GC

35

GC

GC

GC (GC Inlet Resource Guide)

( 5988-3466)

24 GC

GC/MS (Maintaining Your GC/MS System)

( 5988-3960)

48 GC/MS

GC/MS

GC GC/MS

www.agilent.com/chem
www.agilent.com/chem

GC

GC GC/MS
LC
• GC/MS (Maintaining Your
GC/MS System) ( 5988-3960)
• GC ( GC Inlet Resource Guide)
( 5988-3466)
• HPLC (Maintaining Your HPLC
System) ( 5988-4269)

© 2002
2002 4 15
5988-5847CHCN
 PerfectFit

Agilent GC
 GC
35 GC

GC

Agilent GC

3 37
4 38
POST ER ENCL 5 38
O UT OS 5 38
L-
ED
L

13 39
PU

43
oting
14
44
C
G blesho 15
(TCD)

Trou Guide
16
45
19 (NPD)
48
20 (ECD)
50
26 (FPD)
28 52
31 (FID)
34
55
56
36

www.agilent.com/chem/supplies GC ( )
GC ( )

2 www.agilent.com/chem
 GAS MANAGEMENT

GC

GC

GC
GC

Kenji Yamaguchi

www.agilent.com/chem 3
 GC

(0-1 ppm) 1-1000 ppm 1000 ppm-1% 1%-100%

ECD
Research N/A

= (≤99.998%)
(UHP/Zero Grade) (99.999%)
(Ultra-Pure Grade) (99.9995%)
(Research Grade) (99.9999%)

4 www.agilent.com/chem
 ● ●

(99.995%) (99.9995+%) ●

GC

GC
●

S ● GC
●

● GC

www.agilent.com/chem 5
 :
1=
2=
3=
4=
5=
6=

FID

ECD

ELCD

MS
=

GC

GC

GC

56-58

6 www.agilent.com/chem
 1/4 1/2

150
psi GC

1/8 1/4
(cc) (g) (ppb)

13X 4Å – (Lexan) ( )

200 36 18 MT200-2 MT200-4

MT MSR-1 MSR-1
(1 0.551 )

( )

100 16.3 6 GMT-2-HP GMT-4-HP

GMT 250 GMSR GMSR

S –

S – 5060-9084

750 BMT-2 BMT-4

BMT ( 2 ) BMSR-1 BMSR-1

2002-2003
www.agilent.com/chem (Chromatography & Spectroscopy Supplies Reference Guide) 7
 ( 2000 psi)
15-
20 ppb
100 30 mg

GC

1/8 1/4
(mL)

30 IOT-2-HP IOT-4-HP

750 BOT-2 BOT-4

1/8 1/4
(mL)

200 HT200-2 HT200-4

(1 2 ) ACR ACR

750 BHT-2 BHT-4

( 2 ) BACR BACR

S – GC

S 5060-9096

100 HT3-2 HT3-4

(1 3 ) ACR ACR

8 www.agilent.com/chem
 S

● ●

1/8 1/4
(mL)

OT3 100 OT3-2 OT3-4 Agilent OT3

/ 200 HMT200-2 HMT200-4

/
(1 2 ) HCRMS HCRMS

– CO CO2

–
(
GC/MS) 750 RMSH-2 RMSH-4

– 750 RMSHY-2 RMSHY-4

– 750 RMSN-2 RMSN-4

UMC-5-2 UMC-5-2
2/

2002-2003
www.agilent.com/chem (Chromatography & Spectroscopy Supplies Reference Guide) 9
 ● 8

● ●

18
●

1/8 5183-1907

1/4 5182-9776

— 5182-9780

1/8 5183-4598

1/4 5183-4599

5183-4600

10 www.agilent.com/chem
QC+
QC+

4 RQC-P

QC+ —

( )

4-
1/8 RQC-P

GC-1 GC
GC-2
56-58
GC-2-I

GC-3

GC-4

2002-2003
www.agilent.com/chem (Chromatography & Spectroscopy Supplies Reference Guide) 11
 1/8

