Drugs Standard Control
Organization(CDSCO).

SIGNIFICANCE OF FORMULATED HERBAL SHAMPOO: -


The formulated herbal shampoo helps to make the hair dandruff free,
promotes hair growth and cleanse the dirt present on scalp and hairs. The formulated shampoo is
herbal in nature so it can be concluded that it imparts less side effect and is safe to use .

PROHIBITED COSMETICS AND INGREDIENTS IN


COSMETIC INDUSTRY:-

The ingredients which are unsafe for the human use are restricted to be used in
Cosmetic industry . FDA and regulations has prohibited the use of Bithionol,Chlorofluorocarbon
propellants, Chloroform, Hexachlorophene, Mercury compounds, Methylene chloride, Vinyl
chloride in aerosols, Additive colors are only permitted only when FDA has approved.

CONDITIONS FOR OBATAINING LICENSE FOR


MANUFACTURE AND SALE OF COSMETICS:-

All regulation related cosmetics are issued by Central Drugs Control


Organization (CDSO). For manufacture,import and sale of cosmetics the License will be issued
on FORM 22.

HAIR

V.M.S College of Pharmacy Page 9


 Hair is the integral part of human beauty
 Hair is protein filament that grows from follicles on the dermis or skin.
 Scientific is a component of the integumentary system and extends downward into a
dermal layer where it sits in the hair follicle.
 Hair present on head part is related to the beauty, also it provide protection of scalp
from any external injury and UV rays whereas, eyebrows and eyelashes protects eyes
from external foreign particles.
 Toule receptors which are associated with hair follicle which are activated when hair is
moved slightly. So therefore, the hairs function in sensing light touch.

ANATOMY OF HAIR:
The hairs is composed of column of dead keratinized epidermal cells which are bonded by
proteins. The hair shaft is superficial portion of hair, which projects above surface of skin. The
root is portion of hair deep to shaft which penetrates into the dermis and shaft. The shaft and
root of the hair consists of 3 layers of cells

LAYERS OF HAIR
MEDULLA CORTEX CUTICLE

 Middle cortex forms the major part Inner medulla is composed of 2-3 rows of cells which
contains pigment in dark hair and if pigment is less than it is gray hair

 Middle Cortex is the major part of shaft and has elongated cells.

 Cuticle of hairs, the outermost layer has single layer of thin, flat cells which has high
keratin.

At surrounding the root hair is hair follicle which are made up of external sheath and
internal root sheath. Both external & internal root shaft are collectively known as Epithelial root
sheath. The dense dermis surrounding the hair follicle is called Dermal rooth sheath .The hair

V.M.S College of Pharmacy Page 10


matrix cells arise from stratum basal and it is responsible for the growth of existing hair and they
produce new hairs when old hairs shed off.

STRUCTURE OF HAIR & ITS ANATOMY:

FIGURE.1 STRUCTURE OF HAIR

TYPES OF HAIRS:

V.M.S College of Pharmacy Page 11


i. Straight hairs

ii. Wavy hairs

iii. Curly hairs

iv. Coily hair

FIGURE.2 TYPES OF HAIR

HAIR PROBLEMS:

V.M.S College of Pharmacy Page 12


In this contemporary era, High Stress level, Unbalanced Diet and even Home hair treatments
are among the possible reasons younger generations are noticing many problem related to Ha

FIGURE.3 BASIC HAIR ISSUES

VARIOUS PROBLEMS ASSOCIATED WITH HAIRS: -


There are various problems related with hair health and they are discussed as following: -

1.HAIR LOSS: - Here there is the hair loss or fall from the scalp. This hair loss can occur due to
various factors like stress, health issues, intake of various medicines or by using excess or
harmful cosmetic products.

2.SPLIT ENDS: - In these conditions the hair ending has two ends and it is due to lack of
conditioning of hairs or heat exposure of hairs.

3.FRIZZY AND OILY HAIRS: - The hairs become frizzy and dry due to less moisture content
in the hairs.And oily hairs are due to the excessive production of oil from the hair scalp.

