History,01,01,4

Sievers 500 RL TOC Analyzer

Calibration History
Serial Number,3024
Location,PW
Date,14 DEC 2021 14:46

Result,02,002
Single Point Calibration Results
Run Date,21 OCT 2020 15:10
User ID,
Version,2.13,Rev,001

Vial Set Part Number,STD 74501

SiOS Calibration Set A
Vial Set Lot Number,20267-5955
Expires,18 NOV 2020

Vial,Part#,Lot,Expiration Date
1,STD 74008,20267-5955,18 NOV 2020
2,STD 74000,20267-5955,18 NOV 2020
3,STD 74150,20267-5955,18 NOV 2020
4,STD 77035,20267-5955,18 NOV 2020

Vial,Rep,Time,Reject,TOC(ppb),IC(ppb),TC(ppb)
1,1,21 OCT 2020 15:27:41,Y,-1.65,194,192
1,2,21 OCT 2020 15:33:41,Y,2.49,192,194
1,3,21 OCT 2020 15:39:41,Y,2.23,194,196
1,4,21 OCT 2020 15:45:41,Y,2.86,194,197
1,5,21 OCT 2020 15:51:41,Y,2.90,193,196
1,6,21 OCT 2020 15:57:41,Y,2.00,193,195
1,7,21 OCT 2020 16:03:41,Y,1.38,192,193
1,8,21 OCT 2020 16:09:41,N,1.13,190,191
1,9,21 OCT 2020 16:15:41,N,0.90,189,190
1,10,21 OCT 2020 16:21:41,N,0.41,187,187
2,1,21 OCT 2020 16:35:57,Y,8.27,185,193
2,2,21 OCT 2020 16:41:57,N,12.4,181,193
2,3,21 OCT 2020 16:47:57,N,12.8,181,194
2,4,21 OCT 2020 16:53:57,N,12.9,180,193
3,1,21 OCT 2020 17:08:16,Y,1500,197,1700
3,2,21 OCT 2020 17:14:16,N,1520,193,1710
3,3,21 OCT 2020 17:20:16,N,1500,187,1690
3,4,21 OCT 2020 17:26:16,N,1510,187,1700

Vial,Rep,Time,Reject,Cond25.00(uS/cm)
S1_4,1,21 OCT 2020 17:40:32,Y,24.82
S1_4,2,21 OCT 2020 17:46:32,N,25.03
S1_4,3,21 OCT 2020 17:52:32,N,24.85
S1_4,4,21 OCT 2020 17:58:32,N,24.97

Rep,RW IC,RW2 TOC,1.50ppm TOC

1,190 ppb,12.4ppb,1.52ppm
2,189 ppb,12.8ppb,1.50ppm
3,187 ppb,12.9ppb,1.51ppm
Avg,189 ppb,12.7ppb,1.51ppm
Exp,190 ppb,,1.51ppm
Diff,-0.53%,,0.00%
Adj,190 ppb,12.0ppb,1.51ppm
Rep,25.00uS/cm tCond
1,25.03uS/cm
2,24.85uS/cm
3,24.97uS/cm
Avg,24.95uS/cm
Exp,25.00uS/cm
Diff,-0.20%
Adj,25.00uS/cm

Single Point Cal,Pass

Result,02,002
Single Point Calibration Results
Run Date,13 DEC 2021 12:56
User ID,
Version,2.15,Rev,003

Vial Set Part Number,STD 74501

SiOS Calibration Set A
Vial Set Lot Number,21322-5324
Expires,24 FEB 2022

Vial,Part#,Lot,Expiration Date
1,STD 74008,21322-5324,24 FEB 2022
2,STD 74000,21322-5324,24 FEB 2022
3,STD 74150,21322-5324,24 FEB 2022
4,STD 77035,21322-5324,24 FEB 2022