GC/MS
ECD NPD 5182-9704

GC

2 5182-0816

5182-9705

4 ( 2
) 5183-4770

500

(1/8 Swagelok ) RDT-1020

(3/ ) RDT-1023
6

2002-2003
12 (Chromatography & Spectroscopy Supplies Reference Guide) www.agilent.com/chem
 GC GC

GC
GC

Spectra-Link

: 2000 sccm (4.2 scfh); : 70˚F; : 30 psig

GC

( ) ( ) (psig)

1/8* 50 2

1/4* 300 0.5

1/8 50 5180-4196

1/8 12 5021-7107

500 psi

www.agilent.com/chem 13
 (Spectra-Link)
●

● 1x10-5 cc/sec

1/8 36
(Spectra-Link) SL-8

1/4 36
SL-4

5183-1941
( 14 in., 35 cm)

GC

12

AC
( 115 V 220 V)

115 V 5182-9646

220 V 5182-9648

14 www.agilent.com/chem
 GC

NIST-

1000 5183-4779

2000
5183-4780

(AC)
( ) 5183-4781

2000

ADM 1000 ADM 2000

● ± 3% ADM 1000 ADM 2000
● —
●
0 45ºC
-70 135ºC
● — NIST ● RS-232
ADM 1000
● ● 9V
(120 220 VAC)
● CE
●

0.5 1000 mL/min

●

ADM 2000

www.agilent.com/chem 15
 (mL/min) RS-232
(%)

ADM – *
ADM1000 0.5 1000 ±3 9V 220-1170

ADM2000 0.5 1000 ±3 120 VAC 220-1171-U

ADM2000E 0.5 1000 ±3 220 VAC 220-1171-E

– *
Veri-Flow 500 He, H2, Ar/CH4
(110 V) 5.0 500 N2, ±3 110 VAC HVF-500

Veri-Flow 500 He, H2, Ar/CH4

(220 V) 5.0 500 N2, ±3 220 VAC HVF-500-2

(Optiflow) – **
Optiflow 420 0.1 50 +/- 3 9V HFM-420

Optiflow 570 0.5 700 +/- 3 9V HFM-570

Optiflow 650 5.0 5,000 +/- 2 9V HFM-650

*
**

Veri-Flow 500
Optiflow 420

GC

56-58

2002-2003
16 (Chromatography & Spectroscopy Supplies Reference Guide) www.agilent.com/chem
 GC

PerfectFit

Bryan Bente,

2002-2003
www.agilent.com/chem (Chromatography & Spectroscopy Supplies Reference Guide) 17
 GC
●

500

— — — — — —

1 mL 50 µL

3.6 mm*
100 µL
*

18 www.agilent.com/chem
●

●
●
●

●
●

● ● 24
●

● MS ECD 2 mL
●
500/ 5181-3400
●

●
2 mL
500/ 5182-0732
●

2 mL
Viton
● 500/ 5182-0547
●
100 µL 100/ 5181-1270
●

● 32 300 µL 1000/ 9301-0978

100 µL 100/ 9301-0977

15 µL
100/ 5184-3551

30 µL
100/ 5182-3454

www.agilent.com/chem 19
 1.

2.

● 3.
●

( PTV) 23 23/26

23/26 26 530 µm

26/32 320 µm

26/32 250 µm

GC

56-58

20 www.agilent.com/chem
 5 µL, • 1µL • • 1 µL
•
• 0.5 µL • •

10 µL, • • 2 µL •
• •
• •
•
•

10 µL, • • •
•
• • 5 µL •

250 µm 320 µm 1.

2.

3.
4.
5.

www.agilent.com/chem/supplies,
Reference Library ( )
“How-to Video ”
www.agilent.com/chem 21
● ● ●

10
●

● 5-8 10-25%

● 5

● 26 0.53mm

0.32mm 0.25mm

22 www.agilent.com/chem
 ( 0.53 mm )

10 µL 23-26s/42 6/ 5181-3360

5 µL 23-26s/42 6/ 5181-8810

( Merlin )

10 µL 23/42 6/ 9301-0725

5 µL 23/42 6/ 5182-0875

4 mL 144/ 9301-0723

4 mL 12/ 07673-40180

4 mL 144/ 9301-1031

4 mL 25/ 5182-0551

07673-20570

(4 ) 18596-40015

7673
10 mL (6/ ), 23/26
4 mL
(144/ ), 2 mL
(1,000/ ),
GC (25/ ), (5/ ) 07673-60840