4.GRAY HAIRS: - This occurs due to the improper nourishment of the hairs or it occurs due to
the various environmental factors.

5.DANDRUFF: - This occurs due to fungal or bacterial infection in the hairs. This occurs due to
improper cleaning of the dirt from the scalp.

INTRODUCTION ABOUT SHAMPOO:

V.M.S College of Pharmacy Page 13


A liquid or cream preparation of soap or detergent to wash the hair is called as shampoo.
Shampoo are the cosmetics preparations which are prepared for the cleansing of dirt and debris
from the hair scalp. The shampoo generates its action by creating the foam. The additional
functions of shampoo are Hair growth and enhancement, hair conditioning, for dandruff
removal and many more. Shampoo are meant for the massage of head and scalp. This concept
was introduced by Britain and its was derived as ‘CHAMPOO’. Before the evolution of the
shampoo people were using the soaps for their personal care.

In the present scenario, it seems improbable that herbal shampoo, although


better in performance and safer than the synthetic ones, will be popular with the consumers. A
more radical approach in popularizing herbal shampoo would be to change the consumer
expectations from a shampoo, with emphasis on safety and efficacy. The word shampoo in
English is derived from Hindustani shampoo. Shampoos are typically composed of 10 to 30
ingredients.

HISTORY OF SHAMPOO:
In Indian subcontinents, a wide variety of herbs were extracted to prepare the shampoo. In
early days the effective shampoos were prepared by the use of Gooseberry i.e. Amla and the
Sapindus which is called as soapnut.

It contains the fruit pulp which contain the secondary metabolite Saponin which act as
a Natural surfactant.

The Soapberries make the hairs soft, shiny and silky. During the early days in Europe
the hair stylist was using soap and boiling it with water and also added herbs and various
fragrance. In India, the CHIK India the ‘’CHIK INDIA’’ in 1983. It was the first sachet shampoo
introduced in India.

Across India in many households Grandmother still follows various practice like
Drying the parts of medicinal plants like stems, roots, dried leaves etc. and then make the paste
to apply on the hairs.

V.M.S College of Pharmacy Page 14


VARIOUS SHAMPOO MANUFACTURINGINDUSTRES IN INDIA:-

The shampoo manufacturers in India were evolved since 1960’s. This became the part of
lifestyle in new and developing India.

Till 2005 there were only the highly named and famous industries like Hindustan
Unilever and Procter and Gamble.

The shampoo industries are divided in basic 2 sectors or platform like,

1.Synthetic shampoo industries

2.Herbal shampoo industries

• The Hindustan Unilever is a dominating industry in shampoo’s developing market in


India. The brand names of this industries are – Clinic Plus, Sun silk, Dove, TRES Emme
and many more.

• The P & G is also dominating the market with the brands names like Pantene, Head &
Shoulders –

which is highly successful brand in anti-dandruff shampoo.

 The other major manufacturing industries are Daber, Cavin kare and Garnier

• Dev Care is also one of the top list Shampoo manufacturer in India and this industry
believe in offering compelling and innovative products to customers across the globe. It
also manufacture the herbal products.

• Elegant Cosmed Pvt. Ltd. Was established in year 2006. This company is exporting
wide range of pharmaceutical products.

• New moon Cosmetics Private limited was being established in year 2013.

 For the herbal shampoo industries the top names are Himalaya Drug and
Company and Patanjali.

• Himalaya drug company was founded and formed in the year 1930, Total 91 years
ago By Mohamed Manal. It has its headquarters in Bengaluru, Karnataka . It is a global

V.M.S College of Pharmacy Page 15


industry for manufacturing of herbal products Like herbal cosmetics, ayurvedic
medicines, Personal care products, Child care products and Nutrition products. Himalaya
has its presence in 106 countries worldwide.

• Patanjali The Indian Multinational Company Situated in Haridwar India. It was


Founded by Ramdev and Balkrishna in 2006.

It is a ayurvedic industry which formulate its products using natural products. They
are serving Worldwide. This manufacturing industry has wide range of products Start From
food articles Till Personal care products and also manufacture the wide range of medicines
and also all the good and necessary which any person requires on daily basis.