Vial,Rep,Time,Reject,TOC(ppb),IC(ppb),TC(ppb)
1,1,13 DEC 2021 13:13:26,Y,-15.0,210,195
1,2,13 DEC 2021 13:19:26,Y,-10.4,206,196
1,3,13 DEC 2021 13:25:26,Y,-10.3,203,193
1,4,13 DEC 2021 13:31:26,Y,-10.3,202,192
1,5,13 DEC 2021 13:37:26,Y,-10.1,200,190
1,6,13 DEC 2021 13:43:26,Y,-10.1,199,189
1,7,13 DEC 2021 13:49:26,Y,-10.1,197,187
1,8,13 DEC 2021 13:55:26,N,-10.3,195,185
1,9,13 DEC 2021 14:01:26,N,-10.5,194,184
1,10,13 DEC 2021 14:07:26,N,-10.5,192,182
2,1,13 DEC 2021 14:21:42,Y,24.4,197,221
2,2,13 DEC 2021 14:27:42,N,25.3,194,219
2,3,13 DEC 2021 14:33:42,N,25.4,194,219
2,4,13 DEC 2021 14:39:42,N,21.1,194,215
3,1,13 DEC 2021 14:54:01,Y,1510,219,1730
3,2,13 DEC 2021 15:00:01,N,1520,216,1740
3,3,13 DEC 2021 15:06:01,N,1520,214,1730
3,4,13 DEC 2021 15:12:01,N,1520,211,1730

Vial,Rep,Time,Reject,Cond25.00(uS/cm)
S1_4,1,13 DEC 2021 15:26:17,Y,24.82
S1_4,2,13 DEC 2021 15:32:17,N,24.68
S1_4,3,13 DEC 2021 15:38:17,N,24.62
S1_4,4,13 DEC 2021 15:44:17,N,24.78

Rep,RW IC,RW2 TOC,1.50ppm TOC

1,195 ppb,25.3ppb,1.52ppm
2,194 ppb,25.4ppb,1.52ppm
3,192 ppb,21.1ppb,1.52ppm
Avg,194 ppb,23.9ppb,1.52ppm
Exp,184 ppb,,1.53ppm
Diff,5.43%,,-0.65%
Adj,184 ppb,34.3ppb,1.53ppm

Rep,25.00uS/cm tCond
1,24.68uS/cm
2,24.62uS/cm
3,24.78uS/cm
Avg,24.69uS/cm
Exp,25.00uS/cm
Diff,-1.24%
Adj,25.00uS/cm

Single Point Cal,Fail

Result,02,002
Single Point Calibration Results
Run Date,13 DEC 2021 15:50
User ID,
Version,2.15,Rev,003

Vial Set Part Number,STD 74501

SiOS Calibration Set A
Vial Set Lot Number,21322-5324
Expires,24 FEB 2022

Vial,Part#,Lot,Expiration Date
1,STD 74008,21322-5324,24 FEB 2022
2,STD 74000,21322-5324,24 FEB 2022
3,STD 74150,21322-5324,24 FEB 2022
4,STD 77035,21322-5324,24 FEB 2022

Vial,Rep,Time,Reject,TOC(ppb),IC(ppb),TC(ppb)
1,1,13 DEC 2021 16:07:27,Y,-2.67,177,174
1,2,13 DEC 2021 16:13:27,Y,1.96,173,175
1,3,13 DEC 2021 16:19:27,Y,2.21,172,174
1,4,13 DEC 2021 16:25:27,Y,1.85,171,173
1,5,13 DEC 2021 16:31:27,Y,1.71,170,172
1,6,13 DEC 2021 16:37:27,Y,1.59,169,171
1,7,13 DEC 2021 16:43:27,Y,1.44,168,169
1,8,13 DEC 2021 16:49:27,N,1.23,168,169
1,9,13 DEC 2021 16:55:27,N,1.20,167,168
1,10,13 DEC 2021 17:01:27,N,1.08,166,167
2,1,13 DEC 2021 17:15:43,Y,31.5,176,208
2,2,13 DEC 2021 17:21:43,N,34.1,174,208
2,3,13 DEC 2021 17:27:43,N,34.6,173,208
2,4,13 DEC 2021 17:33:43,N,36.9,172,209
3,1,13 DEC 2021 17:48:02,Y,1520,189,1710
3,2,13 DEC 2021 17:54:02,N,1530,186,1720
3,3,13 DEC 2021 18:00:02,N,1540,185,1730
3,4,13 DEC 2021 18:06:02,N,1540,183,1720

