R059-1-e16
R059-1-e16
ORGANISATION INTERNATIONALE
DE MÉTROLOGIE LÉGALE
INTERNATIONAL ORGANIZATION
OF LEGAL METROLOGY
OIML R 59-1:2016 (E)
Contents
Foreword ................................................................................................................................................. 5
Introduction ............................................................................................................................................. 6
1 Scope .................................................................................................................................................. 7
1.1 Requirements and test ............................................................................................................... 7
1.2 Indications ................................................................................................................................ 7
1.3 Application ............................................................................................................................... 7
1.4 Type of measuring instrument .................................................................................................. 7
1.5 New technology ........................................................................................................................ 7
2 Terminology ....................................................................................................................................... 7
2.1 International Vocabulary Metrology (VIM) ............................................................................. 7
2.2 International Organization of Legal Metrology(OIML) Terminology ................................... 10
2.3 Other terminology................................................................................................................... 11
2.4 Abbreviations and acronyms .................................................................................................. 13
2.5 Additional symbols and subscripts used in equations ............................................................ 13
3 Units of measurement ....................................................................................................................... 14
3.1 Moisture content ..................................................................................................................... 14
4 Metrological requirements................................................................................................................ 14
4.1 Influence quantities................................................................................................................. 14
4.2 Rated operating conditions ..................................................................................................... 15
4.3 Reference method ................................................................................................................... 15
4.4 Maximum permissible errors (MPEs) .................................................................................... 16
4.5 Accuracy and precision requirements ..................................................................................... 17
4.6 Instrument environmental operating temperature range ......................................................... 17
4.7 Sample temperature range ...................................................................................................... 17
5 Technical requirements .................................................................................................................... 17
5.1 Grains and minimum moisture ranges .................................................................................... 17
5.2 Selection of grain on the instrument ....................................................................................... 17
5.3 Minimum sample size ............................................................................................................. 18
5.4 Determination of quantity and temperature ............................................................................ 18
5.5 Instrument warm-up period .................................................................................................... 18
5.6 Digital display and recording elements .................................................................................. 18
5.7 Data storage ............................................................................................................................ 18
5.8 External data storage .............................................................................................................. 19
5.9 Meter construction .................................................................................................................. 19
5.10 Marking .................................................................................................................................. 19
5.11 Ambient temperature operating ranges ................................................................................... 20
5.12 Provision for sealing and calibration security......................................................................... 20
5.13 Manufacturer’s manual ........................................................................................................... 20
5.14 Visibility of the moisture meter and of the measurement operations ..................................... 21
5.15 Power supply .......................................................................................................................... 21
5.16 Battery-operated instruments .................................................................................................. 21
5.17 Level indicating means ........................................................................................................... 22
5.18 Software-controlled electronic devices and security .............................................................. 22
6 Bibliography ..................................................................................................................................... 25
Annex A Principles for sealing (Informative) ....................................................................................... 30
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OIML R 59-1:2016 (E)
Foreword
The International Organization of Legal Metrology (OIML) is a worldwide, intergovernmental
organization whose primary aim is to harmonize the regulations and metrological controls applied by
the national metrological services, or related organizations, of its Member States.
The main categories of OIML publications are:
• International Recommendations (OIML R), which are model regulations that establish the
metrological characteristics required of certain measuring instruments and which specify
methods and equipment for checking their conformity. OIML Member States shall implement
these Recommendations to the greatest possible extent;
• International Documents (OIML D), which are informative in nature and which are
intended to harmonize and improve work in the field of legal metrology;
• International Guides (OIML G), which are also informative in nature and which are
intended to give guidelines for the application of certain requirements to legal metrology; and
• International Basic Publications (OIML B), which define the operating rules of the various
OIML structures and systems.
OIML Draft Recommendations, Documents and Guides are developed by Project Groups linked to
Technical Committees or Subcommittees which comprise representatives from the Member States.
Certain international and regional institutions also participate on a consultation basis. Cooperative
agreements have been established between the OIML and certain institutions, such as ISO and the
IEC, with the objective of avoiding contradictory requirements. Consequently, manufacturers and
users of measuring instruments, test laboratories, etc. may simultaneously apply OIML publications
and those of other institutions.