FIGURE.6 BRANDS OF SHAMPOO

EXCIPIENTS USED IN MANUFACTURING OF SYNTHETIC SHAMPOO:

V.M.S College of Pharmacy Page 16


There is the wide range of excipients used in shampoo formulation and they are as follows –

1.SURFACTANTS: - Surfactants are added in shampoo because they are capable in producing
the required quantity of foam.

There are 2 types of Surfactants i.e., ANIONIC AND CATIONIC surfactant. But in
formulation of shampoo the ANIONIC surfactant are preferred widely.

 ANIONIC SURFACTANT: - They have good foaming ability. In its structure the
Hydrophilic part has negative charge and which helps to produce the foam and clean the
dirt.

 CATIONIC SURAFACTANT: - They are Toxic in nature and hence are not used to
avoid the toxicity. But they are used in low concentration in the formulation of Hair
Conditioner.

2.CONDITIONING AGENTS: - This are added in shampoo to add the conditioning property to
the action of shampoo.

Examples – Lanolin, Mineral oils etc.

3.VISCOSITY BINDERS: - This are added to make the shampoo viscous.

Examples: - Electrolytes like NaCl, Natural gums, Cellulose derivatives, PVP Etc.

4.OPACIFYING AGENTS: - Examples – Fatty acids, Propylene glycol, Mg Ca and Zn salts.

5.PERFUMES: - This are added to the shampoos for imparting the pleasant aroma and odour.

6.PRESERVATIVE AGENTS: - This are added to the shampoo for increasing their stability
and shelf life of product. Examples – Formaldehyde and methyl paraben.

7.ANTI-DANDRUFF AGENTS: - These are added in small concentration in shampoo. this


when comes in contact with scalp it helps to remove the Dirt and dandruff from the scalp .

V.M.S College of Pharmacy Page 17


CLEANSING ACTION OF SHAMPOO:

During the preparation of shampoo, the Surfactant are added then this surfactant molecule
present in the shampoo has a Hydrophilic head and lipophilic tail in their structure. When we
apply the shampoo on the scalp or hair using water then it tends to produce the foam.

Here the hydrophilic end of surfactant molecule in in contact with water and lipophilic
tail is in contact with the oil, dirt and grease present on scalp area.

Then this molecule can form the micelle when they are used in high concentration. So, the dirt is

removed and cleansed when it is rinsed off using water.

FIGURE.5 MODE OF ACTION OF SHAMPOO

HERBAL SHAMPOO:

V.M.S College of Pharmacy Page 18


Herbal Shampoo are made with the use of traditional ayurvedic herbs are meant for cleansing
the hair hair & scalp like other shampoo. There are no synthethic additives or surfactants are free
of side effects. They are used for removal of oils, dandruffs, dirt, environmental pollution etc.

FIGURE.4 HERBAL SHAMPOO

IDEAL PROPERTIES OF SHAMPOO:

* EASE APPLICATION

* REMOVAL OF DEBRIS

* SHOULD IMPART PLESEANT ODOUR TO HAIRS

* SHOULD NAVE GOOD SIABILID

* LOW IRRITANCY

* SHOULD PRODUCL ENOCON YOAN

* SHOULD PROVIDE NOURISHMENT TO HAIRS

* SHOULD MAKE HAIRS SILKY, GLOSSY.

ADVANTAGES & DISADVANTAGES OF HERBAL SHAMPOO:


V.M.S College of Pharmacy Page 19
MERITS :

 Easy to manufacture and cheap in cost.

 Easily available and found in large variety and quantity.

 They did not provoke allergic reaction and do not have negative side effects.

 Easily incorporate in skin and hair.

DEMERITS:

 Difficult to hide odour and taste sometimes.

 Herbal drugs having slower effect than allopathic drug hence require long term therapy.

 Manufacturing process is time consuming and complicated.

WONDER HERBS EVERY HAIR NEEDS:-

The HERBS are the magical plants which are present


in any herbal shampoo. They are magical because they do not have an extreme
level of side effects on the hairs.