Vial,Rep,Time,Reject,Cond25.00(uS/cm)
S1_4,1,13 DEC 2021 18:20:18,Y,25.22
S1_4,2,13 DEC 2021 18:26:18,N,24.75
S1_4,3,13 DEC 2021 18:32:18,N,25.08
S1_4,4,13 DEC 2021 18:38:18,N,24.92

Rep,RW IC,RW2 TOC,1.50ppm TOC

1,168 ppb,34.1ppb,1.53ppm
2,167 ppb,34.6ppb,1.54ppm
3,166 ppb,36.9ppb,1.54ppm
Avg,167 ppb,35.2ppb,1.54ppm
Exp,168 ppb,,1.53ppm
Diff,-0.60%,,0.65%
Adj,168 ppb,34.0ppb,1.53ppm

Rep,25.00uS/cm tCond
1,24.75uS/cm
2,25.08uS/cm
3,24.92uS/cm
Avg,24.92uS/cm
Exp,25.00uS/cm
Diff,-0.32%
Adj,25.00uS/cm

Single Point Cal,Pass

Result,05,002
Linearity Results
Run Date,23 OCT 2020 10:48
User ID,
Version,2.13,Rev,001

Vial Set Part Number,STD 74506

Linearity Set
Vial Set Lot Number,20268-5975
Expires,19 NOV 2020
Vial,Part#,Lot,Expiration Date
1,STD 74075,20268-5975,19 NOV 2020
2,STD 74050,20268-5975,19 NOV 2020
3,STD 74025,20268-5975,19 NOV 2020
4,STD 74000,20268-5975,19 NOV 2020

Vial,Rep,Time,Reject,TOC(ppb),IC(ppb),TC(ppb)
1,1,23 OCT 2020 11:04:55,Y,765,74.0,839
1,2,23 OCT 2020 11:10:55,N,768,76.6,845
1,3,23 OCT 2020 11:16:55,N,772,80.6,853
1,4,23 OCT 2020 11:22:55,N,774,84.3,858
2,1,23 OCT 2020 11:37:10,Y,521,67.5,589
2,2,23 OCT 2020 11:43:10,N,527,70.0,597
2,3,23 OCT 2020 11:49:10,N,532,73.6,606
2,4,23 OCT 2020 11:55:10,N,529,77.0,606
3,1,23 OCT 2020 12:09:25,Y,275,40.0,315
3,2,23 OCT 2020 12:15:25,N,278,42.7,321
3,3,23 OCT 2020 12:21:25,N,277,46.7,324
3,4,23 OCT 2020 12:27:25,N,279,50.7,330
4,1,23 OCT 2020 12:41:40,Y,20.1,31.6,51.7
4,2,23 OCT 2020 12:47:40,N,22.9,35.2,58.1
4,3,23 OCT 2020 12:53:40,N,20.5,39.2,59.7
4,4,23 OCT 2020 12:59:40,N,20.5,43.6,64.1

,750 ppb,500 ppb,250 ppb,RW

Avg,750 ppb,508 ppb,257 ppb,21.3ppb

R2,1.00,Pass
Slope,1.01
Intercept,-12.10
,750 ppb,500 ppb,250 ppb,RW
Avg,771 ppb,529 ppb,278 ppb,21.3ppb
SD,3.06ppb,2.52ppb,1.00ppb,1.39ppb

Intercept,0.00
LOD,0.00
LOQ,0.00

Result,03,004
Acc/Prec/Ver Results
Run Date,05 MAY 2021 12:01
User ID,
Version,2.13,Rev,001

Vial Set Part Number,STD 74502

Accuracy/Precision/Verification Set
Vial Set Lot Number,20265-5930
Expires,16 NOV 2020
Vial,Part#,Lot,Expiration Date
2,STD 74000,20265-5930,16 NOV 2020
3,STD 74055,20265-5930,16 NOV 2020
4,STD 77035,20265-5930,16 NOV 2020

