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R059-1-e16

The OIML R 59-1 Recommendation outlines the metrological and technical requirements for moisture meters used in the measurement of cereal grains and oilseeds, emphasizing the importance of accurate moisture content for economic transactions. It details the scope, terminology, measurement units, and specific requirements for instrument performance, including calibration and permissible errors. This 2016 edition updates the previous 1984 version to incorporate new technologies and improved measurement practices.

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0% found this document useful (0 votes)
6 views36 pages

R059-1-e16

The OIML R 59-1 Recommendation outlines the metrological and technical requirements for moisture meters used in the measurement of cereal grains and oilseeds, emphasizing the importance of accurate moisture content for economic transactions. It details the scope, terminology, measurement units, and specific requirements for instrument performance, including calibration and permissible errors. This 2016 edition updates the previous 1984 version to incorporate new technologies and improved measurement practices.

Uploaded by

Mark Smith
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
You are on page 1/ 36

INTERNATIONAL OIML R 59-1

RECOMMENDATION Edition 2016 (E)

Moisture meters for cereal grains and oilseeds.

Part 1: Metrological and technical requirements

Humidimètres pour grains de céréales et graines oléagineuses.

Partie 1: Exigences métrologiques et techniques


OIML R 59-1 Edition 2016 (E)

ORGANISATION INTERNATIONALE
DE MÉTROLOGIE LÉGALE

INTERNATIONAL ORGANIZATION
OF LEGAL METROLOGY
OIML R 59-1:2016 (E)

Contents
Foreword ................................................................................................................................................. 5
Introduction ............................................................................................................................................. 6
1 Scope .................................................................................................................................................. 7
1.1 Requirements and test ............................................................................................................... 7
1.2 Indications ................................................................................................................................ 7
1.3 Application ............................................................................................................................... 7
1.4 Type of measuring instrument .................................................................................................. 7
1.5 New technology ........................................................................................................................ 7
2 Terminology ....................................................................................................................................... 7
2.1 International Vocabulary Metrology (VIM) ............................................................................. 7
2.2 International Organization of Legal Metrology(OIML) Terminology ................................... 10
2.3 Other terminology................................................................................................................... 11
2.4 Abbreviations and acronyms .................................................................................................. 13
2.5 Additional symbols and subscripts used in equations ............................................................ 13
3 Units of measurement ....................................................................................................................... 14
3.1 Moisture content ..................................................................................................................... 14
4 Metrological requirements................................................................................................................ 14
4.1 Influence quantities................................................................................................................. 14
4.2 Rated operating conditions ..................................................................................................... 15
4.3 Reference method ................................................................................................................... 15
4.4 Maximum permissible errors (MPEs) .................................................................................... 16
4.5 Accuracy and precision requirements ..................................................................................... 17
4.6 Instrument environmental operating temperature range ......................................................... 17
4.7 Sample temperature range ...................................................................................................... 17
5 Technical requirements .................................................................................................................... 17
5.1 Grains and minimum moisture ranges .................................................................................... 17
5.2 Selection of grain on the instrument ....................................................................................... 17
5.3 Minimum sample size ............................................................................................................. 18
5.4 Determination of quantity and temperature ............................................................................ 18
5.5 Instrument warm-up period .................................................................................................... 18
5.6 Digital display and recording elements .................................................................................. 18
5.7 Data storage ............................................................................................................................ 18
5.8 External data storage .............................................................................................................. 19
5.9 Meter construction .................................................................................................................. 19
5.10 Marking .................................................................................................................................. 19
5.11 Ambient temperature operating ranges ................................................................................... 20
5.12 Provision for sealing and calibration security......................................................................... 20
5.13 Manufacturer’s manual ........................................................................................................... 20
5.14 Visibility of the moisture meter and of the measurement operations ..................................... 21
5.15 Power supply .......................................................................................................................... 21
5.16 Battery-operated instruments .................................................................................................. 21
5.17 Level indicating means ........................................................................................................... 22
5.18 Software-controlled electronic devices and security .............................................................. 22
6 Bibliography ..................................................................................................................................... 25
Annex A Principles for sealing (Informative) ....................................................................................... 30

3
OIML R 59-1:2016 (E)

Foreword
The International Organization of Legal Metrology (OIML) is a worldwide, intergovernmental
organization whose primary aim is to harmonize the regulations and metrological controls applied by
the national metrological services, or related organizations, of its Member States.
The main categories of OIML publications are:
• International Recommendations (OIML R), which are model regulations that establish the
metrological characteristics required of certain measuring instruments and which specify
methods and equipment for checking their conformity. OIML Member States shall implement
these Recommendations to the greatest possible extent;
• International Documents (OIML D), which are informative in nature and which are
intended to harmonize and improve work in the field of legal metrology;
• International Guides (OIML G), which are also informative in nature and which are
intended to give guidelines for the application of certain requirements to legal metrology; and
• International Basic Publications (OIML B), which define the operating rules of the various
OIML structures and systems.
OIML Draft Recommendations, Documents and Guides are developed by Project Groups linked to
Technical Committees or Subcommittees which comprise representatives from the Member States.
Certain international and regional institutions also participate on a consultation basis. Cooperative
agreements have been established between the OIML and certain institutions, such as ISO and the
IEC, with the objective of avoiding contradictory requirements. Consequently, manufacturers and
users of measuring instruments, test laboratories, etc. may simultaneously apply OIML publications
and those of other institutions.
International Recommendations, Documents, Guides and Basic Publications are published in English
(E) and translated into French (F) and are subject to periodic revision.
Additionally, the OIML publishes or participates in the publication of Vocabularies (OIML V) and
periodically commissions legal metrology experts to write Expert Reports (OIML E). Expert
Reports are intended to provide information and advice, and are written solely from the viewpoint of
their author, without the involvement of a Technical Committee or Subcommittee, nor that of the
CIML. Thus, they do not necessarily represent the views of the OIML.
This publication – reference OIML R 59-1, Edition 2016 – was developed by Project Group 1 in
OIML Technical Subcommittee TC 17/SC 1 Humidity. It was approved for final publication by the
International Committee of Legal Metrology in 2016 and was submitted to the International
Conference on Legal Metrology in 2016 for formal sanction. It supersedes the previous edition of R 59
dated 1984.
OIML Publications may be downloaded from the OIML website in the form of PDF files. Additional
information on OIML Publications may be obtained from the Organization’s headquarters:
Bureau International de Métrologie Légale
11, rue Turgot - 75009 Paris – France
Telephone: 33 (0)1 48 78 12 82
Fax: 33 (0)1 42 82 17 27
E-mail: [email protected]
Internet: www.oiml.org

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OIML R 59-1:2016 (E)

Introduction
1
Moisture content is one of the most critical grain quality measurements because of the direct
economic significance of the fraction of the total product weight that is water and because moisture
content largely determines the rates at which the grain will degrade during handling and storage. Grain
is bought and sold on the basis of weight. Accurate moisture determinations serve as the basis for
appropriate price adjustments.
1
If the moisture content is above the level that ensures safe storage, the grain must be dried to a
suitable level. The energy and handling costs associated with drying grain and the reduction in weight
of the grain during drying result in substantially reduced prices for high moisture grain.
Concomitantly, overly dry grain is discounted from its weight basis and this dockage is partially
justified by the increased susceptibility to breakage during handling for drier grain. The direct
discounts assessed for moist grain and the indirect penalty (giving away dry matter) for dry grain are
powerful inducements to deliver grain with a moisture content that is very close to the established safe
storage level. Because of its significance, moisture content is determined virtually every time grain is
bought and sold.
1
Many technologies have been applied to rapid grain moisture measurement. Rapid indirect methods
measure some physical parameter (such as electrical or optical sensing) and predict moisture content
using calibration equations or charts. These calibrations can change due to changes in crop varieties
planted and seasonal variation in climatic conditions. Invariably, other sample constituents or sample
geometry interfere with the signal caused by water. Temperature usually affects both the water signal
and the interfering signals. Therefore, calibration equations attempt to achieve a best fit between the
measured parameters and the moisture content as defined by an accepted moisture reference method.
Accurate grain moisture measurements depend upon successfully overcoming the effects of interfering
factors such as density, temperature, chemical composition and impurities.
This 2016 edition of OIML R 59 contains significant changes to the 1984 edition, notably to reflect
new measuring technologies and aspects of actual grain analysis.
As noted above, grain moisture meters do not measure moisture directly. An electrical or optical
response to the moisture in a grain type is measured and moisture is predicted using calibration
equations. As such, these instruments must be calibrated to predict the moisture of each grain type
used on the instrument. Grains vary from season to season and also grain types may vary widely from
country to country; therefore, a program to address calibration updates is needed to ensure that grain
moisture meter calibrations represent the current crops. If grain moisture instruments are sold to other
countries the calibrations will need to be verified within that country to ensure that the calibrations are
representative of the grains within that particular country. This Recommendation does not address an
ongoing calibration program for these instruments. Ongoing calibration programs may be subject to
metrological controls by the national responsible body.