V.M.S College of Pharmacy Page 20


In herbal shampoo preparations, the herbs used itself act as excipients
and they are derived from the herbal and medicinal origin. There are many such
herbal plants which has a versatile action on hairs and for hair care.

1. AMLA [Phyllanthus Emblica] :-

Amla is also stated as the Indian gooseberry. Amla contains Vitamin-C which increases
the amount of antioxidants in our body. These antioxidants are Flavonoids and polyphenols.
Amla Extract or amla oil helps to promote hair growth, and it reduce the damage and also
prevent graying of the hairs. Amla powder has the anti-inflammatory effect. It is added to the
herbal hair dyes like henna to enhance the color of dye. It helps to boost the volume of the hairs
and also reduce the Hair Lice. Amla is also rich in tannins, iron, calcium, phosphorus.

FIGURE.7 AMLA

2.REETHA [ Sapindus Mukorossi ]:-

Reetha commonly is called as Indian Soapberry, washnut, and soapnut .Reetha belongs to the
Family Sapindacea. It is the deciduous tree that grows in the lower Foothills and Midhills of

V.M.S College of Pharmacy Page 21


Himalaya. It is used as the hair cleanser. It makes hair healthy, shiny, lustrous. The reetha
powder can be mixed with the warm water to form a paste which can be used to massage the
scalp because it has an Insecticidal Property. The reetha powder along with amla powder is used
to control the Graying of Hairs.Reetha is an Age-old remedy that makes hair extremely soft,
gorgeous and beautiful. Reetha prevents the hair Dandruff. Reetha is antibacterial and antifungal
in nature, so its helps to treat the scalp infections and head lice. Reetha when combined with egg
they help to control the hair fall.

FIGURE .8 REETHA

3.SHIKAKAI [Acacia Concinna]:-

It provides shine to the hairs and also prevents the graying of hairs. It is an herb especially
used for controlling hair fall and dandruff. It has cleansing and antifungal properties

FIGURE.9 SHIKAKI

4. HIBISCUS [Hibiscus Rosa-sinensis] :-

Hibiscus is a Flowering plant belonging to the Malvaceae family. Hibiscus is the most
renowned herb for promoting hair growth. It helps to prevent Hair loss by using flower and leaf
extract when used in shampoo formulation. Hibiscus flower has a ability to reduce the Premature

V.M.S College of Pharmacy Page 22


graying of hairs. It also treats the dandruff and Conditions the hairs. Hibiscus Oil is beneficial for
promoting the Nourishment of hairs.

FIGURE.10 HIBISCUS

5. ALOE VERA [ ALOE BARBADENSIS] :-

Aloe Vera belongs to Family Liliacea. Aloe vera cleanses the scalp while keeping your hair
shiny and soft. Aloe vera can significantly decrease the scaliness and itchiness.

FIGURE .11 ALOE VERA

PREPRATATION 0F HERBAL SHAMPOO:

V.M.S College of Pharmacy Page 23


Importance:
 The selection of active ingredients for hair care shampoo is often based on the ability of
the ingredient to prevent damage to skin as well as to improve the quality of the
skin by way of cleansing, nourishing, and protecting the skin.

 It have not make the hand rough and chapped.


 It’s not give any side effects or causes irritation to the eye.
 It produces a good amount of foam to satisfy the psychological requirements.

Objective:
1) To formulate the herbal shampoo.

2) To evaluate the herbal shampoo.

3) The part used for formulation is leaves, fruits and root.

4) To reduce side effects of chemical formulation.

5) To improve hairs texture.

6) To darkening the hair color.

7) To imparting gloss to hair and to maintain their manageability and oiliness for hairs.