International Recommendations, Documents, Guides and Basic Publications are published in English
(E) and translated into French (F) and are subject to periodic revision.
Additionally, the OIML publishes or participates in the publication of Vocabularies (OIML V) and
periodically commissions legal metrology experts to write Expert Reports (OIML E). Expert
Reports are intended to provide information and advice, and are written solely from the viewpoint of
their author, without the involvement of a Technical Committee or Subcommittee, nor that of the
CIML. Thus, they do not necessarily represent the views of the OIML.
This publication – reference OIML R 59-1, Edition 2016 – was developed by Project Group 1 in
OIML Technical Subcommittee TC 17/SC 1 Humidity. It was approved for final publication by the
International Committee of Legal Metrology in 2016 and was submitted to the International
Conference on Legal Metrology in 2016 for formal sanction. It supersedes the previous edition of R 59
dated 1984.
OIML Publications may be downloaded from the OIML website in the form of PDF files. Additional
information on OIML Publications may be obtained from the Organization’s headquarters:
Bureau International de Métrologie Légale
11, rue Turgot - 75009 Paris – France
Telephone: 33 (0)1 48 78 12 82
Fax: 33 (0)1 42 82 17 27
E-mail: [email protected]
Internet: www.oiml.org
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Introduction
1
Moisture content is one of the most critical grain quality measurements because of the direct
economic significance of the fraction of the total product weight that is water and because moisture
content largely determines the rates at which the grain will degrade during handling and storage. Grain
is bought and sold on the basis of weight. Accurate moisture determinations serve as the basis for
appropriate price adjustments.
1
If the moisture content is above the level that ensures safe storage, the grain must be dried to a
suitable level. The energy and handling costs associated with drying grain and the reduction in weight
of the grain during drying result in substantially reduced prices for high moisture grain.
Concomitantly, overly dry grain is discounted from its weight basis and this dockage is partially
justified by the increased susceptibility to breakage during handling for drier grain. The direct
discounts assessed for moist grain and the indirect penalty (giving away dry matter) for dry grain are
powerful inducements to deliver grain with a moisture content that is very close to the established safe
storage level. Because of its significance, moisture content is determined virtually every time grain is
bought and sold.
1
Many technologies have been applied to rapid grain moisture measurement. Rapid indirect methods
measure some physical parameter (such as electrical or optical sensing) and predict moisture content
using calibration equations or charts. These calibrations can change due to changes in crop varieties
planted and seasonal variation in climatic conditions. Invariably, other sample constituents or sample
geometry interfere with the signal caused by water. Temperature usually affects both the water signal
and the interfering signals. Therefore, calibration equations attempt to achieve a best fit between the
measured parameters and the moisture content as defined by an accepted moisture reference method.
Accurate grain moisture measurements depend upon successfully overcoming the effects of interfering
factors such as density, temperature, chemical composition and impurities.
This 2016 edition of OIML R 59 contains significant changes to the 1984 edition, notably to reflect
new measuring technologies and aspects of actual grain analysis.
As noted above, grain moisture meters do not measure moisture directly. An electrical or optical
response to the moisture in a grain type is measured and moisture is predicted using calibration
equations. As such, these instruments must be calibrated to predict the moisture of each grain type
used on the instrument. Grains vary from season to season and also grain types may vary widely from
country to country; therefore, a program to address calibration updates is needed to ensure that grain
moisture meter calibrations represent the current crops. If grain moisture instruments are sold to other
countries the calibrations will need to be verified within that country to ensure that the calibrations are
representative of the grains within that particular country. This Recommendation does not address an
ongoing calibration program for these instruments. Ongoing calibration programs may be subject to
metrological controls by the national responsible body.
1
An Investigation of the Nature of the Radio Frequency Dielectric Response in Cereal Grains and Oilseeds with
Engineering Implications for Grain Moisture Meters, A Dissertation in Physics and Engineering, David B.
Funk, Ph.D., D.H.C.
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1 Scope
1.2 Indications
This Recommendation applies to digitally indicating automatic grain moisture meters that directly
display moisture content.