1
An Investigation of the Nature of the Radio Frequency Dielectric Response in Cereal Grains and Oilseeds with
Engineering Implications for Grain Moisture Meters, A Dissertation in Physics and Engineering, David B.
Funk, Ph.D., D.H.C.

6
OIML R 59-1:2016 (E)

Moisture meters for cereal grain and oilseeds


Part 1: Metrological and technical requirements

1 Scope

1.1 Requirements and tests


This Recommendation specifies the metrological and technical requirements, test methods and
maximum permissible errors for the type approval of grain moisture meters used in commercial
transactions of cereal grains and oilseeds.

1.2 Indications
This Recommendation applies to digitally indicating automatic grain moisture meters that directly
display moisture content.

1.3 Application
This Recommendation applies to moisture measuring instruments that estimate moisture based on
indirect physical means (e.g. electrical or optical sensing). Drying methods or any other direct
moisture measurement technology are not specifically covered, but may qualify if they perform to the
requirements of this Recommendation.

1.4 Type of measuring instrument


This Recommendation applies to grain moisture meters that measure the moisture content of a fixed
representative-size grain sample. It does not apply to devices used for in-motion measurement of grain
or seed moisture content.

1.5 New technology


This Recommendation specifies instrument performance specifications and is not intended to preclude
the application of new technologies to grain moisture measurement.

2 Terminology

2.1 Terminology in OIML V 2-200 International Vocabulary of Metrology – Basic and General
Concepts and Associated Terms (VIM) [1], and OIML V 1 International Vocabulary of Terms in Legal
Metrology (VIML) [2]

2.1.1 adjustment [VIM 3.11]


set of operations carried out on a measuring system so that it provides prescribed indications
corresponding to given values of a quantity to be measured
Additional note: A change in the value of any of a device’s sealable calibration parameters or sealable
configuration parameters.

2.1.2 accuracy; measurement accuracy [VIM 2.13]


closeness of agreement between a measured quantity value and a true quantity value of the measurand
Note 1: The concept of ‘measurement accuracy’ is not a quantity and is not given a numerical
quantity value. A measurement is said to be more accurate when it offers a smaller
measurement error.

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OIML R 59-1:2016 (E)

Note 2: The term “measurement accuracy” should not be used for measurement trueness and the
term “measurement precision” should not be used for “measurement accuracy”, which,
however, is related to both concepts.
Note 3: ‘Measurement accuracy’ is sometimes understood as closeness of agreement between
measured quantity values that are being attributed to the measurand.

2.1.3 calibration [VIM 2.39]


operation that, under specified conditions, in a first step, establishes a relation between the quantity
values with measurement uncertainties provided by measurement standards and corresponding
indications with associated measurement uncertainties and, in a second step, uses this information to
establish a relation for obtaining a measurement result from an indication
Note 1: A calibration may be expressed by a statement, calibration function, calibration diagram,
calibration curve, or calibration table. In some cases, it may consist of an additive or
multiplicative correction of the indication with associated measurement uncertainty.
Note 2: Calibration should not be confused with adjustment of a measuring system, often mistakenly
called “self-calibration”, nor with verification of calibration.
Note 3: Often, the first step alone in the above definition is perceived as being calibration.

2.1.4 certified reference material; CRM [VIM 5.14]


reference material, accompanied by documentation issued by an authoritative body and providing one
or more specified property values with associated uncertainties and traceabilities, using valid
procedures

2.1.5 maximum permissible measurement error (MPE) (maximum permissible error, limit of
error) [VIM 4.26]
extreme value of measurement error, with respect to a known reference quantity value, permitted by
specifications or regulations for a given measurement, measuring instrument, or measuring system
Note 1: Usually the term “maximum permissible errors” or “limits of error” are used, where there are
two extreme values.
Note 2: The term “tolerance” should not be used to designate “maximum permissible error”.
Additional note: The MPEs in 4.4.2 of this Recommendation are errors associated with a meter in use
in the market place. The errors for the OIML test procedures are based on 4.4.1.

2.1.6 measurement error (error of measurement, error) [VIM 2.16]


measured quantity value minus a reference quantity value
Note 1: The concept of ‘measurement error’ can be used both
(a) when there is a single reference quantity value to refer to, which occurs if a calibration is
made by means of a measurement standard with a measured quantity value having a
negligible measurement uncertainty or if a conventional quantity value is given, in which
case the measurement error is known, and true quantity values of negligible range, in which
case the measurement error is not known, and
(b) if a measurand is supposed to be represented by a unique true quantity value or a set of true
quality values of negligible range, in which case the measurement error is not known.
Note 2: Measurement error should not be confused with production error or mistake.

2.1.7 measurement repeatability (repeatability)[VIM 2.21]


measurement precision under a set of repeatability conditions of measurement

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OIML R 59-1:2016 (E)

2.1.8 measurement reproducibility (reproducibility) [VIM 2.25]


measurement precision under reproducibility conditions of measurement
Note: Relevant statistical terms are given in ISO 5725-1:1994 and ISO 5725-2:1994.
Additional note: In this Recommendation, the reproducibility of measurements between units of the
same type of instrument under reference conditions is assessed by the standard
deviation of differences (SDDI). The reproducibility of measurements from one
instrument when select influence factors are varied is assessed by the magnitude of
the error shift or fault.

2.1.9 rated operating condition [VIM 4.9]


operating condition that must be fulfilled during measurement in order that a measuring instrument or
measuring system performs as designed
Note: Rated operating conditions generally specify intervals of values for a quantity being measured
and for any influence quantity.

2.1.10 reference condition [VIM 4.11]


operating condition prescribed for evaluating the performance of a measuring instrument or measuring
system or for comparison of measurement results
Note 1: Reference conditions specify intervals of values of the measurand and influence quantities.
Note 2: In IEC 60050-300, item 311-06-02, the term “reference condition” refers to an operating
condition under which the specified instrumental measurement uncertainty is the smallest
possible.

2.1.11 reference quantity value; reference value [VIM 5.18]


quantity value used as a basis for comparison with values of quantities of the same kind

2.1.12 repeatability condition of measurement (repeatability condition) [VIM 2.20]


condition of measurement, out of a set of conditions that includes the same measurement procedure,
same operators, same measuring system, same operating conditions and same location, and replicate
measurements on the same or similar objects over a short period of time
Note 1: A condition of measurement is a repeatability condition only with respect to a specified set of
repeatability conditions.
Note 2: In chemistry, the term “intra-serial precision condition of measurement” is sometimes used to
designate this concept.

2.1.13 reproducibility condition of measurement (reproducibility condition) [VIM 2.24]


condition of measurement, out of a set of conditions that includes different locations, operators,
measuring systems, and replicate measurements on the same or similar objects
Note 1: Different measuring systems may use different measurement procedures.
Note 2: A specification should give the conditions changed and unchanged, to the extent practical.

2.1.14 type approval [VIML 2.05]


decision of legal relevance, based on the review of the type evaluation report, that the type of a
measuring instrument complies with the relevant statutory requirements and results in the issuance of
the type approval certificate
Note: See also VIML A.25

9
OIML R 59-1:2016 (E)

2.1.15 type (pattern) evaluation [VIML 2.04]


conformity assessment procedure on one or more specimens of an identified type (pattern) of
measuring instruments which results in an evaluation report and/or an evaluation certificate
Note: ‘Pattern’ is used in legal metrology with the same meaning as ‘type’; in the entries below, only
‘type’ is used.

2.1.16 verification of a measuring instrument [VIML 2.09]


conformity assessment procedure (other than type evaluation) which results in the affixing of a
verification mark and/or issuing of a verification certificate
Note: See also OIML V2-200:2010, 2.44.

2.2 International Organization of Legal Metrology(OIML) terminology

2.2.1 audit trail [OIML D 31, 3.1.2]


continuous data file containing a time stamped information record of events, e.g. changes in the values
of parameters of a device or software updates, or other activities that are legally relevant and which
may influence the metrological characteristics

2.2.2 cryptographic means [OIML D 31, 3.1.11]


encryption of data by the sender (storing or transmitting program) and description by the receiver
(reading program) with the purpose of hiding information from unauthorized persons. Electronic
signing of data with the purpose of enabling the receiver or user of the data to verify the origin of the
data, i.e. to prove their authenticity

2.2.3 fault [OIML D 11, 3.10]


[with reference to a certified measurement standard]: difference between the error of indication
[during or after exposure to a disturbance] and the mean intrinsic error of a measuring instrument
Note 1: Principally, a fault is the result of an undesired change of data contained in or flowing
through an electronic measuring instrument.
Note 2: From the definition it follows that a “fault” is a numerical value which is expressed either in
a unit of measurement or as a relative value.
Additional note: If a certified measurement standard is not used, a fault is the difference between a
single indication during or after a disturbance, and the mean indication at reference
conditions prior to test.