Vial,Rep,Time,Reject,TOC(ppb),IC(ppb),TC(ppb)
2,1,05 MAY 2021 12:18:41,Y,60.3,36.4,96.7
2,2,05 MAY 2021 12:24:41,Y,33.5,42.3,75.8
2,3,05 MAY 2021 12:30:41,Y,30.6,47.0,77.6
2,4,05 MAY 2021 12:36:41,Y,34.6,51.7,86.3
2,5,05 MAY 2021 12:42:41,Y,22.0,56.5,78.5
2,6,05 MAY 2021 12:48:41,Y,12.6,60.9,73.5
2,7,05 MAY 2021 12:54:41,Y,16.1,65.8,81.9
2,8,05 MAY 2021 13:00:41,N,16.3,70.9,87.2
2,9,05 MAY 2021 13:06:41,N,20.6,76.1,96.7
2,10,05 MAY 2021 13:12:41,N,8.10,80.0,88.1
3,1,05 MAY 2021 13:27:00,Y,479,31.6,511
3,2,05 MAY 2021 13:33:00,N,484,37.7,522
3,3,05 MAY 2021 13:39:00,N,485,43.3,528
3,4,05 MAY 2021 13:45:00,N,485,47.8,533

Vial,Rep,Time,Reject,Cond25.00(uS/cm)
4,1,05 MAY 2021 13:59:16,Y,24.77
4,2,05 MAY 2021 14:05:16,N,25.27
4,3,05 MAY 2021 14:11:16,N,24.85
4,4,05 MAY 2021 14:17:16,N,25.01

,RW,500 ppb,25.00uS/cm
Rep,TOC,TOC,tCond
1,16.3ppb,484 ppb,25.27uS/cm
2,20.6ppb,485 ppb,24.85uS/cm
3,8.10ppb,485 ppb,25.01uS/cm
Avg,15.0ppb,485 ppb,25.04uS/cm

Rw Avg(ppb),15.0
Rw Adj Std Concentration(ppb),515

TOC Avg(ppb),485
TOC SD(ppb),0.58
TOC RSD,0.12%,Pass
TOC Accuracy,-5.83%,Pass

Cond Avg(uS/cm),25.04
Cond SD(uS/cm),0.212
Cond RSD,0.85%,Pass
Cond Accuracy,0.16%,Pass

Result,03,004
Acc/Prec/Ver Results
Run Date,05 MAY 2021 14:21
User ID,
Version,2.13,Rev,001

Vial Set Part Number,STD 74502

Accuracy/Precision/Verification Set
Vial Set Lot Number,21095-1569
Expires,31 MAY 2021
Vial,Part#,Lot,Expiration Date
2,STD 74000,21095-1569,31 MAY 2021
3,STD 74055,21095-1569,31 MAY 2021
4,STD 77035,21095-1569,31 MAY 2021

Vial,Rep,Time,Reject,TOC(ppb),IC(ppb),TC(ppb)
2,1,05 MAY 2021 14:38:08,Y,1.61,62.2,63.8
2,2,05 MAY 2021 14:44:08,Y,2.69,66.2,68.9
2,3,05 MAY 2021 14:50:08,Y,2.17,69.8,72.0
2,4,05 MAY 2021 14:56:08,Y,-1.14,73.9,72.8
2,5,05 MAY 2021 15:02:08,Y,1.72,78.1,79.8
2,6,05 MAY 2021 15:08:08,Y,-0.16,82.2,82.0
2,7,05 MAY 2021 15:14:08,Y,-0.34,86.2,85.9
2,8,05 MAY 2021 15:20:08,N,4.92,90.6,95.5
2,9,05 MAY 2021 15:26:08,N,1.12,93.4,94.5
2,10,05 MAY 2021 15:32:08,N,0.25,96.8,97.1
3,1,05 MAY 2021 15:46:27,Y,481,53.3,534
3,2,05 MAY 2021 15:52:27,N,492,57.3,549
3,3,05 MAY 2021 15:58:27,N,496,61.3,557
3,4,05 MAY 2021 16:04:27,N,491,65.1,556

Vial,Rep,Time,Reject,Cond25.00(uS/cm)
4,1,05 MAY 2021 16:18:43,Y,25.16
4,2,05 MAY 2021 16:24:43,N,25.14
4,3,05 MAY 2021 16:30:43,N,25.10
4,4,05 MAY 2021 16:36:43,N,25.05

