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GC Column Installation Quick Reference

The Agilent GC Support Quick Reference Guide provides detailed procedures for installing gas chromatography (GC) columns in various inlets and detectors. It includes specific instructions for Split/Splitless, Purged Packed, Multimode, Cool On Column, PTV, and Volatiles Interface inlets, as well as FID/NPD, TCD, and uECD detectors. Each section outlines necessary components, measurements, and tightening techniques to ensure proper installation and functionality.

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GC Column Installation Quick Reference

The Agilent GC Support Quick Reference Guide provides detailed procedures for installing gas chromatography (GC) columns in various inlets and detectors. It includes specific instructions for Split/Splitless, Purged Packed, Multimode, Cool On Column, PTV, and Volatiles Interface inlets, as well as FID/NPD, TCD, and uECD detectors. Each section outlines necessary components, measurements, and tightening techniques to ensure proper installation and functionality.

Uploaded by

development51
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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Agilent GC Support - Quick Reference Guide

GC Column Installation Quick Reference Guide - Inlets


Inlet Diagram Procedure
Place a septum over the column, then the
column nut and ferrule. Trim the end of the
column with a column cutter.
Split/Splitless Pull the column back so that 4-6 mm of column is
extending past the end of the ferrule.
Thread the column nut and column into the inlet
and tighten slightly past where the column grabs
– retighten after heating.

Place a septum over the column, then the


column nut and ferrule. Trim the end of the
column with a column cutter.
Purged Packed Pull the column back so that 1-2 mm of column is
extending past the end of the ferrule.
Thread the column nut and column into the inlet
and tighten slightly past where the column grabs
– retighten after heating.

Multimode

NOTE: Make sure the column adapter nut on


the inlet base is fully threaded on and
spinning freely.

Tighten with two wrenches - ¼” and 5/16”


Failure to use two wrenches can damage the
inlet.
Cool Insert the column all the way into the inlet until
On Column you feel the spring tension – do not withdraw.
The column cut is critical.
Tighten with two wrenches - ¼” and 5/16”
Failure to use two wrenches can damage the
inlet.
There should be 17mm of column above the
graphpak ferrule – the graphpak ferrule should
PTV be installed with the graphite end towards the
inlet base. The column nut is slotted. Use a 5
mm wrench to tighten the fitting.

There is a longer column nut for the VI so that


you don’t have to remove the inlet block.
Volatiles
Interface Part Number - G3504-20504

06 April 2010 Page 1 of 2


Agilent GC Support - Quick Reference Guide
GC Column Installation Quick Reference Guide - Detectors
Detector Diagram Procedure
Place a septum over the column, then the
column nut and ferrule. Trim the end of the
column with a column cutter.
FID/NPD Thread the column nut and column into the
detector base. Insert the column all the way
into the detector jet until it stops, then
withdraw 1-2 mm before tightening the nut.
The dimensions shown of 48 and 68 mm
are provided for very narrow columns
(<100um) which may go all the way through
the jet.

Place a 1/8” Swagelok nut and the Back


and Front ferrules over the column. (Be
TCD – sure to select the front ferrule size to match
Using the the column) Trim the end of the column with
standard a column cutter.
Low
Thread the column nut and column into the
Leakage detector base. Insert the column all the way
Ferrules into the detector jet until it stops, then
withdraw 1-2 mm before tightening the nut.
Re-tighten after heating.
Install the column adapter to the 1/8”
Swagelok TCD base using a
TCD – graphite/vespel ferrule.
Original
Design Thread the column nut and column into the
adapter. Insert the column all the way into
Column
the detector jet until it stops, then withdraw
Adapter 1-2 mm before tightening the nut. Re-
tighten after heating.
Thread the column nut and column into the
make-up gas adapter. Insert the column all
the way into the detector jet until it stops,
uECD then withdraw 1-2 mm before tightening the
nut. Re-tighten after heating.
The dimension shown is provided for very
narrow columns (<100um) which may go all
the way through the mixing liner.
Install the column into the Column
Measuring Tool Provided. Trim the column
such that 1 mm extends from the end of the
FPD tool. Tighten the column nut and mark the
position of the column at the back of the
nut. Install into the detector base.

06 April 2010 Page 2 of 2

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