2.2.4 intrinsic error [OIML D 11, 3.8]


error of a measuring instrument, determined under reference conditions

2.2.5 legally relevant [OIML D 31, 3.1.29]


software/hardware/data or part of the software/hardware/data of a measuring instrument which
interferes with properties regulated by legal metrology, e.g. the accuracy of the measurement or the
correct functioning of the measuring instrument

2.2.6 open network [OIML D 31, 3.1.35]


network of arbitrary participants (electronic devices with arbitrary functions). The number, identity
and location of a participant can be dynamic and unknown to the other participants. This is in contrast
to a closed network [D 31, 3.1.6] which is a network of a fixed number of participants with a known
identity functionality and location

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OIML R 59-1:2016 (E)

2.2.7 universal computer [OIML D 31, 3.1.54]


computer that is not constructed for a specific purpose but that can be adapted to the metrological task
by software. In general this software is founded on an operating system that permits loading and
execution of software for specific purposes

2.2.8 (software) validation [OIML D 31, 3.1.56]


confirmation by examination and provision of objective evidence (i.e. information that can be proved
true, based on facts obtained from observations, measurement, test, etc.) that the particular
requirements for the specific intended use are fulfilled. In the present case the related requirements are
those of this Recommendation

2.3 Other terminology

2.3.1 accuracy of a grain moisture calibration; calibration accuracy


performance characteristic of a calibration assessed at reference conditions
Additional note: The assessment requires calculation of , the bias over a set of test samples or the
‘calibration bias’, and the standard deviation of the difference (SDD) between the
meter and the reference method for each of the 2 % moisture intervals which is the
standard deviation of measurement errors from the same sample set. Refer to
R 59-2, A.1.2 for the calculation of  and SDD from measured values. The limiting
values for  and SDD in column 2, Table 4.4.1 shall be observed in order to deem a
calibration as sufficiently accurate.

2.3.2 average error shift


algebraic mean of error shift values calculated from samples of the same grain type with different
moisture levels. The resulting ‘average’ value is indicative of the average variation over the
encompassed measurement range, as opposed to the variation in measured values at one point of the
range
Note: In this Recommendation, reference to a resulting ‘mean’ value is reserved for the mean of
replicated measurements, i.e. the mean of measured values on the same test sample (usually
taken under repeatability conditions).

2.3.3 auxiliary battery


battery that is
(a) mounted in, or connected to, an instrument that can also be powered by the mains power, and
(b) capable of completely powering the instrument for a reasonable period of time.

2.3.4 back-up battery


battery intended to power specific functions of an instrument in the absence of the primary power
supply. Example: to preserve stored data

2.3.5 calibration equation; calibration


set of calibration coefficients for one type of grain to convert raw instrument data into a moisture
content measurement
Note: Both these terms are used in the same context as ‘calibration function’ in Note 1 of VIM 2.39.

11
OIML R 59-1:2016 (E)

2.3.6 checking facility


facility incorporated in a measuring instrument and which enables significant faults to be detected and
acted upon
Note: “Acted upon” refers to any adequate response by the measuring instrument (luminous signal,
acoustic signal, prevention of the measurement process, etc.).

2.3.7 enabling/inhibiting sealable hardware


physically sealable hardware, such as a two-position switch, located on a remotely configurable
device, that enables and inhibits the capability to receive adjustment values or changes to sealable
configuration parameters from a remote device

2.3.8 error shift


with reference to a certified measurement standard: difference between the mean error of indication
while one or more influence quantities are varied within the rated operating conditions and the mean
intrinsic error of a measuring instrument. See 4.4.1 for the error shifts associated with grain moisture
meter testing
Note: If a certified measurement standard is not used, the error shift is the difference between two
measured values: the indication under rated operating conditions and the mean indication at
reference conditions prior to test.

2.3.9 grain
for the purpose of this Recommendation grain means oil seeds, pulses and cereal grains

2.3.10 integrity of programs, data or parameters


assurance that the programs, data or parameters have not been subjected to any unauthorized or
unintended changes during their use, transfer, storage, repair or maintenance

2.3.11 moisture content wet-basis


ratio of moisture to the total mass of the grain sample

2.3.12 moisture meter


instrument that measures a parameter (electrical, optical, etc.) to predict the moisture content of a grain
within specified error limits

2.3.13 sample temperature sensitivity (STS)


measurement variation (relative to the moisture values obtained at reference conditions) resulting from
the range of grain sample temperatures permitted in commercial measurements
Note: STS is controlled in approved moisture calibrations. During assessment, a limit is placed on
the value of the average error shift caused by allowable temperature variations.

2.3.14 significant fault [VIML 5.14]


fault greater than the value specified in this Recommendation (see 4.4.1)
Note: The relevant Recommendation may specify that the following faults are not significant, even
when they exceed the value defined in 4.4.1:
(a) faults arising from simultaneous and mutually independent causes (e.g. EM fields and
discharges) originating in a measuring instrument or in its checking facilities;
(b) faults implying the impossibility to perform any measurement;

12
OIML R 59-1:2016 (E)

(c) transitory faults being momentary variations in the indication, which cannot be interpreted,
memorized or transmitted as a measurement result;
(d) faults giving rise to variations in the measurement result that are serious enough to be noticed
by all those interested in the measurement result; the relevant Recommendation may specify
the nature of these variations.

2.4 Abbreviations and acronyms


AC alternating current
DC direct current
EM electromagnetic
EMC electromagnetic compatibility
e.m.f. electromotive force
ESD electrostatic discharge
EUT equipment under test
IEC International Electrotechnical Committee
ISO International Organization for Standardization
M reference moisture
MPE maximum permissible error
OIML International Organization of Legal Metrology
RF radio frequency
RH relative humidity
SD: standard deviation [See R 59-2, A.1.3]
SDD standard deviation of differences [See R 59-2,A.1.2]
STS sample temperature sensitivity [See R 59-2, A.3]
t actual temperature during a test
t reference temperature during a test
ref
Δt magnitude of the temperature difference between a sample and an instrument at Tt
ref

t minimum environmental temperature specified by the national responsible body for type testing
C

t maximum environmental temperature specified by the national responsible body for type testing
H

 average of the difference between meter reading and reference method (see R 59-2, 2.3.1 and R 59-2,
3.13.11)

2.5 Additional symbols and subscripts used in equations


Additional subscript and symbols are defined in R 59-2, Annex A Test procedures for each equation
associated with each test.

13
OIML R 59-1:2016 (E)

3 Units of measurement

3.1 Moisture content


The unit of measurement for the moisture content of a grain sample, which is to be displayed on a
moisture meter, is the % moisture by mass. Reference moisture (M) is expressed as the percentage
mass loss of the sample as determined by the reference method. The equation below represents wet-
basis moisture content:
m0 − m1
M = × 100%
m0
where m 0 is the original mass of the sample and m1 is the final mass of the sample.

4 Metrological requirements

4.1 Influence quantities

4.1.1 Reference conditions


(a) Ambient temperature: 20 °C to 27 °C
(b) Relative humidity: 30 % to 70 %
(c) Atmospheric pressure: 86 kPa to 106 kPa
(d) Power voltage: nominal mains or test voltage, Vnom or Unom

(e) Power frequency: nominal frequency, Fnom


(f) Instrument tilt position: level at 0º ± 0.1º
Note: During each test, the tref and RHref shall not vary by more than ±2 °C and ±10 % respectively
within the allowable ranges.

4.1.2 Disturbance test ranges


(a) AC mains voltage dips, short interruptions and voltage variations: reduction to 0 %
(0.5 cycle), reduction to 0 % (1 cycle), reduction to 70 % (25 / 30(1) cycles), reduction to 0 %
(250 / 300(1) cycles).
(b) Bursts (transients) on AC mains: Amplitude 1 kV, repetition rate 5 kHz
(c) Radiated radio-frequency fields, electromagnetic fields: 26 MHz – 2 GHz, 10 V/m
(d) Conducted radio-frequency fields: 0.15 MHz – 80(2) MHz, 10 V (e.m.f.)
(e) Electrostatic discharge – direct application: Up to 6 kV contact discharge
(f) Electrostatic discharge – indirect application: Up to 8 kV air discharge
(g) Storage temperature (extreme shipping conditions): –20 ºC to 50 ºC or greater as specified by
the national responsible body.

Note 1: The cycle counts apply for 50 Hz / 60 Hz respectively


Note 2: Testing up to 26 MHz is permitted. Refer to R 59-2, A.4.4 for conditions.

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OIML R 59-1:2016 (E)

4.2 Rated operating conditions


Measuring instruments shall be designed and manufactured such that their errors do not exceed the
MPEs for initial verification as defined in 4.4.2 when operated within the operating conditions defined
below:
(a) Ambient temperature: 10 °C to 30 °C (1)
(b) Relative humidity: up to 85 % no condensation
(c) Atmospheric pressure: 86 kPa to 106 kPa (or as specified by the
national responsible body)
(d) Power voltage: –15 % to +10 % of mains or test voltage
(e) Power frequency: nominal frequency, Fnom
(f) Instrument tilt position: 5 % or maximum allowable on level indicator
where indicator is present
(g) Grain sample temperature: 2 °C to 40 °C (2)
(h) Sample and instrument temperature differential: 10 °C (3)
(i) Grain sample moisture range: Specified by the manufacturer (See 5.1)
(1)
This is the minimum range. The manufacturer or national responsible body may specify a wider
range (see 4.6).
(2)
This is the minimum grain sample temperature range. The manufacturer shall specify the
temperature range for each grain or seed for which the meter is to be used (see 4.7).
(3)
This is the minimum differential. The manufacturer may specify a larger differential. If the
instrument is unable to measure sample temperature then the operating procedure shall be defined
by the national responsible body (see 4.7).