,RW,500 ppb,25.00uS/cm
Rep,TOC,TOC,tCond
1,4.92ppb,492 ppb,25.14uS/cm
2,1.12ppb,496 ppb,25.10uS/cm
3,0.25ppb,491 ppb,25.05uS/cm
Avg,2.10ppb,493 ppb,25.10uS/cm

Rw Avg(ppb),2.10
Rw Adj Std Concentration(ppb),502

TOC Avg(ppb),493
TOC SD(ppb),2.65
TOC RSD,0.54%,Pass
TOC Accuracy,-1.79%,Pass
Cond Avg(uS/cm),25.10
Cond SD(uS/cm),0.045
Cond RSD,0.18%,Pass
Cond Accuracy,0.40%,Pass

Result,03,004
Acc/Prec/Ver Results
Run Date,14 DEC 2021 12:10
User ID,
Version,2.15,Rev,003

Vial Set Part Number,STD 74502

Accuracy/Precision/Verification Set
Vial Set Lot Number,21333-5437
Expires,07 MAR 2022
Vial,Part#,Lot,Expiration Date
2,STD 74000,21333-5437,07 MAR 2022
3,STD 74055,21333-5437,07 MAR 2022
4,STD 77035,21333-5437,07 MAR 2022

Vial,Rep,Time,Reject,TOC(ppb),IC(ppb),TC(ppb)
2,1,14 DEC 2021 12:27:36,Y,26.8,102,129
2,2,14 DEC 2021 12:33:36,Y,20.0,104,124
2,3,14 DEC 2021 12:39:36,Y,18.3,107,125
2,4,14 DEC 2021 12:45:36,Y,18.0,109,127
2,5,14 DEC 2021 12:51:36,Y,14.3,112,126
2,6,14 DEC 2021 12:57:36,Y,15.0,114,129
2,7,14 DEC 2021 13:03:36,Y,13.0,115,128
2,8,14 DEC 2021 13:09:36,N,13.8,117,131
2,9,14 DEC 2021 13:15:36,N,15.2,118,133
2,10,14 DEC 2021 13:21:36,N,18.1,120,138
3,1,14 DEC 2021 13:35:55,Y,501,107,608
3,2,14 DEC 2021 13:41:55,N,505,107,612
3,3,14 DEC 2021 13:47:55,N,503,109,612
3,4,14 DEC 2021 13:53:55,N,505,111,616

Vial,Rep,Time,Reject,Cond25.00(uS/cm)
4,1,14 DEC 2021 14:08:11,Y,25.26
4,2,14 DEC 2021 14:14:11,N,24.42
4,3,14 DEC 2021 14:20:11,N,25.13
4,4,14 DEC 2021 14:26:11,N,25.09

,RW,500 ppb,25.00uS/cm
Rep,TOC,TOC,tCond
1,13.8ppb,505 ppb,24.42uS/cm
2,15.2ppb,503 ppb,25.13uS/cm
3,18.1ppb,505 ppb,25.09uS/cm
Avg,15.7ppb,504 ppb,24.88uS/cm

Rw Avg(ppb),15.7
Rw Adj Std Concentration(ppb),516

TOC Avg(ppb),504
TOC SD(ppb),1.15
TOC RSD,0.23%,Pass
TOC Accuracy,-2.33%,Pass

Cond Avg(uS/cm),24.88
Cond SD(uS/cm),0.399
Cond RSD,1.60%,Pass
Cond Accuracy,-0.48%,Pass

Result,04,002
System Suitability Results
Run Date,01 MAR 2013 11:15
User ID,
Version,2.13,Rev,001

