Numerical investigation of composite metal foams using substructure techniques
Numerical investigation of composite metal foams using substructure techniques
Composite Structures
journal homepage: www.elsevier.com/locate/compstruct
A R T I C L E I N F O A B S T R A C T
Keywords: An accurate description of the mechanical behaviour of inhomogeneous, anisotropic composite materials, such as
Composite metal foams metal matrix syntactic foams (MMSFs), is a challenging task. This paper is based on the so-called substructure
Porous materials technique, which has never been used for the mechanical modelling of metal foams or MMSFs. Using this
Substructure technique
method, a finite element model with low computational requirements but still modelling inhomogeneous
FEM
properties can be constructed that reproduces the results of laboratory measurements with high accuracy. In all
cases, the tests presented in this paper are limited to the linearly elastic phase. As the most common investigation
of MMSFs is the compression test, this study considers only this loading case. A more detailed discussion of the
stress analysis of MMSFs is given at the end of this work. A potential cause of 45◦ crack planes during
compression tests and the evolution of stresses as a function of space-filling are also investigated.
* Corresponding author at: Department of Applied Mechanics, Faculty of Mechanical, Computer and Electrical Engineering, Széchenyi István University, Egyetem
tér 1., Győr 9026, Hungary.
E-mail address: [email protected] (M. Kovács).
https://doi.org/10.1016/j.compstruct.2024.118731
Received 5 June 2024; Received in revised form 4 October 2024; Accepted 18 November 2024
Available online 20 November 2024
0263-8223/© 2024 The Authors. Published by Elsevier Ltd. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-
nc-nd/4.0/).
M. Kovács et al. Composite Structures 353 (2025) 118731
of time is required to prepare and correct errors. In addition, despite the shown in Fig. 1.
small size, this method results in a model with a high computational The figure above shows the random distribution of hollow spheres in
complexity due to the large number of degrees of freedom (DoF) the transparent matrix material. In order to understand this novel
[13–15]. methodology, the substructure technique is first introduced in general
Another approach to studying the mechanical properties of MMSFs is and then a specific adaptation for modelling composite metal foams is
homogenization techniques. There are several different approaches. The presented.
simplest is when generalised material properties are defined, as if the
internal structure were homogeneous. Another method is to build the 2.1. Basics of substructure technique
model by repeating representative volume elements (RVEs). This allows
faster and significantly simpler models to be built with less computa- The substructure technique is based on the discretized equilibrium
tional requirements, but in many cases the accuracy of these finite equation in case of small displacements:
element models is less than that of the X-ray-based method [16–19].
One of the main aims of this study is to combine the advantages of Ku = f (1)
the two methods described above and to tackle their disadvantages. To
achieve this goal, to the Authors’ knowledge, a never-before-used where K is the stiffness matrix of the structure, f is the load vector and u
technique for modelling metal foams and MMSFs, namely the sub- is the unknown nodal displacement vector to be determined. In addition,
structure technique, is used. This is a technique that was invented in the the method also requires the definition of boundary conditions. The
1970 s, but until now it has been used to solve completely different basic idea behind the substructure technique is to separate the finite
problems. Typically, it has been used for vibration testing of large element model into nodes of interest that are usually on the surface of
structures, including aircrafts [20,21]. Subsequently, it has also been the body (boundary points) and nodes that are inside the body (internal
increasingly used for structural analysis of bridges and large buildings points). After that, Eq. (1) can be partitioned according to internal and
[22]. This technique has been largely combined with the finite element boundary points:
method (FEM) and model updating methodology [23–25]. [
Kii Kib
][ ] [ ]
ui fi
Due to the time step used in the model updating technique often = (2)
Kbi Kbb ub fb
being small, the reduction of the DoF is especially important to reduce
the calculation time and therefore the substructure technique has come where Kii is the stiffness matrix concerning the interior points, Kib and
to the fore [26–28]. It is essential to note, however, that the substructure Kbi describe the connection between the boundary and the interior
technique also needs to be adapted slightly for each application [29]. points, while Kbb is the stiffness matrix concerning the boundary points.