4.3 Reference method


1
An air oven method is the most common rapid reference method for grain moisture determination.
National air oven methods vary widely in procedures and results, but all are based on heating a known
mass sample for a prescribed period of time (or until the sample no longer loses mass) at a prescribed
temperature and measuring the loss of mass. The amount of mass lost is assumed to be the amount of
water that was present in the sample. Unfortunately, water is not the only constituent that is driven off
by heating. In the “ideal” oven method, the heating times and temperatures would be set so that the
amount of non-aqueous material driven off is approximately equal to the amount of water that remains
after drying. Those parameters are determined by comparing the air oven method to other more basic
(and more difficult) methods such as the phosphorous pentoxide (P2O5) method or the Karl Fischer
method. Most air oven methods require hours or days to complete.
The reference method for grain moisture content is the method defined by the national responsible
body.

1
An Investigation of the Nature of the Radio Frequency Dielectric Response in Cereal Grains and Oilseeds with
Engineering Implications for Grain Moisture Meters, A Dissertation in Physics and Engineering, David
B. Funk, Ph.D., D.H.C.

15
OIML R 59-1:2016 (E)

4.4 Maximum permissible errors (MPEs)


For type evaluation the maximum permissible error for grain moisture meters as a function of the grain
type and moisture content is half the MPE that is applied at verification or in-field inspection: The
maximum value within a given interval of moisture content shall be used as the reference moisture
content for all requirements in calibration/testing. For consistency of application in testing laboratories
in different countries, it is recommended that each of the 2 % moisture intervals should begin and end
with an even number of moisture (e.g. within a moisture interval of 10 % to 12 % the MPE will be
calculated based on 12 % moisture).

4.4.1 MPEs for type evaluation

MPEs for type evaluation


(1) (2) (3) (4) (5)
Grain type MPEs in percent Average Repeatability Reproducibility
moisture content (M)
Error shift SD SDDI
%
% %
Corn, oats, If 0.025 × M < 0.4 0.5 × column 2 0.5 × column 2 0.6 × column 2
pulses, rice, then
sorghum, MPEs = 0.4; else
sunflower
MPEs = 0.025 × M

(e.g. If M < 16 then


MPEs = 0.4; else
MPEs = 0.025 × M)

All other If 0.02 × M < 0.35 0.5 × column 2 0.5 × column 2 0.6 × column 2
grains and oil then
seeds MPEs = 0.35; else
MPEs = 0.02 × M
(e.g. If M < 17.5 then
MPEs = 0.35; else
MPEs = 0.02 × M)

4.4.2 MPEs at verification/ in-field inspection


MPEs at verification/ in-field inspection

MPES in percent moisture content (M)


Type of grain or seed
If 0.05 × M < 0.8 then
MPEs = 0.8; else MPEs = 0.05 × M
(I) Corn, oats, pulses, rice, sorghum, sunflower
If 0.04 × M < 0.7 then
MPEs = 0.7; else MPEs = 0.04 × M
(II) All other cereal grains and oilseeds

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OIML R 59-1:2016 (E)

4.5 Accuracy and precision requirements


The error of a moisture meter for a given sample of grains or seeds is the difference between the
average of a result of a series of repeat measurements of a grain sample and the conventional true
value of the moisture content determined using a method defined as the reference by the national
responsible body.

4.6 Instrument environmental operating temperature range


A meter shall meet the moisture accuracy specification over a minimum environmental operating
range of 20 ºC. The minimum environmental operating temperature range is 10 ºC to 30 ºC. No
moisture value may be displayed when the instrument’s environmental operating temperature range is
exceeded. An appropriate error message shall be displayed when the moisture meter is outside its
specified environmental operating temperature range.
The manufacturer may specify a wider temperature range than the t to t required by the national
C H
responsible body in order to meet international requirements. The manufacturer may request type
testing and approval over the wider environmental operating temperature range (i.e. for that particular
type approval application, the manufacturer’s specified ranges are adopted as t to t ).
C H

4.7 Sample temperature range


The manufacturer shall specify the temperature range for each grain or seed for which the meter is to
be used. The minimum sample temperature range for each grain shall be 2 °C to 40 °C. No moisture
value shall be displayed when the temperature range is exceeded. An appropriate error message shall
be displayed when the temperature of the grain sample exceeds the specified temperature range for the
grain. The manufacturer shall specify the maximum allowable difference in temperature between the
meter and the sample for which an accurate moisture determination can be made. The moisture meter
shall be able to take into account a temperature difference of at least 10 °C. No moisture value may be
displayed when the maximum allowable temperature difference is exceeded. An appropriate error
message shall be displayed when the difference in temperature between the meter and the sample
exceeds the specified difference. If the instrument is not able to measure sample temperature, then the
operating procedure shall be defined by the national responsible body.

5 Technical requirements

5.1 Grains and minimum moisture ranges


Due to climatic and crop variability, the national responsible body shall specify a list of grains and
commercially important moisture content ranges (at least 6 % moisture) for the grain types for which a
manufacturer may seek national approval. For meters designed to be used on a number of different
grain types, at least three calibrations shall be submitted for national moisture meter examination. The
grains specified are typically those which
(a) are of greatest economic importance, and
(b) are significantly different in their physical structure to adequately test the instrumentation (e.g.
large grains, small grains, and oil seeds), and
(c) are variable and are typically grown in regions of the national responsible body.
The manufacturer shall specify the grain and oil seed types and the applicable moisture range for the
meter, subject to the minimum ranges specified in 4.1.1.

5.2 Selection of grain on the instrument


Moisture meters shall permit the selection of grain or seeds being measured and the selection of the
grain shall be clearly identified and visible to all parties present.

17
OIML R 59-1:2016 (E)

5.3 Minimum sample size


The minimum allowable sample size used in analysis shall be 100 g or 400 kernels or seeds,
whichever is smaller, except where the national responsible body determines otherwise.

5.4 Determination of quantity and temperature


The moisture meter system shall not require the operator to judge the precise volume or weight and
temperature needed to make an accurate moisture determination. External grinding, weighing and
temperature measurement operations are not permitted.

5.5 Instrument warm-up period


When a meter is turned on it shall not display or record any usable values until the operating
temperature necessary for accurate determination has been attained. This requirement may not be
necessary for instruments which do not require any warm-up time.

5.6 Digital display and recording elements


Meters shall be equipped with a digital indicating element.
The minimum height for the digits used to display moisture content shall be 10 mm.
Moisture content results shall be displayed as percent moisture, wet-basis and if recorded, recorded as
percent moisture content, wet-basis. Subdivisions of this unit shall be in terms of decimal subdivisions
(not fractions).
The display shall permit moisture value determination to 0.1 % resolution. The 0.1 % resolution is for
commercial transactions; at the national responsible body’s option the display and printout shall also
permit 0.01 % resolution for type evaluation only.
The national responsible body may require meters to be equipped with an internal recording device
and/or a communication interface that permits interfacing with an external recording device.
Correspondence between the displayed information and the recording device shall be verified.
The measurement records shall include at least the date, grain type, sample I.D., grain moisture results,
calibration version identification and, as appropriate, error messages.
A digital indicating element shall not display, and a recording device shall not record, any moisture
content values before the end of the measurement cycle.
Especially on multi-constituent meters (e.g. meters which also measure grain protein), provision shall
be made to ensure an unambiguous relation between the displayed/recorded values and the
constituents.

5.7 Data storage


If data storage is required, the measurement data must be stored automatically when the measurement
is concluded. The storage device must have sufficient permanency to ensure that the data are not
corrupted under normal storage conditions. There shall be sufficient memory storage for any particular
application.
The measurement value stored shall be accompanied by all relevant information necessary for future
legally relevant use. The measurement records shall include as a minimum: unambiguous identifier of
the measurement, measurement date, unique identification of the instrument, grain type, moisture
results and units, calibration version identification, error messages and constituent labels (on multi-
constituent meters). Acceptable examples of a measurement identifier include consecutive numbers
enabling assignment to values printed on an invoice, or a test sample ID.

18
OIML R 59-1:2016 (E)

5.8 External data storage


When external stored data are considered as legally relevant, the following additional requirements
have to be fulfilled:
 The data shall be protected by software means to guarantee its authenticity and integrity. The
software that displays or further processes the measurement values and accompanying data
shall check the time of measurement, authenticity and integrity of the data after having read
them from the insecure storage or after having received them from an insecure transmission
channel. If an irregularity is detected, the data shall be discarded or marked unusable. For
instruments using an open network, a higher severity level according to D 31 is required.
Note: Software modules that prepare data for storing or sending, or that check data after
reading or receiving, belong to the legally relevant software part.
 The measurement shall not be inadmissibly influenced by a transmission delay.
 If a transmission interruption occurs because the network services become unavailable, no
measurement data shall be lost. The measurement process shall be stopped to avoid the loss of
measurement data.
Note: General national regulations (for instance for tax purposes) may contain strict limitations for
deleting stored measurement data.