Agilent 2002-2003
www.agilent.com/chem (Chromatography & Spectroscopy Supplies Reference Guide) 23
 +50˚C

1/8-
1/4-
1/4-

( )

1/8-
1/4-

20-40 mL/min N2
30-60 mL/min He H2

24 www.agilent.com/chem
6890/6850/5890 GC *

1
1 18740-60835 2
3
2 4
11 mm** 50/ 5183-4757

3 19243-80570

4 Viton O 12/ 5080-8898

5 25/ 5080-8732

5/ 5181-3382

6 Vespel/ 1/4 10/ 5080-8774

7 1/4 10/ 5180-4105

Liner

8 0.53 mm 19244-80540

1/8 19243-80530
5

1/4 19243-80540
6
9 ‡ 19243-00067 7

10 19234-60720 8 1/4in.in.Vespel/
1/4 Vespel/
graphite ferrule

11 0.53 mm 2/ 5181-8830 Inside of 1/4in.in.nutnut

1/4
Oven
1/8in.in.oror
1/8 1/41/4
in. in
** 6890 GC 9 stainless steel liner
*‡ 6890/6850 10
** Agilent’s GC
(GC Inlet Resource Guide)
11

5890

EPC 19243-60570

1/8 19243-80510

1/4 19243-80520

( ) GC

19243-60505
56-58
1/4 in. 10/ 5180-4105

www.agilent.com/chem 25
 GC

50˚C

0.5-3 µL
0.10-10 mL

50:1 500:1

2-3 mL/min

www.agilent.com/chem/supplies,
Reference Library ( )
“How-to Video ”
26 www.agilent.com/chem
 ( 20˚C)

>0.8 mL
<0.2 mL

0.5-2 µL 10˚C

>1µL
1-2µL
<1µL

20-50 mL/min

20-80 sec

10-25˚C

>2 mL/min

2-3 mL/min

1-3 m,
( µL 1-2 m )

GC

56-58

www.agilent.com/chem 27
●

( 41 )
6890/6850/5890 *

1 18740-60835

2 **

3 **

4 O **

5 **

6 ( 6890/6850 ) G1544-80550
G1544-80530

7 ( 6890/6850 ) G1544-20590
( 5890 ) 19251-20620

8 18740-20880
18740-20885

9 0.375 12/ 5061-5869

10 18740-20800

11 ( 3 ) 19243-00067

12 19243-00070

13 **

14 ( 6890/5890 ) 2/ 5181-8830

( 6850 ) 2/ 5183-4732

19251-00100

** 6890/6850/5890 GC
** Agilent’s GC (GC Inlet Resource Guide)

28 www.agilent.com/chem
 ● (0.5 µL 2.0 µL)

● ●

●
●

●
●

●
3˚C
●

0.1-2.0 µL

50-80 cm/sec H2
30-50 cm/sec He
12-15 mL/min

1-3 m,

www.agilent.com/chem/supplies,
Reference Library ( )
“How-to Video ”
www.agilent.com/chem 29
 0.5m

2/ 5181-8830

250 µm /Vespel 10/ 5181-3323

320 µm 0.5 mm /Vespel 10/ 5062-3514

250 µm (5m ) 160-2255-5

320 µm (5m ) 160-2325-5

530 µm (5m ) 160-2535-5

0.18-0.53 mm 5/ 5181-3396

GC

56-58

30 www.agilent.com/chem
6890/5890

1a
1b 1c
1d

1c 19320-80625

1d 10/ 19245-40050
2
6/ 19091-63000 3
4

10 µL 9301-0658

3 19245-60760

4
200 µm ( ) 19245-20510

250 µm ( ) 19245-20515

320 µm ( ) 19245-20525

530 µm ( ) 19245-20580
5
530 µm ( ) 19245-20780
6
5 5080-8853

6 2/ 5181-8830

6890 GC

1a 320 mm 19245-80521

1b 530 mm G1545-80520

2 5 mm 50/ 5183-4760
BTO 5 mm 50/ 5183-4758

5890 GC

1a (5890 II GC) 19245-80520

1b ( 7673A ) 19245-20670

* 6890/5890 GC

Agilent 2002-2003
www.agilent.com/chem (Chromatography & Spectroscopy Supplies Reference Guide) 31
 (PTV)
PTV PTV

PTV
( 2˚C/sec
12˚C/sec)
●

PTV
Peltier ( N2,
0.1-1.5 µL
CO2).