INGREDIENTS:-

V.M.S College of Pharmacy Page 24


Sr,No. Name of Ingredients Role of Agents Quantity required

1. Reetha Extract As Foaming Agent 10gm

2. Amla Extract To Provide Nourishment to 10gm


Hair
3. Shikaki Extract As Anti-Dandruff Agent 10gm

4. Hibiscus Extract As Hair Growth Promoter 10 gm

5. Gelatin Solution As Base 2%

6. Methyl Paraben As Preservative 1gm

7. Rose Oil To Adjust PH Level 2-3 drops

8. Citric Acid To Impart Fragrance As per requirement

FIGURE .12 INGREDIENTS USED FOR HERBAL SHAMPOO

PROCEDURE:-

V.M.S College of Pharmacy Page 25


1.Initially prepare the reetha extract by adding 30ml of 70% of ethyl alcohol and Keep aside for
the Cold Maceration.

2.Then prepare the Extract of Hibiscus , Amla And Shikakai by adding each powder in separate
Beaker and then add 50ml of sterile water in each and boil that extract .

3.Then add 1gm of gelatin powder to 50ml of Boiling Water For preparing the Gelatin Solution.

4.Then Take Mortar Pestle and then add all 4 extracts of herbs in that and triturate them.

FIGURE.13 TRITURATION OF HERBAL EXTRACTS

5.Then Strain that mixture using sieve and then take that residue in Measuring Cylinder and
Make Up the Volume Using Gelatin Solution

6.Then add Few Drops of Rose Oil Using Dropper to impart the Pleasant Fragrance to the
Shampoo.

7.Then Check the PH Level of formulation and then adjust the ph. adding Citric acid.

8.Then Perform the Various Evaluation Tests of prepared Formulation.

V.M.S College of Pharmacy Page 26


EVALUATION OF PREPARED FORMULATION :-

1.FOAMING INDEX DETERMINATION: -


Initially here place 5 test tubes in the test tube stand. Then add the stock solution i.e., the
prepared shampoo in each test tube by increase in volume means 1ml in first test tube, 2ml in
second test tube and so on. Then Make up the volume of each Test tube up to 10 ml using distil
water. Then Shake Each test tube to produce enough amount of foam. Then Measure the
produced foam using Ruling Scale and then Calculate the foaming index

FIGURE.14 TEST TUBE SHOWING FOAMING INDEX

Sr.No Quantity of stock Solution Height of Foam


.
1. 1ml 0.6 cm
2. 2ml 1.5 cm
3. 3ml 1.8 cm
4. 4ml 2.0 cm

2. DIRT 5. 5ml 2.3 cm

DISPERSSION TEST: -
This evaluation test is performed to Check the Cleansing or Dirt Removing Action of the
prepared Shampoo. Here initially shampoo is taken in test tub and then water is added and then
add the drops of ink in test tube. Then shake test tube and check the intensity of the foam. The
light foam produced is the indication good cleansing action of shampoo.
V.M.S College of Pharmacy Page 27
FIGURE.15 DIRT DISPERSION TEST RESULT

3. SOLID CONTENT DETERMINATION: -


In this test initially the Evaporating Dish or a Porcelain dish is taken and weighed and
recorded the initial weight. Then 4 gm of Shampoo is added in that and the plate is kept in hot air
oven. After drying then again weigh the dish and record the final weight.

FIGURE.16 SOLID CONTENT DETERMINAION RESULTS(A&B)

Calculations: -
The initial weight of the Porcelain dish (A)= 76.10 gm

The Final weight after evaporation (B) =76.45

Weight of sample = B-A = 76.45-76.10 = 0.35 gm

V.M.S College of Pharmacy Page 28


% Solid Content= (B-A) /4. 100 = 0.35/4.100 =0.0875.100=8.75%

RESULTS:

FIGURE.17 FORMULATED HERBAL SHAMPOO & LABEL OF HERBAL SHAMPOO

COLOR OF FORMULATION BROWNISH


ODOUR OF FORMULATION ROSE LIKE PLEASANT
APPAREANCE TURBID
FOAMING INDEX 500
DIRT DESPERENCY LIGHT
%SOLID CONTENT 8.75%

OTHER VARIOUS HAIR CARE PRODUCTS:

1.Hair Conditioners: - This helps to change the texture and appearance of hairs and helps to
recover the hair damage. It makes hairs shiny, silky, glossy, make hair easy to comb.