Vial Set Part Number,

Vial Set Lot Number,

Expires,
Vial,Part#,Lot,Expiration Date
1,,,
2,,,
3,,,
4,,,

Vial,Rep,Time,Reject,TOC(ppb),IC(ppb),TC(ppb)
1,1,01 MAR 2013 11:33:40,Y,44.3,163,207
1,2,01 MAR 2013 11:39:40,Y,42.9,164,207
1,3,01 MAR 2013 11:45:40,Y,35.5,166,202
1,4,01 MAR 2013 11:51:40,Y,28.8,167,196
1,5,01 MAR 2013 11:57:40,Y,27.0,168,195
1,6,01 MAR 2013 12:03:40,Y,30.4,169,199
1,7,01 MAR 2013 12:09:40,Y,26.9,169,196
1,8,01 MAR 2013 12:15:40,N,26.8,170,197
1,9,01 MAR 2013 12:21:40,N,28.5,169,198
1,10,01 MAR 2013 12:27:40,N,27.6,169,197
2,1,01 MAR 2013 12:41:58,Y,541,177,718
2,2,01 MAR 2013 12:47:58,N,549,174,723
2,3,01 MAR 2013 12:53:58,N,548,174,722
2,4,01 MAR 2013 12:59:58,N,552,174,726
3,1,01 MAR 2013 13:14:13,Y,531,191,722
3,2,01 MAR 2013 13:20:13,N,550,188,738
3,3,01 MAR 2013 13:26:13,N,538,188,726
3,4,01 MAR 2013 13:32:13,N,539,187,726

Rw(ppb),27.6
Rs(ppb),550
Rss(ppb),542

Response Efficiency,98.5%,Pass
Response Limit(ppb),522

Result,04,002
System Suitability Results
Run Date,22 OCT 2020 13:45
User ID,
Version,2.13,Rev,001

Vial Set Part Number,STD 74503

System Suitability Set
Vial Set Lot Number,20268-5973
Expires,17 DEC 2020
Vial,Part#,Lot,Expiration Date
1,STD 74000,20268-5973,17 DEC 2020
2,STD 74054,20268-5973,17 DEC 2020
3,STD 74058,20268-5973,17 DEC 2020
4,STD 74004,20268-5973,17 DEC 2020

Vial,Rep,Time,Reject,TOC(ppb),IC(ppb),TC(ppb)
1,1,22 OCT 2020 14:02:06,Y,21.2,44.8,66.0
1,2,22 OCT 2020 14:08:06,Y,23.5,47.9,71.4
1,3,22 OCT 2020 14:14:06,Y,24.8,52.3,77.1
1,4,22 OCT 2020 14:20:06,Y,25.3,57.0,82.3
1,5,22 OCT 2020 14:26:06,Y,24.3,61.8,86.1
1,6,22 OCT 2020 14:32:06,Y,25.5,66.4,91.9
1,7,22 OCT 2020 14:38:06,Y,24.1,70.6,94.7
1,8,22 OCT 2020 14:44:06,N,24.4,75.4,99.8
1,9,22 OCT 2020 14:50:06,N,23.4,79.7,103
1,10,22 OCT 2020 14:56:06,N,24.0,83.8,108
2,1,22 OCT 2020 15:10:24,Y,504,52.1,556
2,2,22 OCT 2020 15:16:24,N,512,54.9,567
2,3,22 OCT 2020 15:22:24,N,518,59.0,577
2,4,22 OCT 2020 15:28:24,N,525,63.0,588
3,1,22 OCT 2020 15:42:39,Y,511,49.7,561
3,2,22 OCT 2020 15:48:39,N,519,53.0,572
3,3,22 OCT 2020 15:54:39,N,521,57.0,578
3,4,22 OCT 2020 16:00:39,N,521,60.8,582

Rw(ppb),23.9
Rs(ppb),518
Rss(ppb),520

Response Efficiency, 100%,Pass

Response Limit(ppb),494

Result,04,002
System Suitability Results
Run Date,06 MAY 2021 09:53
User ID,
Version,2.13,Rev,001

Vial Set Part Number,STD 74503

System Suitability Set
Vial Set Lot Number,21092-1557
Expires,25 JUN 2021
Vial,Part#,Lot,Expiration Date
1,STD 74000,21092-1557,25 JUN 2021
2,STD 74054,21092-1557,25 JUN 2021
3,STD 74058,21092-1557,25 JUN 2021
4,STD 74004,21092-1557,25 JUN 2021