5.9 Meter construction


Moisture meters and all accessory equipment shall be of such materials, design and construction as to
make it probable that, under normal service conditions
(a) accuracy will be maintained,
(b) operating parts will continue to function as intended, and
(c) adjustments will remain reasonably permanent.
Undue stresses, deflections or distortions of parts shall not occur to the extent that accuracy or
permanence is detrimentally affected.
The housing of moisture meters shall be constructed so that the main components of the instrument are
protected from dust and moisture.
The measured quantity may be a quantity or a function of various quantities such as: mass, volume,
temperature, electrical resistance, spectral data or capacitance.
When the principle of measurement of a moisture meter requires the use of a grinding mill, the mill
shall be considered an integral part of the moisture determining process. Its design, method of use and
integration with the moisture meter shall be appropriate and complete for the measurement.

5.10 Marking

5.10.1 General marking


Each moisture meter shall be clearly and permanently marked for the purposes of identification with
the following information:
(a) manufacturer’s name or trademark;
(b) designation of the instrument type (model number) and serial number, given by the
manufacturer; and
(c) type approval mark, if the instrument is approved.

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OIML R 59-1:2016 (E)

5.10.2 Location of marking


The required information shall be so located that it is readily observable without the need to
disassemble parts, requiring the use of any means separate from the device.

5.10.3 Marking operational controls, indications, and features


All operational controls, indications and features indicating switches, light displays and push buttons
shall be clearly identifiable. However, keys necessary only to the operator shall be marked to the
extent that a trained operator can understand the function of each key.

5.11 Ambient temperature operating ranges


A meter shall automatically and clearly indicate when the operating range of the meter has been
exceeded by either an error indication, or by blanking the display.

5.11.1 Moisture range of grain and seed


A meter shall not display or record any moisture content values when the moisture content of the grain
sample is beyond the operating range of the device, unless the moisture representation includes a clear
error indication (and recorded error message with the recorded representation).

5.11.2 Temperature range


A meter shall not display or record any moisture content values and an appropriate error message shall
be displayed when its temperature range and/or the temperature range of the grain and seed and/or the
maximum allowable difference in the meter temperature and sample temperature are exceeded. If the
moisture meter is not able to measure the sample temperature then the operating procedure shall be
defined by the national responsible body.

5.12 Provision for sealing and calibration security


Provision shall be made for appropriate sealing by mechanical, electronic and/or cryptographic means,
making any change that affects the metrological integrity of the instrument impossible or evident.
Calibrations, zero-setting and test point adjustments are considered to affect metrological
characteristics and shall be sealed.
Examples of appropriate sealing means are: mechanical sealing, event counter, audit trail, and access
only via interfaces protected by cryptographic means.
After securing and/or verification, the software of an instrument shall not be modifiable or uploadable
via any interface or by other means without breaking the seal.
Refer to Annex C which contains practical guidance for sealing moisture measuring instruments,
including consideration of sealable parameters and details of sealing mechanisms, e.g. metrological
audit trails.

5.13 Manufacturer’s manual


With each instrument, the manufacturer shall provide a manual that describes the installation,
operation and routine maintenance of the moisture meter and its accessories. In addition, the manual
must include the following information:
(a) name and address of the manufacturer;
(b) type or pattern of the meter with which it is intended to be used;
(c) date of issue;
(d) kind or varieties of grain for which the meter is designed to be used; and
(e) limitations of use, including, but not confined to the moisture measurement range, grain or
seed temperature, maximum allowable temperature difference between the grain sample and

20
OIML R 59-1:2016 (E)

the meter, meter operating temperature range, voltage and frequency ranges, electromagnetic
interferences and electromagnetic compatibility. In addition, the manual shall be supplied to
the owner/user of the instrument in the official language(s) of the countries in which it is used
or in a language accepted by the national responsible body.

5.14 Visibility of the moisture meter and of the measurement operations


Moisture meters in service shall be so placed that all parties present have the possibility of
simultaneously seeing all the measurement operations. The indicating or recording device should be
seen at the same time, and all necessary steps shall be taken to eliminate any possibility of error or
fraud.

5.15 Power supply


A meter that uses alternating current must perform within applicable limits when tested in accordance
with R 59-2, A.2.4.1

5.16 Battery-operated instruments


Battery-operated instruments shall not indicate or record values outside the applicable tolerance limits
when battery power output is excessive or deficient.

5.16.1 Non-rechargeable batteries


Instruments powered by non-rechargeable batteries or by rechargeable batteries that cannot be
(re)charged during the operation of the measuring instrument shall comply with the following
requirements:
(a) an instrument provided with new or fully charged batteries of the specified type shall comply
with the metrological requirements; and
(b) as soon as the battery voltage has dropped to a value specified by the manufacturer as the
minimum value of voltage at which the instrument complies with metrological requirements,
this shall be detected and acted upon by the instrument.
For these instruments, no special tests for disturbances associated with the “mains” power (R 59-2,
A.4.1 and R 59-2, A.4.2) have to be carried out.
In the criteria for (categories of) instruments, a minimum period of time shall be stated during which
the instrument shall function correctly without renewing or recharging the batteries and (in particular
for continuous totalizing measuring equipment) provisions may be prescribed that prevent the loss of
stored data.

5.16.2 Rechargeable auxiliary batteries


Instruments powered by rechargeable auxiliary batteries that are intended to be (re)charged during the
operation of the measuring instrument shall both
(a) comply with the requirements of 5.16.1 with the mains power switched off, and
(b) comply with the requirements for AC mains powered instruments with the mains power
switched on.

5.16.3 Backup batteries


Instruments powered by the mains power and provided with a backup battery for data-storage only
shall comply with the requirements for AC mains powered instruments.
A minimum period of time shall be stated during which the relevant function of the instrument shall
function properly without renewing or recharging the batteries.
The provisions of 5.16.1(b) and 5.16.2 do not apply for backup batteries.

21
OIML R 59-1:2016 (E)

5.17 Level indicating means


A meter shall be equipped with a level indicator and leveling adjustment if its performance is changed
by an amount greater than the applicable tolerance when the meter is moved from a level position to a
position that is out of level in any direction up to 5 % from its normal operating position. The level
indicating means shall be readable without removing any meter parts requiring a tool.

5.18 Software-controlled electronic devices and security


The requirements of OIML D 31 shall be fulfilled. In general, for moisture meters the severity level I,
examined with validation procedure A, is required.
Note: The severity levels describe different protection levels of the software, depending on the risk
of fraud or on the level of conformity. The validation procedures define the level of
examination for type approvals.

5.18.1 Specifications of the software requirements


For instruments and modules operated by software, the manufacturer shall describe or declare how the
software is implemented within the instrument or module, i.e. if it is installed in a fixed hardware and
software environment (embedded) or on a universal computer system (implemented into the housing
or external).
Legally relevant software shall be clearly identifiable via a unique software version or a checksum. In
the normal operation mode of the instrument, the software version or the checksum shall be displayed
or printed out on command or shall be displayed during the start-up procedure of the instrument.
Legally relevant measuring algorithms and functions shall be appropriate and functionally correct as
evidenced by the instrument correctly displaying and recording the measurement result and the
required accompanying information. It shall be possible to validate algorithms and functions where
required by metrological tests.
The conformity of the legally relevant software on each instrument to that in the approved type shall
be at level (b) described in D 31, 5.2.5. In types where selected functions or parts of the source code
can be modified, it shall be possible to detect software variations, e.g. via checksum values.
Further measurements shall not be possible when a significant fault is detected.
If the software of the instrument is separated into legally relevant and non-relevant parts, the
requirements of D 31, 5.2.1.2 shall be fulfilled.
For instruments/measuring systems using an internal or external universal computer, the legally
relevant software shall be operated only in the environment specified for its correct functioning.
If necessary to secure the correct functioning of the legally relevant software, the operating system
shall be fixed to a defined invariant configuration.
Note: A fixed environment for software is also required for instruments where cryptographic data
protection is implemented or when software changes on a verified instrument are permitted
without an appointed verifier onsite (i.e. the ‘Traced updates’ described in D 31, 5.2.6.3).
The national responsible body may apply the requirements in 5.8 if measurement data has to leave the
measuring instrument and be stored or transmitted in an insecure environment before it is used for
commercial purposes.

5.18.2 Acceptable solutions for software identification


The software identification is provided in the normal operation mode by either
 a clearly identified operation of a physical or soft key, button, or switch, or
 a continuously displayed version number or checksum, etc.,

22
OIML R 59-1:2016 (E)

accompanied in both cases by clear instructions on how to check the actual software identification
against the reference number (as listed in the OIML certificate) marked on or displayed by the
instrument.