PTV 1.5 µL

PTV
10-25˚C

30-50 cm/sec

1-5 mL/min

1-3 m,

PYV
www.agilent.com/chem/supplies,
Reference Library ( )
“How-to Video ”
32 www.agilent.com/chem
6890 PTV

1
3
1 G2617-60507 2
2 G2618-80500
3 18740-60835
4 PTV G2617-60506
5 PTV CO2 G2617-60508
G2619-60501 4
6 PTV N2
7 5/ 5182-9763
8 Graphpak 0.20 mm 5182-9754
0.25-0.33 mm 5182-9761
0.53 mm 5182-9762
5, 6
9 Graphpak 0.20 mm 10/ 5182-9756
0.25 mm 10/ 5182-9768 7
8
0.32 mm 10/ 5182-9769 9
10
0.53 mm 10/ 5182-9770
10 5062-3525
11 PTV G2617-20510
11
PTV ( ) G2617-60510
( ) 5182-9748
Kalrez 5182-9759
5182-9757
5182-9758
Viton 5182-9775
5182-9760 PTV
CO2 3150-0602 PTV
5182-9747 PTV
Kalrez
Graphpak 3D
5/ 5182-9749
3D G2617-80540

PTV

PTV 2 mm 180 µL 5183-2038

PTV 2 mm 200 µL 5183-2036
PTV 1.5 mm 150 µL 5183-2037
PTV 1.5 mm 150 µL 5183-2041

www.agilent.com/chem 33
 PTV

4 mm
(≥ 2 µL)
(≤ 0.5 µL)

GC
GC/MS
5183-4647 (
) 8270 EPA

6890/5973 GC/MSD

5181-3316

EPC O
5183-4647 O
O

5183-4711 350 ºC

5181-8818 (
)

34 www.agilent.com/chem
 5/ 25/
(µl)

870 5183-4647 5183-4701 5183-4702

990 19251-60540 5183-4691 5183-4692

800 18740-80190 5183-4699 5183-4700

800 18740-60840 5183-4697 5183-4698

[
(EPC)]

870 5183-4711 5183-4712 5183-4713

900 5062-3587 5183-4693 5183-4694

800 5181-3315 5183-4705 5183-4706

900 5181-3316 5183-4695 5183-4696

250 5181-8818 5183-4703 5183-4704

2 mm (

)
250 18740-80220 5183-4707 5183-4708
2 mm
140 18740-80200 5183-4709 5183-4710
1.5 mm
[
]
990 210-3003 210-3003-5
4 mm

4 mm , G1544-80730
4 mm , G1544-80700

, 4 mm, 210-4004-5
, 4mm, 210-4022-5
O
O (12/ ) 5180-4182
O (10/ ) 5180-4173
O (10/ ) 5180-4168

www.agilent.com/chem 35
 ●

1/4
●
●
●
●
● ●
●
●
●
●
●

● ●
●

● ●

●
GC
●
(Agilent’s GC Inlet
Resource Guide).
( 5988-3466)