As mentioned above, several studies have investigated how the In addition, ub is the boundary and ui is the interior column vector of the
properties of MMSFs are affected by the geometry of the hollow spheres displacements and f b and f i denotes the load vectors of the boundary and
and their filling percentage. For this reason, this study will include the interior points. Since this paper deals with a quasi-static compression
effects of hollow spheres on each other and on the matrix material. The test, no volumetric load is applied, so f i equal to zero. When the
mechanical properties and meshing criteria of hollow spheres by multiplication of the matrix equation (2) is done, it results in the
themselves have already been dealt with before, but here it is not following equations:
enough to examine one piece by itself [30–32]. In many cases, the mesh
is densified at the contact points of spheres, but this is not possible for a Kii ui +Kib ub = f i = 0 (3)
large foam model because the number of DoF would be increased
enormously due to the large number of spheres [33]. It is important to Kbi ui +Kbb ub = f b (4)
note that the matrix material plays an essential role, as it has a large
An important assumption in this method is that the displacements of the
influence on the variation of the stress, so considering only the hollow
interior points are excluded and only the displacements of the boundary
spheres would be inaccurate [34]. In many cases, the effect of changing
points are taken into account. If Eq. (3) and Eq. (4) are combined and the
a single geometric property is investigated, but the effect of several
displacements of the boundary points are derived from them, the result
different parameters, such as the thickness of the walls of the hollow
is:
spheres or the distance between them are less studied [35]. The effects of
parameters can best be traced for models where the DoF is not very high − 1
(Kbb − Kbi K−ii 1 Kib ) f b = ub (5)
due to the size of the whole structure. However, those models must still
contain more hollow spheres [36,37]. Eq. (5) allows to define only the displacements of the boundary points.
This work has two main aims. One main goal is to use the sub- This is particularly useful in the present case, because the deformations
structure technique to construct a model of tetrahedral elements with
low computational requirements that accurately models the properties
of MMSFs [38–40]. The tetrahedral elements were chosen for easy nu-
merical integration [41,42]. This method has been previously discussed
by the author in the two-dimensional case [43]. In this work, the linearly
elastic phase is investigated.
The other part of the paper examines the combined effect of geo-
metric size, spacing, and material of the hollow spheres on stress, which
cannot be investigated under laboratory conditions.
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M. Kovács et al. Composite Structures 353 (2025) 118731
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M. Kovács et al. Composite Structures 353 (2025) 118731
The meshing software GMSH [44] was used to create the MMSF
models. In an experiment to verify the accuracy of the numerical
method, the MMSF specimen was compressed between two rigid plates.
An aluminium foil and lubricant were placed between the pressure
plates and the metal foam to avoid galling. The moving pressure plate
was modelled as a y − axial kinematic load. The plate at rest was
modelled as an elastic support where the y − axial displacement is
limited by a high stiffness value. The free displacement in the x and z
directions was allowed by the near-zero values of the stiffness matrix in
these directions. These boundary conditions are shown in the schematic
illustration in Fig. 5.
Since the kinematic load requires a specific load vector, the sum of
these vectors at each predetermined displacement value gives the force
that the pressure plates have to exert on the foam model. This force
value will be important for further comparison with laboratory results.
An example of a loading case on a finite element model is shown on the
left-hand side of Fig. 6. In the model assembled from the SFEs, one of the
Fig. 4. A schematic representation of the use of substructure techniques side plates was removed to show that the internal nodes no longer play a
for MMSFs. role in the displacement calculation. However, it can be seen that the
interpolated displacement field is different from the homogeneous ma-
inclusion sizes should be. But since inhomogeneity is not a quantifiable terial. Any arbitrarily selected substructure can be converted back into a
parameter, these cannot be precisely determined. This can also be seen conventional, solid structure. This is calculated by applying Eq. (9) to
from the fact that there is an extraordinary variety of MMSFs, since the the boundary displacement of the SFE. This gives the detailed
number of material pairs, hollow spheres, wall thicknesses and ratios in displacement field to the right-hand side of Fig. 6. However, this should
the matrix allow an infinite number of combinations. not be used too often, as it will significantly reduce the effectiveness of
Another approach could be to build the whole domain as one large the method. It is important to note that the substructure technique re-
model and include it in a single SFE. This would not be advantageous quires even more care in the preparation of the finite element mesh than
because then the meshing of a complex internal structure has to be re- a conventional model. This is because if an overly distorted element is
investigated and this leads back to the problem of finite element included in a substructure, it will cause inaccuracy as many times as that
model building based on X-ray imaging. substructure is built into the overall model.
Regardless of which method is chosen, only the displacements of the The efficiency of the method can be significantly increased if the
external points will be known. However, going back to Eq. (3), it can be point density at the boundaries of the SFEs is lower than inside the
seen that if the displacements of the boundary points are known, then substructures. At this point, it is useful to make a comparison between
after a rearrangement a formula can be obtained which can be used to three modelling aspects, which highlights the memory efficiency of the
determine the internal displacements of an arbitrary SFE: model on the left-hand side of Fig. 6. The first and most general method
( )− 1 has already been discussed, which involves a full meshing of the X-ray
− Krii Krib urb = uri (9)
where r is the number of the selected SFE and uri donates the internal
displacement field.