5.18.3 Software documentation


In addition to the documentation required in R 59-2, 2.2, the manufacturer shall submit the following
documentation:
a) description of the legally relevant software and how the requirements of 5.18.1 are met;
b) description of suitable system configuration and minimal required resources;
c) description of security means of the operating system (password, etc. if applicable);
d) description of the (software) sealing method(s);
e) overview of the system hardware, e.g. topology block diagram, type of computer(s), type of
network, etc. – where a hardware component is deemed legally relevant or where it performs
legally relevant functions, this should also be identified;
f) description of the accuracy of the algorithms (e.g. filtering of A/D conversion results, price
calculation, rounding algorithms, etc.);
g) description of the user interface, menus and dialogues;
h) description of the software identification which has to be clearly assigned to the legally
relevant functions including the description of all encryption means (if any);
i) clear instructions on how to check the actual software identification against the reference
number as listed in the type approval certificate. This reference may additionally be marked on
or displayed by the instrument;
j) list of commands of each hardware interface of the measuring instrument / electronic device /
sub-assembly including a statement of completeness;
k) list of durability errors that are detected by the software and if necessary for understanding;
l) description of the detecting algorithms;
m) description of data sets stored or transmitted;
n) if fault detection is realized in the software, a list of faults that are detected and a description
of the detecting algorithm; and
o) operating manual.

5.18.4 Grain calibrations and integrity


Grain moisture meters measure the effect of moisture on certain electrical or optical properties of
grain. So, as the grain crop changes, the effect of moisture on these physical properties of the grain
may change based on the crop year. The national responsible body may authorize updates on
calibrations based on grain data collected during the current and/or recent years to accommodate for
the seasonal and crop year variations. The national responsible body may also require retention of the
data that is used to adjust the grain calibration. In many cases the grain calibration data are
downloaded to the instrument using a communication interface. These are not considered software
changes that would require a change to the software identification. Changes to the grain calibrations of
the device shall be recorded in an audit trail or event logger.

5.18.4.1Calibration version

A meter shall be capable of displaying calibration constants, a unique calibration name, or a unique
calibration version number for use in verifying that the latest version of the calibration is being used to
make moisture content determinations.

23
OIML R 59-1:2016 (E)

5.18.4.2Calibration protection

If calibration constants are digitally stored in an electronically alterable form, the meter shall be
designed to make automatic checks to detect unauthorized modification. An error message shall be
displayed if calibration constants have been electronically corrupted and no further measurement shall
be possible.

5.18.4.3Calibration transfer

The instrument hardware/software design and calibration procedures shall permit calibration
development and the transfer of calibrations between instruments of like models without requiring
user slope or bias adjustments.

5.18.5 Correctness of algorithms and functions


The measuring algorithms and functions of a measuring device shall be functionally correct.
The measurement result and any accompanying information shall be displayed, recorded and printed
correctly.
It shall be possible to validate algorithms and functions by metrological tests.

5.18.6 Software protection

5.18.6.1Prevention misuse

A measuring instrument, and especially the software, shall be constructed in such a way that
possibilities for unintentional, accidental or intentional misuse are minimal.

5.18.6.2Fraud protection

For protection against fraudulent use, the following requirements shall be fulfilled:
 the legally relevant software shall be secured against unauthorized modification, loading, or
changes by swapping the memory device. In addition to mechanical sealing, technical means
may be necessary to secure measuring instruments having an operating system or an option to
load software. Only clearly documented functions are allowed to be activated by the user
interface, which shall be realized in such a way that it does not facilitate fraudulent use; and
 parameters that fix the legally relevant characteristics of the measuring instrument shall be
secured against unauthorized modification. If necessary for the purpose of verification, it shall
be possible to display or print the current parameter settings.

5.18.7 Fault detection


Appropriate fault detection criteria (i.e. operating ranges) are included in the relevant sections of this
Recommendation.

24
OIML R 59-1:2016 (E)

6 Bibliography
At the time of publication, the editions indicated were valid. All normative documents are subject to
revision, and the users of this Recommendation are encouraged to apply the most recent editions of the
normative documents indicated below. Members of the IEC and ISO maintain registers of currently
valid International Standards.
The actual status of the Standards referred to can also be found on the Internet:
• IEC Publications: http://www.iec.ch/searchpub/cur_fut.htm
• ISO Publications: http://www.iso.org/iso/iso_catalogue.htm
• OIML Publications: http://www.oiml.org/en/publications/recommendations
(with free download of PDF files).
In order to avoid any misunderstanding, it is highly recommended that all references to Standards in
OIML Recommendations and Documents be followed by the version referred to (generally the year or
date).

Ref. Standards and reference documents Description


[1] ISO/IEC Guide 99; OIML V 2-200: 2012 An international agreement on terminology,
prepared as a collaborative work of experts
International Vocabulary of Metrology –
appointed by the BIPM, IEC, IFCC, ISO,
Basic and General Concepts and Associated
IUPAC, IUPAP and OIML. This vocabulary
Terms (VIM)
covers subjects relating to measurement and
includes information on the determination of
physical constants and other fundamental
properties of materials and substances. In
practice, these publications are usually
referred to as the “VIM”.
[2] OIML V 1:2013 No abstract available.
International Vocabulary of Terms in Legal
Metrology (VIML)
[3] OIML D 11:2013 Guidance for establishing appropriate
metrological performance testing
General requirements for electronic
requirements for influence quantities that
measuring instruments
may affect the measuring instruments
covered by International Recommendations.
[4] OIML D 31:2008 Specifies the general requirements
applicable to software related functionality
General requirements for software
in measuring instruments and gives guidance
controlled measuring instruments
for verifying the compliance of an
instrument with these requirements.
[5] ISO/DIS 7700-2: 20XX Specifies a method for checking the
performance of meters in service for
Check of the calibration of moisture meters
measuring the moisture content of oilseeds.
in use - Part 2:moisture meters for oilseeds
[6] IEC/TR 61000-2-1: 1990-05 Provides information on the various types of
disturbances that can be expected on public
Electromagnetic compatibility (EMC) Part 2
power supply systems.
Environment Section 1: Description of the
environment-Electromagnetic environment
for low-frequency conducted disturbances

25
OIML R 59-1:2016 (E)

and signaling in public power supply


systems
[7] IEC 61000-2-2: 2002 This standard is concerned with conducted
disturbances in the frequency range from
Electromagnetic compatibility (EMC) Part
0 kHz to 9 kHz, with an extension up to
2-2: Environment- Compatibility levels for
148.5 kHz specifically for mains signaling
low-frequency conducted disturbances and
systems.
signaling in public power supply systems
[8] IEC 61000-4-1: (2000-04) Provides EMC standards on testing and
measurement techniques and provides
Basic Electromagnetic compatibility (EMC)
general recommendations concerning the
Part 4-1: Testing and measurement
choice of relevant tests.
techniques-Overview of IEC 61000-4 series

[9] IEC 61326-1: 2005 Specifies minimum requirements for


immunity and emissions regarding
Electrical equipment for measurement,
electromagnetic compatibility (EMC) for
control and laboratory use-EMC
electrical equipment, operating from a
requirements
supply of less than 1000 V a.c. or 1500 V
d.c.
[10] National Conference on Weights and U.S. type evaluation procedures for grain
Measures, Publication 14, Grain moisture moisture meters and protein, starch and oil
meters and near infrared grain analyzers: analyzers.
2014
[11] An investigation of the nature of the radio A dissertation in physics and engineering.
frequency dielectric response in cereal
grains and oilseeds with engineering
implications for grain moisture meters, a
dissertation in physics and engineering,
David B. Funk, Ph.D. H.C: 2001
[12] OIML D 3:1979 This Document deals with official actions
which may be undertaken by a State for the
Legal qualification of measuring
purpose of attributing a “legal” quality to
instruments
measuring instruments. Every effort has
been made to consider all possible methods
involved in these official actions.
[13] ISO 650:1977 The requirements for five series of glass
hydrometers concerning reference levels for
Relative density 60/60 degrees F
adjustment and reading, materials,
hydrometers for general purposes
dimensions, form, scale and handling.
[14] OIML R 76-1:2006 This Recommendation specifies the
metrological and technical requirements for
Non-automatic weighing instruments
non-automatic weighing instruments that are
subject to official metrological control. It is
intended to provide standardized
requirements and testing procedures to
evaluate the metrological and technical
characteristics in a uniform and traceable
way.