36 www.agilent.com/chem
 GC
GC

GC
GC

GC

Eberhardt Kuhn,

www.agilent.com/chem 37
GC

DB-1ms, 0.25mm i.d., 30m, 0.25µm 122-0132

●

HP-5ms, 0.25mm i.d., 30m, 0.25µm 19091S-433

●

DB-XLB, 0.25mm i.d., 30m, 0.25µm 122-1232

●
DB-35ms, 0.25mm i.d., 30m, 0.25µm 122-3832

HP-INNOWax, 0.25mm i.d.,

30m, 0.25µm 19091N-133
●

● GC

● ●

● ●

GC ●

56-58

38 www.agilent.com/chem
 (4/ ) 5181-8836

20 430-1020

(0.5mm
≤ 0.32mm ) 10/ 5080-8853

(1.0mm
0.45-0.53mm ) 10/ 5080-8773

115V 5182-9646
220V ( ) 5182-9648

GC

● (5/ ) 705-0905

( 0.45-0.53mm) (5/ ) 5181-3396

●

6 (5 ) 500-1200

2-3

Agilent 2002-2003
www.agilent.com/chem (Chromatography & Spectroscopy Supplies Reference Guide) 39
 ●
GC
–
–
–
●
–
–
–
–
5-10
● GC

● 8-16

● 10-15
●

2000 5183-4780

(750 cc, 1/8” ) BOT-2

(750 cc, 1/8” ) BMT-2

( )
(750cc, 1/8” ) RMSH-2

(11 mm, 50/ ) 5183-4759

40 www.agilent.com/chem
 ●

● 1-10 5-10
( 1%
)
●

DuraGuard

● 0.5 1
● 5

GC

INJECTOR DETECTOR

Column
Guard Column

Union

www.agilent.com/chem “Consumer Products.”

Agilent 2002-2003
www.agilent.com/chem (Chromatography & Spectroscopy Supplies Reference Guide) 41
 (SPE) 5988-2685EN/CHCN

(5/ ) 5183-4712
(-OH) (-NH)
(-SH)
(5/ ) 5183-4695

(5/ ) 5181-3396
●

(5 ) 500-1200
●

10m, 0.53mm 160-2535-10

●

● 10m, 0.25mm 160-2255-10

– 430-3000

–
– 0.5 1
●

GC
●
● GC GC

2-4
●

GC
● 1-2

42 www.agilent.com/chem
 GC
GC

FID TCD NPD ECD FPD

GC

Bernhard Rothweiler

Only a small sampling of FID supplies are shown here. For a complete selection of FID supplies,
www.agilent.com/chem see the Agilent 2002-2003 Chromatography & Spectroscopy Supplies Reference Guide. 43
 (TCD)
TCD

1.
10-15

TCD
2.

TCD

6890/6850/5890 TCD

TCD ( 6890/6850) G1532-60675

TCD 10/ 18740-20950

TCD 18740-20960

1.0 mm 10/ 5080-8773

0.5 mm 10/ 5080-8853

6890 2/ 5181-8830

6850 2/ 5183-4732

TCD ( 6890/6850) G1532-20710

TCD 3
0.5 mL, 0.3% C14 C15 C16,
18711-60060

5890 TCD

TCD 19232-80550

TCD 1/8 1/4 19302-80020

TCD 19232-60676

44 www.agilent.com/chem
 5.
10
1.
20-30˚C
2.
6. 30
3.

4. 20-100 µL
1
TCD

(NPD)

● NPD
NPD
100˚C 30
NPD ● 150˚C 30
●

6
●

● (320 – 335˚C)
●

NPD

www.agilent.com/chem 45
 NPD

( 53
NPD FID )

NPD

NPD
(99.999% )

2-3
C

NPD FID

NPD

(mm)

(0.011 ./0.29 mm )
( 6890 ) 48 G1531-80560

6890/5890

0.53 mm (0.011 in. ) 61.5 19244-80560

(0.018 in. ) 63.5 18710-20119

46 www.agilent.com/chem
 (NPD)

6890 NPD

1 , M3 x 0.5 x 8 mm (Pozidriv) 0515-0655

2 NPD * G1534-60570
2
1
NPD ** 5183-2007

3 G1534-80510 3

4 C 0905-2580
9
5 G1534-40020 11
10
4 12
6 G1534-20530
5
6
7 G1534-40030

8 C 0905-1284 8 7

9 M4 x 10 mm 0515-2495

10 J- 1400-0015

11 M4 x 10 mm 0515-2495

12 NPD G1534-60610 13
14
13 G1531-40020

14 ( 54 )