1.3 Application
This Recommendation applies to moisture measuring instruments that estimate moisture based on
indirect physical means (e.g. electrical or optical sensing). Drying methods or any other direct
moisture measurement technology are not specifically covered, but may qualify if they perform to the
requirements of this Recommendation.
2 Terminology
2.1 Terminology in OIML V 2-200 International Vocabulary of Metrology – Basic and General
Concepts and Associated Terms (VIM) [1], and OIML V 1 International Vocabulary of Terms in Legal
Metrology (VIML) [2]
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Note 2: The term “measurement accuracy” should not be used for measurement trueness and the
term “measurement precision” should not be used for “measurement accuracy”, which,
however, is related to both concepts.
Note 3: ‘Measurement accuracy’ is sometimes understood as closeness of agreement between
measured quantity values that are being attributed to the measurand.
2.1.5 maximum permissible measurement error (MPE) (maximum permissible error, limit of
error) [VIM 4.26]
extreme value of measurement error, with respect to a known reference quantity value, permitted by
specifications or regulations for a given measurement, measuring instrument, or measuring system
Note 1: Usually the term “maximum permissible errors” or “limits of error” are used, where there are
two extreme values.
Note 2: The term “tolerance” should not be used to designate “maximum permissible error”.
Additional note: The MPEs in 4.4.2 of this Recommendation are errors associated with a meter in use
in the market place. The errors for the OIML test procedures are based on 4.4.1.
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2.3.9 grain
for the purpose of this Recommendation grain means oil seeds, pulses and cereal grains
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(c) transitory faults being momentary variations in the indication, which cannot be interpreted,
memorized or transmitted as a measurement result;
(d) faults giving rise to variations in the measurement result that are serious enough to be noticed
by all those interested in the measurement result; the relevant Recommendation may specify
the nature of these variations.
t minimum environmental temperature specified by the national responsible body for type testing
C
t maximum environmental temperature specified by the national responsible body for type testing
H
average of the difference between meter reading and reference method (see R 59-2, 2.3.1 and R 59-2,
3.13.11)
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3 Units of measurement
4 Metrological requirements
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1
An Investigation of the Nature of the Radio Frequency Dielectric Response in Cereal Grains and Oilseeds with
Engineering Implications for Grain Moisture Meters, A Dissertation in Physics and Engineering, David
B. Funk, Ph.D., D.H.C.
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All other If 0.02 × M < 0.35 0.5 × column 2 0.5 × column 2 0.6 × column 2
grains and oil then
seeds MPEs = 0.35; else
MPEs = 0.02 × M
(e.g. If M < 17.5 then
MPEs = 0.35; else
MPEs = 0.02 × M)
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5 Technical requirements
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5.10 Marking
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the meter, meter operating temperature range, voltage and frequency ranges, electromagnetic
interferences and electromagnetic compatibility. In addition, the manual shall be supplied to
the owner/user of the instrument in the official language(s) of the countries in which it is used
or in a language accepted by the national responsible body.
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accompanied in both cases by clear instructions on how to check the actual software identification
against the reference number (as listed in the OIML certificate) marked on or displayed by the
instrument.
5.18.4.1Calibration version
A meter shall be capable of displaying calibration constants, a unique calibration name, or a unique
calibration version number for use in verifying that the latest version of the calibration is being used to
make moisture content determinations.
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5.18.4.2Calibration protection
If calibration constants are digitally stored in an electronically alterable form, the meter shall be
designed to make automatic checks to detect unauthorized modification. An error message shall be
displayed if calibration constants have been electronically corrupted and no further measurement shall
be possible.
5.18.4.3Calibration transfer
The instrument hardware/software design and calibration procedures shall permit calibration
development and the transfer of calibrations between instruments of like models without requiring
user slope or bias adjustments.
5.18.6.1Prevention misuse
A measuring instrument, and especially the software, shall be constructed in such a way that
possibilities for unintentional, accidental or intentional misuse are minimal.