Table 1
Elastic properties of the filler and the matrix.
iron aluminium
Fig. 5. Schematic representation of boundary conditions where the kinematic
Modulus on elasticity [GPa] 19.6 71.0
load is represented by the blue arrows and the elastic support is indicated by the
Poisson’s ratio 0.250 0.334
arrows in red.
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M. Kovács et al. Composite Structures 353 (2025) 118731
Fig. 6. The complete model built from SFEs and the back-transformed displacement field of a selected SFE.
based model. In this case, there is not much possibility to increase the measuring 1000 hollow spheres on an Olympus SZX 16 type stereo
size of the finite elements to a large extent. For the case where the model microscope). The set of the MHSs was fixed by a stainless steel net at the
shown in Fig. 6 is not built using the substructure technique, but in the top of the assembly and the whole assembly was pre-heated to 300 ◦ C.
conventional way and the element size remains the same as shown on Subsequently and molten Al99.5 alloy (at 710 ◦ C) was poured on the top
the walls of the hollow spheres, the number of DoF is 6529008. When of the MHSs set. Ar gas was applied to force the molten matrix between
the substructure technique is used but the element size is not reduced the individual hollow spheres. After the casting and initial solidification,
towards the boundaries, this number is 1835181. This already repre- the whole structure was water cooled to room temperature. Afterwards,
sents a reduction of 71.9 %. However, if the element size increases to- the cast block was removed from the mould and the block was machined
wards the boundaries, as shown in Fig. 6, the number of DoF is only into 10.5 × 10.5 × 10.5 mm cubes for compressive tests. For further
24384. This represents a reduction of 99.63 % compared to the tradi- details about the production of MMSFs please refer to [45].
tional method, which already shows the inherent potential of the The compressive tests were conducted between flat plates in a
method. On the detailed displacement field of an SFE, it is already compression tool with four guide bars. The samples were lubricated by
possible to calculate a stress field on each pre-selected cubic region of Teflon foils to reduce the friction between the compressive plates. The
the entire model. An example of this is shown in Fig. 7, where Von Mises crosshead speed was set to 0.1 [mm/min] to ensure quasi-static condi-
stress is displayed. tion. During the measurement, the force and the displacement were
High-stress zones at 45◦ to the sides of the substructure can be registered by a 250 kN force cell and an extensometer. The force-
observed in the stress field. This phenomenon can be considered as one –displacement curves were transformed into engineering stress- engi-
of the reasons why the slip planes of the MMSFs appear at 45◦ . A more neering strain plots. The tests were conducted along the ISO13314
detailed understanding of stresses in MMSFs will be discussed in Section standard. During the finite element modelling, the material parameters
4. from Table 1 have been applied. Seven specimens were subjected to the
compression test, the curves of them are shown in Fig. 8. The complete
evaluation of the compressive results and the failure mechanisms of the
3.2. Experimental validation samples have been published in [45].
It can be seen that the curves differ from each other, which is a
For the validation of the numerical results, compression tests of the consequence of the inhomogeneous internal structure. Since the mea-
MMSF specimens with the same volume as the finite element model surement points do not coincide at all locations during the measure-
were performed. The MMSF samples were produced by low-pressure ment, the values of each curve must be determined by linear
infiltration. The metallic hollow spheres (MHSs, pure Fe in composi- interpolation at the same point on the x-axis. Afterwards, the data can be
tion, supplied by Hollomet GmbH, Dresden, Germany) were loosely used to construct the average pressure curve. This is shown in Fig. 9.
poured (ensuring ~ 50 vol% filling) into a steel mould coated by a However, this curve alone would not be enough to compare with the
graphite layer (N-77 graphite spray by DUE-CI ELECTRONIC s.n.c., results of the finite element model, so the standard deviation of the mean
Avesa, Italy) to prevent reactions between the matrix material and the values must be determined. This standard deviation becomes the one
mould. The nominal diameter of the hollow spheres was 1.92 ± 0.07 sigma value. Two times of this sigma has been selected for comparison.
mm, while their average wall thickness was 23 ± 0.6 µm (obtained by
5
M. Kovács et al. Composite Structures 353 (2025) 118731
Fig. 10. Comparison between the numerical approximation and the measurements.
