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Volumetric Analysis

The document outlines a series of experiments focused on determining the molarity and strength of potassium permanganate and ammonium sulfate solutions. It details the apparatus and chemicals required, as well as the procedures for conducting the experiments and calculating results. Observations and calculations for molarity and strength are also included, demonstrating the chemical reactions involved.

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vijay292085
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4 views9 pages

Volumetric Analysis

The document outlines a series of experiments focused on determining the molarity and strength of potassium permanganate and ammonium sulfate solutions. It details the apparatus and chemicals required, as well as the procedures for conducting the experiments and calculating results. Observations and calculations for molarity and strength are also included, demonstrating the chemical reactions involved.

Uploaded by

vijay292085
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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Page Nio

EtN

AVA:SS
Shont Poadune

)BuneRt e solut en Po tasiwn Perarng anate


soletfOn

&) Ppette solui n a0 m e fon 9us Aneru um


Sulphate soub'on
3) Meot um (aiolic) I testtule 6ul H2 SO,
4) Ternpvatwre Roorn tepeatue
5) Inol
Tno¯ cator se Potastm Pen arg anate
(sely)
6) Enol point Appeau un ce Puman ent
Pale P t colowt
1) Mola maus ) LFASJ 392 9 pr mel
1580 peH
Amgunt o, FAS Requi ned Aolai
t x Molay mas xi
Nolasu ty -O0 25M
40
: -025 x 392 XOQ 0.48q
LO00
Expt. No. Page No.
/24
Date 29 /6

Estinatien otausiwn Rrmanyanate


Sout'e
Cusing &tandad fevows Ammoniwm susph ade bouti'orn)

J0 oleteknine the molauity and sthingth


potausiuwnt peumarnganate solution suing Zho M.
Standad foeus Amoniun slphate solut'er

Ionic eo/uati on
MnO,t 8H + 5 e ’ Mn +4H20
5 fe ’ 5fe+5e

+ 8 H ’ Mnt 5 fe

Appaxatus Rsqyireod :
Buxette Pipete, Buette &tanol, corieol
flast, fwnel, panelain tile test tule and
standad flash
chemi cas Reguined :
tonHGus Ammorm Bsphate cys tale,
pptasian pekrnanqu t e solution, aelute
&ulphute aid and olistilol wateL

AA standlano solutienq fe4us anmonin


Autphene ppocl by
obsewati'on
Standand frs Vs KMnO
volume o% Bwet Readeng (m) voune % Conlovdant
no FAS Cm) ntttal tinal KMnOuCm) vaue (ma)
) 133 13-3

13-3. 13-3 13-d

3) Ro 13:2 13-2

Molan'ty caleat'on :
M
kMn O4 xVKMnO4
n fAS

Nolaity nKMn OyI


KMn O,
VOluune kMn O% 13 m

Mo lau fAS O-0 25 M n FA s = 5

Voluwme & FAS 20m


M KMnOy
nFAS
VKMnOy
= O"025 x 20x) o-o015 M
5x13:

Strangth KMnOn - Aolaity O}


kMnOy KMnoy
s O:0015 x i58
Expt No
Page NoS
Date :

stanoard ask htla phupaúog the kolution

butedte stand

Jhe pipette i washeslwh aate and than


hinacd with stanolas etHOLUA arEncniLun kulphate
Hhe
But ntD_a claan corica glask: A testbule fall
added to i

he Lontints h the Lonials flask aa tithratil


a0atost thhe potaKsiea plunagacate solutiorn takan ia

aptote to que contorolat titae Vale sia thls


Value the nolasi byand stuagth patausiuexg

Resut
)Aolaiky O potassiuen puonlg aaate 0:00 75 M
soutiern
: 1)65 9li
4oliutio4
DBAutte bouution Potosturn Ponag orat
Boution
2 Pipute s0lut'en
AOml
3) Medw (Aoic) test tue full o,
4) Tempatuwte 6o to toC
5) IndiatoY Aseod
Potas turn Pmogorate Csy )
Appeoan e O pornan ent pale
Pink colowe
Oxalic 1269 mol'
8 Molat mas 1589 mol!

Ameunt e Oxaléc a°cl eoyirol - Molatty xMo lar may


X100
Molosi tu L :O+05 M

= 0-639
l000

Obsewa'on
KMn O Vs Atanda oxale Aud
Sno Bunette Reocling volune % Con cor dant
ittal Binal KNnO Cme) valelm)
Page No

ktlnmacen g Atascan Pemoganate Soutir.


Caaing standand oraic acid soluti on)

Jo oletenne the atkeeg th the gien. potatstur

Tonic

2+

5Ca O, 0CO2 t_5e

9 M n R C +|0C2

App D4ats Regpu'hed


Bauette, picette Batte stanol Loni cal flack
Auntl porein tile, testtule anol CaxilStanolad

uystala, olite kilphic aol arol olistlled


wwater

Proeui
A stanodano solution & ccale'c aeiol

pto 00ml ina Atandat


Oy
MKNnOy Vnin Oy - Mc2H20Oh xVCzHa
nKMnO

Nolaxity
: O+05M
Molvd ty
Volume C2HaOt

naH2 O, 5

M Ot

-O05x 20x2 001201M

Moloityby 9% Molot mawb

0O1801

8466
Expt No. Page No.
Date

Jhe buHette washl othJntEA_ad tod

ano claopeol in he bututte stad


Jhe pipette As washesl wotth wntA and inseol t

soldienii pipeted out iato lean cetlal lakk

The centents , he conilal lask i heateol to beate


Lable wkumth anol tityd aactnst patasiun
pmagarate solution taken in the buLtte J a t

oloLt JitYat'sns
cenlakdad Value aro taluela teol uatoa tha lonlorolant

pmoqaule kaluetion ioo be

Resue :

M
pliaganaie
soluutie

oluti oa

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