5.18.6.2Fraud protection
For protection against fraudulent use, the following requirements shall be fulfilled:
the legally relevant software shall be secured against unauthorized modification, loading, or
changes by swapping the memory device. In addition to mechanical sealing, technical means
may be necessary to secure measuring instruments having an operating system or an option to
load software. Only clearly documented functions are allowed to be activated by the user
interface, which shall be realized in such a way that it does not facilitate fraudulent use; and
parameters that fix the legally relevant characteristics of the measuring instrument shall be
secured against unauthorized modification. If necessary for the purpose of verification, it shall
be possible to display or print the current parameter settings.
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6 Bibliography
At the time of publication, the editions indicated were valid. All normative documents are subject to
revision, and the users of this Recommendation are encouraged to apply the most recent editions of the
normative documents indicated below. Members of the IEC and ISO maintain registers of currently
valid International Standards.
The actual status of the Standards referred to can also be found on the Internet:
• IEC Publications: http://www.iec.ch/searchpub/cur_fut.htm
• ISO Publications: http://www.iso.org/iso/iso_catalogue.htm
• OIML Publications: http://www.oiml.org/en/publications/recommendations
(with free download of PDF files).
In order to avoid any misunderstanding, it is highly recommended that all references to Standards in
OIML Recommendations and Documents be followed by the version referred to (generally the year or
date).
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Annex A
Principles for sealing
(Informative)
This Annex highlights considerations for determining which parameters of a grain moisture measuring
instrument require sealing. It also provides examples of sealing methods, such as metrological audit
trails, and the minimum requirements for an effective seal.
A.1.2 adjustment
change in the value of the sealable calibration parameters or the sealable configuration parameters of
an instrument
A.1.5 event
while in adjustment mode, an action in which
one or more changes are made to configuration parameters, or
adjustments are made to one value (or values for a set of values) for a calibration parameter
(e.g. adjustments for a set of calibration factors to linearize device output)
If no adjustment is made, then there is no event. In the case of a centralized audit trail, the same values
for the same parameter sent to multiple devices shall be considered to be the same event. In the case of
a centralized event logger, the event logger must identify both the device and the parameter that was
changed.
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A.1.12 seal
as a verb, to seal a device is to make a device secure so that access to adjustments and other sealable
parameters will be detectable
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For parameters protected by physical means of security, once a physical security seal is applied to the
instrument it should not be possible to make a metrological change to those parameters without
breaking that seal. For parameters protected by electronic means of security, it shall not be possible to
make a metrological change to those parameters without that change being reflected in an audit trail.
Since this philosophy addresses provisions for protecting access to any metrological adjustment, the
philosophy should be applied consistently to all electronic device types.
If a device must undergo a physical act, such as cutting a wire and physically repairing the cut to
reactivate the parameter, then this physical repair process would be considered an acceptable way to
select parameters without requiring a physical seal or an audit trail.
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Note: The above examples of adjustments, parameters and features to be sealed are to be considered
“typical” or “normal”. This list may not be all-inclusive, and there may be other parameters
which affect the metrological performance of the device and which must, therefore, be sealed.
If listed parameters or other parameters which may affect the metrological function of the
device are not sealed, the manufacturer must demonstrate that all settings comply with the
most stringent requirements for the application of the device.
A.4.1 Scope
The ability of users to make changes that affect the metrological integrity of the device (e.g. slope,
bias, etc.) in normal operation and the remote configuration capability of commercial moisture
measuring instruments has led to new, more appropriate means of sealing being implemented. These
instruments must either be physically sealed or must incorporate an approved form of audit trail.
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Included below are the requirements for the acceptable forms of metrological audit trail, which are
recognized as providing acceptable security.
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2) Accessing the audit trail information shall not affect the normal operation of a device
before or after accessing the information.
3) A key (for a panel lock) may be required to gain access to the means to view the contents
of the audit trail. Access may be through the supervisor’s mode of operation of the device.
4) Accessing the audit trail information shall not require the removal of any additional parts
other than normal requirements to inspect the integrity of a physical seal.
(g) The printed form of the audit trail information shall be readily interpretable by an official.
(h) The information from an event logger shall be printed in order from the most recent event to
the oldest event. If a device is not capable of printing all the information for a single event on
one line or at one time, the information shall be displayed in blocks of information, which are
readily understandable.
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