V.M.S College of Pharmacy Page 29


Conditioners are used to reduce the friction, detangle of hairs, and minimize the frizz.

2.Hair Oils: - Hair Oils are used to nourish the hairs. They are used to increase growth of the
hairs, strength of the hairs. This hair oils are prepared by extracting the oils of herbs from natural
methods. They are used to promote the hair growth by massaging the oil on scalp which
penetrates in the scalp deeply and give nutrition to hairs.

2. Hair Dyes and Colorants: - They are used to color the hairs with different color shades
from black,brown to red and many more. They are used to deal with graying of hairs. The
most famous brands of Hair dyes are L’Oréal Paris, Garnier, Wellwa and etc.

FIGURE.18 HAIR CARE PRODUCTS

CONCLUSION:-

V.M.S College of Pharmacy Page 30


There is the great development in COSMETICS SCIENCE. All over worldwide the
consumers are using the herbal cosmetics instead of chemical containing synthetic shampoos.
Because it is proven that the herbal products are not imparting the side effects hairs and skin.

The development of naturally emerging HERBAL cosmetics will be the wide and
major area of growth in the cosmetics industries in the upcoming years.

The use of herbal cosmetics has been increased to many folds in personal care system
and there is a great demand for this herbal cosmetic.

The use of bioactive ingredients in cosmetics which influence the biological


functions of hairs and skin and provides nutrients necessary for the healthy skin or hair.In future
there is the tremendous scope to launch and develop various and numerous herbal cosmetics
using appropriate bioactive ingredients with other suitable additives, excipients, and the
preservatives.

REFERENCES:
1) Smith, J. (2020). "Introduction to Cosmetic Science: A Comprehensive Overview."
Journal of CosmeticScience, 20(3), 123-135.
2) Johnson, A. B. (2018). "Evolution of Cosmetic Products: From Ancient Times to Modern
Innovations."Cosmetic History Review, 15(2), 87-102.
3) Regulatory Authority, National. (2020). "Guidelines for Cosmetic Product Regulation: A
Comparative Analysis." Regulatory Journal, 35(4), 265-278.
4) .Ishii MK. Objective and instrumental methods for evaluation of hair

V.M.S College of Pharmacy Page 31


care product efficacy and substantiation of claims. In: Hair and hair care.New York:
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Science and Technology, 2nd edition, Vol‐2, John Wiley India, New Delhi, 2008.
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Technology, 3rd Edition, Informa Healthcare, New York.
9) Badi KA, Khan SA. Formulation, evaluation and comparison of the herbal shampoo with
the commercial shampoo. Beni-Suef Univ J Basic Appl Sci 2014;3:301-5.
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and Distributer; 2001. p. 81-105.
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Science 2000;22:385-91.
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13) Ali HS, Kadhim RB. Formulation and evaluation of herbal shampoo from Ziziphus
spina leaves extract. Int J Res Appl Pharm 2011;2:1802-6.
14) Boonme P, Pakpayat N, Yotmanee K, Kunlawijitrungsee S, Maneenuan D. Evaluation of
shampoos containing silicone quaternary microemulsion. J App Pharm Sci 2011;1:59-63.
15) Principals of anatomy and physiology by GERARD J TORTORA / BRYAN
DERRICKSON 15TH EDITION.
16) Current Review on Herbs for derma care By Rashmi Saxena pal.
17) Review on hair problems and its solution By Ameya Lanjewar.
18) Maurya, Pawan, et al. "A Review Article on Herbal Shampoo." Journal of Emerging
Technologies and Innovative Research 8.5 (2021): 366.
19) 5 Patel, I. M. R. A. N., and A. D. N. Y. A. Talathi. "Use of traditional Indian herbs for the
formulation of shampoo and their comparative analysis." International Journal of
Pharmacy and Pharmaceutical Sciences 8.3 (2016): 28-32.
20) Rashid, K., et al. "Hair care promising herbs: a review." Pharmaceutical Research 10.03
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