26
OIML R 59-1:2016 (E)

[15] ISO 7700-1:2008 Food products – checking the performance


of moisture meters in use part 1: moisture
Food products—Checking the performance
meters for cereals
of moisture meters in use—Part1:Moisture
meters for cereals
[16] IEC 61000-4-6 (2003-05) with amendment 1 Relates to the conducted immunity
(2004-10) requirements of electrical and electronic
equipment to electromagnetic disturbances
Electromagnetic compatibility (EMC) -
emanating from intended radio-frequency
Part 4: Testing and measurement techniques
(RF) transmitters in the frequency range
Section 6: Immunity to conducted
9 kHz up to 80 MHz. Equipment not having
disturbances, induced by radio-frequency
at least one conducting cable (such as mains
fields
supply, signal line or earth connection),
which can couple the equipment to the
disturbing RF fields is excluded. This
standard does not intend to specify the tests
to be applied to particular apparatus or
systems. Its main aim is to give a general
basic reference to all concerned product
committees of the IEC. The product
committees (or users and manufacturers of
equipment) remain responsible for the
appropriate choice of the test and the
severity level to be applied to their
equipment.
[17] IEC 61000-4-2 Edition 2.0 (2008-12) This publication is based on IEC 60801-2
(second edition: 1991). It relates to the
Basic EMC Publication
immunity requirements and test methods for
Electromagnetic compatibility (EMC) - electrical and electronic equipment subjected
Part 4-2 Testing and measurement to static electricity discharges, from
techniques - Electrostatic discharge operators directly, and to adjacent objects. It
immunity test additionally defines ranges of test levels
which relate to different environmental and
installation conditions and establishes test
procedures. The object of this standard is to
establish a common and reproducible basis
for evaluating the performance of electrical
and electronic equipment when subjected to
electrostatic discharges. In addition, it
includes electrostatic discharges which may
occur from personnel to objects near vital
equipment.
[18] IEC 61000-4-11 (2004-03) Defines the immunity test methods and
range of preferred test levels for electrical
Electromagnetic compatibility (EMC) -
and electronic equipment connected to low-
Part 4-11: Testing and measuring
voltage power supply networks for voltage
techniques - Voltage dips, short
dips, short interruptions, and voltage
interruptions and voltage variations
variations. This standard applies to electrical
immunity tests
and electronic equipment having a rated
input current not exceeding 16 A per phase,
for connection to 50 Hz or 60 Hz AC
networks. It does not apply to electrical and
electronic equipment for connection to
400 Hz AC networks. Tests for these

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OIML R 59-1:2016 (E)

networks will be covered by future IEC


standards. The object of this standard is to
establish a common reference for evaluating
the immunity of electrical and electronic
equipment when subjected to voltage dips,
short interruptions and voltage variations. It
has the status of a Basic EMC Publication in
accordance with IEC Guide 107.
[19] IEC 61000-6-1 (1997-07) Defines the immunity test requirements in
relation to continuous and transient,
Electromagnetic compatibility (EMC) -
conducted and radiated disturbances,
Part 6: Generic standards - Section 1:
including electrostatic discharges, for
Immunity for residential, commercial and
electrical and electronic apparatus intended
light-industrial environments
for use in residential, commercial and light-
industrial environment, and for which no
dedicated product or product-family
standard exists. Immunity requirements in
the frequency range 0 kHz to 400 GHz are
covered and are specified for each port
considered. This standard applies to
apparatus intended to be directly connected
to a low voltage public mains network or
connected to a dedicated DC source which is
intended to interface between the apparatus
and the low-voltage public mains network.
[20] IEC 61000-6-2 (1999-01) Applies to electrical and electronic apparatus
intended for use in industrial environments,
Electromagnetic compatibility (EMC) -
for which no dedicated product or product-
Part 6-2: Generic standards – Immunity for
family immunity standard exists. Immunity
industrial environments
requirements in the frequency range 0 Hz to
400 GHz are covered, in relation to
continuous and transient, conducted and
radiated disturbances, including electrostatic
discharges. Test requirements are specified
for each port considered. Apparatus intended
to be used in industrial locations are
characterized by the existence of one or
more of the following:
– a power network exists powered by a high
or medium voltage power transformer
dedicated for the supply of an installation
feeding a manufacturing or similar plant;
– industrial, scientific and medical (ISM)
apparatus;
– heavy inductive or capacitive loads are
frequently switched; and
– currents and associated magnetic fields are
high.

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OIML R 59-1:2016 (E)

[21] IEC 61000-4-4 (2004-07) Establishes a common and reproducible


reference for evaluating the immunity of
Electromagnetic compatibility (EMC) -
electrical and electronic equipment when
Part 4-4: Testing and measurement
subjected to electrical fast transient/burst on
techniques - Electrical fast transient/burst
supply, signal, control and earth ports.
immunity test
[22] IEC 61000-4-3 Applies to the immunity of electrical and
electronic equipment to radiated
Consolidated Edition 2.1 (2002-09) with
electromagnetic energy. Establishes test
amendment 1 (2002-08)
levels and the required test procedures.
Electromagnetic compatibility (EMC) - Establishes a common reference for
Part 4: Testing and measurement evaluating the performance of electrical and
Techniques Section 3: Radiated, radio- electronic equipment when subjected to
frequency, electromagnetic field immunity radio-frequency electromagnetic fields.
test
[23] ISO 24333: 2009 Specifies requirements for the dynamic or
static sampling, by manual or mechanical
Cereals and cereal products – Sampling
means, of cereals and cereal products, for
assessment of their quality and condition.
[24] ISO 6540:1980 Section one specifies the reference method.
It consists of grinding of sample, if
Maize – Determination of moisture content
necessary, after pre-conditioning, if
(on milled grains and on whole grains
required, then drying a test portion at a
temperature between 130 and 133 °C under
conditions which enable a result to be
obtained which is in agreement with that
obtained by the absolute method (prescribed
in the annex). Section two specifies the
routine method on whole grains. It consists
of drying whole grains for 38 h at a
temperature between 130 and 133 °C.
Note: The reference method for grain
moisture content is the method defined by
the national responsible body.
[25] ISO 712:2009 Specifies a routine reference method for the
determination of the moisture content of
Cereals and cereal products –
cereals and cereal products.
Determination of moisture content –
Reference method Note: The reference method for grain
moisture content is the method defined by
the national responsible body.

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OIML R 59-1:2016 (E)

Annex A
Principles for sealing
(Informative)

This Annex highlights considerations for determining which parameters of a grain moisture measuring
instrument require sealing. It also provides examples of sealing methods, such as metrological audit
trails, and the minimum requirements for an effective seal.

A.1 Terminology specific to this Annex

A.1.1 adjustment mode


operational mode of a measuring instrument which enables the user to make adjustments to sealable
parameters, including changes to configuration parameters

A.1.2 adjustment
change in the value of the sealable calibration parameters or the sealable configuration parameters of
an instrument

A.1.3 audit trail


electronic count and/or information record of the changes to the values of the calibration or
configuration parameters of a measuring instrument

A.1.4 enabling/inhibiting sealable hardware


physically sealable hardware, such as a two-position switch located on a remotely configurable
instrument, that enables and inhibits the sealable parameters of the instrument from being changed
from a remote device

A.1.5 event
while in adjustment mode, an action in which
 one or more changes are made to configuration parameters, or
 adjustments are made to one value (or values for a set of values) for a calibration parameter
(e.g. adjustments for a set of calibration factors to linearize device output)
If no adjustment is made, then there is no event. In the case of a centralized audit trail, the same values
for the same parameter sent to multiple devices shall be considered to be the same event. In the case of
a centralized event logger, the event logger must identify both the device and the parameter that was
changed.

A.1.6 event counter


non-resettable counter that increments once each time the mode that permits changes to sealable
parameters is entered and one or more changes are made to sealable parameters of the instrument

A.1.7 event logger


form of audit trail containing a series of records where each record contains the number from the event
counter corresponding to the change to a sealable parameter, the identification of the parameter that
was changed, the time and date on which the parameter was changed, and the new value of the
parameter

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OIML R 59-1:2016 (E)

A.1.8 physical seal


physical means, such as lead and wire, used to seal a device to detect access to those adjustable
features that are required to be sealed

A.1.9 remote configuration capability


ability to adjust a measuring instrument or change its sealable parameters from or through some other
device that is not itself necessary for the measurement operation or is not a permanent part of the
instrument

A.1.10 remote device


device that (1) is not required for the measurement operation of the instrument or for computing the
transaction information in one or more of the available operating modes for commercial
measurements, or (2) is not a permanent part of the measuring instrument. In the context of this
Annex, a remote device has the ability to adjust a measuring instrument or change its sealable
configurable parameters

A.1.11 remotely configurable device


measuring instrument with remote configuration capability that permits sealable configuration or
calibration parameter values to be deleted, appended to, modified or substituted in whole or in part by
downloading over any type of communications link from another device, such as a geographically
local or remote console or computer

A.1.12 seal
as a verb, to seal a device is to make a device secure so that access to adjustments and other sealable
parameters will be detectable

A.1.13 sealable parameters


calibration and configuration parameters that are required to be sealed
Additional note: Unrestricted access means that a physical security seal is not present, so that access
to the sealable parameters is available from a remote device at any time at the
request of an authorized operator subject to the operating status of the receiving
device.

A.2 Principles for determining features to be sealed


The need to seal certain features depends upon both the following:
 the ease with which the feature or the selection of the feature can be used to facilitate fraud;
and
 the likelihood that the use of the feature will result in fraud being undetected.
Features or functions which the operator routinely uses as part of device operation, such as selecting
the grain calibration to be used, are not sealable parameters and shall not be sealed.
If selection of a parameter or set of parameters would result in performance that would be obviously in
error, such as the selection of parameters for different countries, then it is not necessary to seal the
selection of these features.
If individual device characteristics are selectable from a “menu” or a series of programming steps,
then access to the “programming mode” must be sealable.
Note: If an audit trail is the only means of security, then it shall update only after at least one
sealable parameter has been changed. Simply accessing the sealable parameters via a menu
shall not update the audit trail.