G1534-80500 15
15 NPD
16

NPD G1534-80540

16 G1534-20590 17

NPD
4, 5, 7 8 5182-9722
18

17 NPD

18 19234-60720

5890 NPD

NPD (NPD ) 19234-60540

10 5080-8872

19231-60790

**

NPD Agilent 2002-2003

www.agilent.com/chem (Chromatography & Spectroscopy Supplies Reference Guide) 47
 (ECD)

(ECD) (µ-ECD) (
10 )
— ECD µ-ECD

GC

(99.9995%)
63Ni ß x-

ECD

48 www.agilent.com/chem
 (ECD)

6890 ECD

ECD * G1533-80565

19234-60720 1

2
5890 ECD

1 Vespel 1/4 10/ 5080-8774 3

Vespel/ 85%/15%
1/4 10/ 0100-1331
ECD 1/4
2 1/4 10/ 5180-4105

3 ECD 1/4 1/8 19301-80530

7
4 ECD G2397-80520
6
5 ECD 19233-80565

6890/5890 ECD 5, 4

6 ECD ( ) 19233-20625

ECD ECD G2397-20540 ECD

7 ECD 19233-20755
( ECD)

ECD
(0.033 ppm) 3 0.5 mL 18713-60040

ECD 18713-60050

* 19233-20625 19233-20755

GC

56-58

www.agilent.com/chem 49
 (FPD)
● ●

PMT
PMT PMT ●

65500
GC
5A
PMT ●

●
FPD

( FPD ●

53 FID )

53
FPD

(PMT) FPD
PMT ●

●
GC

50 www.agilent.com/chem
6890/5890 FPD

1 19256-60700
1
2 1/4 10/ 5180-4105 2
3
4 19256-80560 4
9
5 O Kalrez 0905-1102 5 10
6
7 11
6 19256-20590
12
7 0854-0141 8 13
14
8 ( 6890) G1535-60600 15

9 19256-80040
16
10 19256-80030 17
18

11 19256-20580 19

12 19256-20550 20

21
14 M3 x 12 ( 4 ) 0515-0911
15 19256-00090
16 O 12/ 5061-5886
17 19256-80060
18 O 12/ 5061-5891
19 19256-20510
20 19256-00200
21 O Viton, 1.239 12/ 5061-5890
1/8 19256-80590
19256-80570
( 5890) 19256-60500
FPD O ( 5890) 12/ 5061-5867
19256-60590 393 nm
19256-80000 525 nm

19256-80010
Kalrez O 2-002 0905-1101
Kalrez O 2-011 0905-1103
O
0.926 12/ 5061-5889
FPD 20 ng/mL (20 ppm)

3 19305-60580

www.agilent.com/chem 51
 (FID)

FID
100˚C

FID

FID
FID

FID

FID

52 www.agilent.com/chem
 (FID)

( FID 9301-0985)
6890/6850
1.
G1531-20700
G1531-20690
FID * G1531-60690
G1531-20700
2. FID G1531-60680
5
G1531-20740
3.
5890
4. 5
* 19231-60690
19231-20970
19231-20960
5.
19231-21080
GC
19231-20950
6.
6890/6850/5890
PTFE ( ) 19231-21050
19231-20940
10/ 5181-3311
19231-20910
19231-21060
19231-60680
FID 2/ 8710-1346
FID
(5880, 5890, 6890) 19301-00150
FID 1/4 8710-1561
FID 19301-60660
O 12/ 5080-4978
FID
0.03% C14, C15 C16
18710-60170
0.03 5/ 5180-4150
530 mm
0.018 5/ 5180-4152
FID 9301-0985
*

FID Agilent 2002-2003

www.agilent.com/chem (Chromatography & Spectroscopy Supplies Reference Guide) 53
FID

(mm)

FID ( 6890)
(0.011 ./0.29 mm ) 48 G1531-80560

( 0.018 ) 48 G1531-80620

FID (6890/6850/5890)

0.53 mm (0.011 ) 61.5 19244-80560 FID

(0.018 ) 63.5 18710-20119

(0.030 ) 63.5 18789-80070

0.53 mm (0.018 ) 61.5 19244-80620

FID
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ISO
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“Education ( )” GC
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“Education ( )”
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● H5308A (6890 GC)

● H4001A (5890 GC)

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● PerfectFit

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GC

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