6
M. Kovács et al. Composite Structures 353 (2025) 118731
plane to the load. The centre of such a region is shown by point P1 (see
Fig. 11). These are the regions with the highest stress in the matrix
material, which may be one reason for the frequent 45◦ slip planes in
MMSFs. The other matrix area under consideration is the scenario where
a volume of matrix material is under investigation between two hollow
spheres, and these hollow spheres are aligned with the load. The centre
of this region is shown by point P2 (see Fig. 11). Such zones are at that
point where the stress is always lowest. By increasing the distances t1
and t2 under constant load, the change in the stresses at points P1 and P2
was observed. The change in these distances represents a variation in the
space-filling percentage. Since a stress value by itself is meaningless, it
will be compared to a point near the boundary of the model at which the
stress is no longer affected by the hollow spheres. This point is P3. In
each step, when the distance t1 and t2 was increased, the stress values for
both ceramic and iron hollow spherical shells were investigated. The Fig. 12. Stress difference between P1 and P3 as a function of increase in dis-
properties of iron and matrix material are summarised in Table 1. tance t1.
Commonly used materials were chosen as the ceramic shell, the
composition of which is summarised in Table 2:
The properties of the mixed ceramics were determined by a simple
mixing rule. The modelled hollow spheres have a radius of 0.96 mm and
a wall thickness of 0.023 mm. It would not be necessary to specify these
dimensions, because if they change proportionally, the diagrams would
not change. The reason for specifying these values is to be able to assign
a unit of measurement to the axes. In the simulation, the distance be-
tween the hollow spheres was increased until the stress at reference
point P3 was sufficiently close to the stress of the points P1 and P2.
Therefore, from this point onwards, the difference between the reference
point and the point P1 or P2 must be observed. Fig. 12 shows how the
stress difference between points 1 and 3 changes with increasing dis-
tance t1.
The distance t1 started from 0.02 mm and was increased until the
stress at point P1 was nearly equal to the reference point. It can be seen
Fig. 13. Stress difference between P3 and P2 as a function of increase in dis-
that iron and ceramic hollow spheres result in nearly equal stresses, so
tance t2.
this factor does not have a large effect on the stress of the matrix ma-
terial. At the beginning, even with a small increase in the distance t1, the
stress difference decreases steeply up to 0.2 mm. It can be concluded that on the rearrangement of elements of matrices already existing in the
reducing the high space-filling percentage causes a significant change in conventional case and on the rearrangement of equations, no additional
the properties of the composite foam, which is in agreement with the numerical error is added to the calculation. In Section 4 of the paper, an
general experience. After a distance of 0.2 mm for both types of hollow additional analysis of the evolution of internal stresses in relation to
spheres, the stress difference shows a degressive characteristic after a space-filling percentage is also presented. Other factors, such as the wall
slight increase. However, at point P2 the distance, t2 had to be signifi- thickness of hollow spheres or the dispersion of spheres, were either not
cantly greater to reach the stress at the reference point. Fig. 13 shows mentioned because they have already been discussed in previous
how the stress difference between points 3 and 2 changes with studies, or because the specific location of hollow spheres had to be fixed
increasing distance t2. in order to observe specific stress zones. The following conclusions can
In this case, there is also no significant difference between hollow be drawn from the literature review and the results presented in this
spheres of different materials. It can be seen that the stress reduction paper:
effect between hollow spheres oriented in the direction of the load is also
detectable at larger distances. Therefore, this phenomenon is not as 1. This specific application of the substructure technique has proven to
affected by the space-filling percentage as in the previous case. be a tool that, unlike X-ray-based techniques, can be used to easily
build inhomogeneous models of arbitrarily large dimensions. All that
5. Conclusions is needed is a few substructures with different internal structures and
their random assembly on the edges.
The aim of this study is to determine the linear elastic behaviour of 2. The experimental results have verified the numerical approximation
MMSFs under external loading using the substructure technique. This of the pressure diagram of MMSFs using substructure techniques at
special finite element technique has never been used before to model the quasi-linear phase at the two sigma significance level.
composite metal foams. It allows the creation of a model with low 3. From the numerical internal stress analysis, it was found that the
computational and memory requirements, which incorporates the variation of the space-filling has a large effect on the matrix material
properties of the complex internal structure. Since this method is based between the hollow spheres for which the line connecting the centres
of the shells makes an angle of 45◦ with the direction of loading. For
those hollow spheres where this is 0◦ , this effect is significantly
Table 2 smaller.
Amount and elastic properties of ceramic hollow spheres’ components.
Mass Percentage [%] Modulus on elasticity [GPa] Poisson’s ratio The substructure technique has been demonstrated for MMSFs in this
Al2O3 33 38.0 0.22
study, but could be extended to other inhomogeneous anisotropic ma-
Mullit 19 12.7 0.24 terials in the following studies. A further aim will be to extend the
SiO2 48 7.3 0.17 substructure technique to the characterisation of non-linear behaviour
7
M. Kovács et al. Composite Structures 353 (2025) 118731
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