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For parameters protected by physical means of security, once a physical security seal is applied to the
instrument it should not be possible to make a metrological change to those parameters without
breaking that seal. For parameters protected by electronic means of security, it shall not be possible to
make a metrological change to those parameters without that change being reflected in an audit trail.
Since this philosophy addresses provisions for protecting access to any metrological adjustment, the
philosophy should be applied consistently to all electronic device types.
If a device must undergo a physical act, such as cutting a wire and physically repairing the cut to
reactivate the parameter, then this physical repair process would be considered an acceptable way to
select parameters without requiring a physical seal or an audit trail.

A.3 Typical features and parameters to be sealed


The following provides examples of parameters that are to be sealed. The examples are provided for
guidance and are not intended to cover all possible parameters.

A.3.1 Calibration parameters


Calibration parameters are those adjustable parameters that can affect measurement or performance
accuracy, and whose values need to be updated on an ongoing basis to maintain device accuracy.
Calibration parameters can be classified into three categories:
(a) those parameters which are adjusted to standardize or normalize instrument response to
changes in the physical parameter being measured. Examples include zero-setting and test
point adjustments, temperature sensing element zero and span adjustments, amplifier gain
settings, optical wavelength standardization adjustments, etc. These parameters are normally
set by the manufacturer or a competent service representative;
(b) those parameters which are common to all instruments of the same type for a given grain type
(e.g. grain calibration coefficients). The approval certificate lists the calibration coefficients
(or a unique identifier) for each grain type which has been approved for use on a particular
type of grain protein measuring instrument; and
(c) those parameters which are adjusted for each grain type to standardize moisture readings on
similar instruments (e.g. slope and bias settings).

A.3.2 Configuration parameters


Configuration parameters are those adjustable or selectable parameters that can affect the accuracy of
a transaction or that can significantly increase the potential for fraudulent use of the device, and whose
values only need to be updated during instrument installation or upon replacement of a component and
which are not expected to change after the initial installation settings have been made:
(a) system date and time (only if used by an event logger as audit trail information);
(b) value of minimum indication and recorded moisture;
(c) sample size and/or number of sub portions measured (if not determined by individual
calibrations);
(d) password for access to sealable parameters (if used);
(e) enable/disable display of constituent values that are not legally relevant;
(f) format for the display and recording of results;
(g) operating range limits (e.g. temperatures); and
(h) enable/disable display or recording of results for out-of-limits conditions.

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A.3.3 Grain moisture meter features and parameters


Typical features or parameters Typical features or parameters
to be sealed not to be sealed
Measuring element adjustments (both Communications protocol
mechanical and electronic)
Weight sensing adjustments (both mechanical
and electronic)
Temperature sensing adjustments (both
mechanical and electronic)
Any tables or parameters residing in software
to normalize the response of similar
instruments
Temperature probes and temperature offsets
in software
Grain calibration coefficients
Slope and bias coefficients
System date and time (only if used by an event
logger as audit trail information)

Note: The above examples of adjustments, parameters and features to be sealed are to be considered
“typical” or “normal”. This list may not be all-inclusive, and there may be other parameters
which affect the metrological performance of the device and which must, therefore, be sealed.
If listed parameters or other parameters which may affect the metrological function of the
device are not sealed, the manufacturer must demonstrate that all settings comply with the
most stringent requirements for the application of the device.

A.4 Methods of sealing and metrological audit trails

A.4.1 Scope
The ability of users to make changes that affect the metrological integrity of the device (e.g. slope,
bias, etc.) in normal operation and the remote configuration capability of commercial moisture
measuring instruments has led to new, more appropriate means of sealing being implemented. These
instruments must either be physically sealed or must incorporate an approved form of audit trail.

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A.4.2 Categories of device and methods of sealing


Categories of device Method of sealing
Category 1: No remote configuration capability Seal by physical seal or two event counters: one
for calibration parameters (000 to 999) and one
for configuration parameters (000 to 999.) If
equipped with event counters, the device must
be capable of displaying, or printing through
the device or through another on-site device,
the contents of the counters.
Category 2: Remote configuration capability, The hardware enabling access for remote
but access is controlled by physical hardware. communication must be at the device and
sealed using a physical seal or two event
The device shall clearly indicate that it is in the
counters; one for calibration parameters (000 to
remote configuration mode and shall not be
999) and one for configuration parameters (000
capable of operating in the measuring mode
to 999.) If equipped with event counters, the
while enabled for remote configuration.
device must be capable of displaying, or
printing through the device or through another
on-site device, the contents of the counters.
Category 3: Remote configuration capability, An event logger is required in the device; it
access may be unlimited or controlled through a must include an event counter (000 to 999), the
software switch (e.g. password). parameter ID, the date and time of the change
and the new value of the parameter (for
When accessed for the purpose of modifying
calibration changes consisting of multiple
sealable parameters, the device shall clearly
constants, the calibration version number may
indicate that it is in the configuration mode and
be used rather than the calibration constants).
shall not be capable of operating in the
A printed copy of the information must be
measuring mode.
available through the device or through another
on-site device. The event logger shall have a
capacity to retain records equal to 25 times the
number of sealable parameters in the device,
but not more than 1000 records are required.
Note: This does not require 1000 changes to be
stored for each parameter.
Category 3a: No remote capability, but operator Same as Category 3.
is able to make changes that affect the
metrological integrity of the device (e.g. slope,
bias, etc.) in normal operation.
When accessed for the purpose of modifying
sealable parameters, the device shall clearly
indicate that it is in the configuration mode and
shall not be capable of operating in the
measuring mode.
Category 3b: No remote capability, but access Same as Category 3.
to metrological parameters is controlled through
a software switch (e.g. password).
When accessed for the purpose of modifying
sealable parameters, the device shall clearly
indicate that it is in the configuration mode and
shall not be capable of operating in the
measuring mode.

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Included below are the requirements for the acceptable forms of metrological audit trail, which are
recognized as providing acceptable security.

A.4.3 Event logger: an acceptable form of audit trail


An event logger is the minimum form of audit trail for instruments that allow unrestricted access
whether by an operator or a remote device, to the configuration or calibration parameters.
(a) An event logger shall contain the following information: event counter; date and time;
parameter ID; new value.
Note: For calibration changes consisting of multiple calibration constants, the calibration
version number shall be used as the new value rather than the calibration constants.
(b) This information shall be automatically entered into the event logger by the measuring
instrument. Additional relevant information is permitted (e.g. the identification of the person
who made the adjustment or the old value of the parameter that was changed).
(c) The date and time shall be presented in an understandable format. The date shall include the
month, day and year. The time shall include the hour and minutes.
(d) A hard copy printout of the contents of the event logger shall be available upon demand from
the instrument or an associated device on the site of the instrument installation. The printing of
the event logger contents shall exclude other information not relevant to the changes logged
such as transaction data, number of measurements performed, etc.
(e) An event logger shall have a capacity of at least 25 times the number of sealable parameters;
however, it is not required to retain more than 1000 events for all parameters combined.

A.4.4 General requirements for metrological audit trails


The following general requirements for metrological audit trails shall be satisfied:
(a) The adjustment mode shall address only sealable parameters in order to avoid entering the
adjustment mode to access non-sealable parameters that must be routinely changed as part of
the normal use of the device.
(b) An event counter shall have a capacity of at least 1000 values (e.g. 000 to 999).
(c) In the case of an event logger, the event counter will increment once for each change to a
sealable parameter since each new value must be retained in the event logger. If an adjustment
mode is entered but no changes are made, this does not constitute an event and the counter
must not increment.
(d) When the storage memory of the event logger has been filled to capacity, any new event shall
cause the oldest event to be deleted. The event counter used in the event logger shall continue
to increment to its capacity, although the event logger may retain fewer records than the count
capacity of the event counter. The event counter provides the necessary information to indicate
the number of records that have been overwritten in the event logger as new information
overwrites the old records.
(e) The audit trail data shall be:
1) Stored in non-volatile memory and shall be retained for at least 30 days if power is
removed from the device; and
2) Protected from unauthorized erasure, substitution, or modification.
(f) Access to the audit trail information for the purpose of printing the contents must be
“convenient” for an enforcement official of the national responsible body:
1) Accessing the audit trail information for review shall be separate from the calibration
mode so there is no possibility for the official to change or corrupt the device
configuration or the contents of the audit trail.

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2) Accessing the audit trail information shall not affect the normal operation of a device
before or after accessing the information.
3) A key (for a panel lock) may be required to gain access to the means to view the contents
of the audit trail. Access may be through the supervisor’s mode of operation of the device.
4) Accessing the audit trail information shall not require the removal of any additional parts
other than normal requirements to inspect the integrity of a physical seal.
(g) The printed form of the audit trail information shall be readily interpretable by an official.
(h) The information from an event logger shall be printed in order from the most recent event to
the oldest event. If a device is not capable of printing all the information for a single event on
one line or at one time, the information shall be displayed in blocks of information, which are
readily understandable.

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