Vial,Rep,Time,Reject,TOC(ppb),IC(ppb),TC(ppb)
1,1,06 MAY 2021 10:14:28,Y,0.28,68.2,68.5
1,2,06 MAY 2021 10:20:28,Y,-0.59,72.6,72.0
1,3,06 MAY 2021 10:26:28,Y,-0.49,75.8,75.3
1,4,06 MAY 2021 10:32:28,Y,-0.10,79.1,79.0
1,5,06 MAY 2021 10:38:28,Y,0.71,82.3,83.0
1,6,06 MAY 2021 10:44:28,Y,1.42,85.6,87.0
1,7,06 MAY 2021 10:50:28,Y,2.36,89.2,91.6
1,8,06 MAY 2021 10:56:28,N,3.33,92.7,96.0
1,9,06 MAY 2021 11:02:28,N,4.04,96.5,101
1,10,06 MAY 2021 11:08:28,N,4.71,99.6,104
2,1,06 MAY 2021 11:22:46,Y,501,66.3,567
2,2,06 MAY 2021 11:28:46,N,504,70.3,574
2,3,06 MAY 2021 11:34:46,N,506,73.7,580
2,4,06 MAY 2021 11:40:46,N,507,76.9,584
3,1,06 MAY 2021 11:55:01,Y,494,75.9,570
3,2,06 MAY 2021 12:01:01,N,499,79.4,578
3,3,06 MAY 2021 12:07:01,N,501,82.4,583
3,4,06 MAY 2021 12:13:01,N,501,85.3,586

Rw(ppb),4.03
Rs(ppb),506
Rss(ppb),500

Response Efficiency,98.8%,Pass
Response Limit(ppb),502

Result,04,002
System Suitability Results
Run Date,14 DEC 2021 08:51
User ID,
Version,2.15,Rev,003

Vial Set Part Number,STD 74503

System Suitability Set
Vial Set Lot Number,21328-5420
Expires,02 MAR 2022
Vial,Part#,Lot,Expiration Date
1,STD 74000,21328-5420,02 MAR 2022
2,STD 74054,21328-5420,02 MAR 2022
3,STD 74058,21328-5420,02 MAR 2022
4,STD 74004,21328-5420,02 MAR 2022

Vial,Rep,Time,Reject,TOC(ppb),IC(ppb),TC(ppb)
1,1,14 DEC 2021 09:34:50,Y,33.4,66.7,100
1,2,14 DEC 2021 09:40:50,Y,21.9,70.0,91.9
1,3,14 DEC 2021 09:46:50,Y,26.1,73.4,99.5
1,4,14 DEC 2021 09:52:50,Y,20.5,76.8,97.3
1,5,14 DEC 2021 09:58:50,Y,19.4,80.1,99.5
1,6,14 DEC 2021 10:04:50,Y,21.3,83.7,105
1,7,14 DEC 2021 10:10:50,Y,24.5,87.0,112
1,8,14 DEC 2021 10:16:50,N,20.1,90.2,110
1,9,14 DEC 2021 10:22:50,N,17.8,94.2,112
1,10,14 DEC 2021 10:28:50,N,21.9,97.3,119
2,1,14 DEC 2021 10:43:08,Y,499,67.3,566
2,2,14 DEC 2021 10:49:08,N,503,69.6,573
2,3,14 DEC 2021 10:55:08,N,504,72.9,577
2,4,14 DEC 2021 11:01:08,N,522,76.1,598
3,1,14 DEC 2021 11:15:23,Y,469,89.3,558
3,2,14 DEC 2021 11:21:23,N,474,91.1,565
3,3,14 DEC 2021 11:27:23,N,475,94.6,570
3,4,14 DEC 2021 11:33:23,N,476,97.5,574

Rw(ppb),19.9
Rs(ppb),510
Rss(ppb),475

Response Efficiency,92.9%,Pass
Response Limit(ppb),490

Result,10,002
Specificity Results
Run Date,26 OCT 2020 09:22
User ID,
Version,2.13,Rev,001

Vial Set Part Number,STD 74509

Specificity Set
Vial Set Lot Number,20259-5833
Expires,10 NOV 2020
Vial,Part#,Lot,Expiration Date
1,STD 74000,20259-5833,10 NOV 2020
2,STD 74059,20259-5833,10 NOV 2020
3,STD 74060,20259-5833,10 NOV 2020
4,STD 74050,20259-5833,10 NOV 2020

Vial,Rep,Time,Reject,TOC(ppb),IC(ppb),TC(ppb)
1,1,26 OCT 2020 09:39:22,Y,14.6,19.0,33.6
1,2,26 OCT 2020 09:45:22,Y,16.7,21.0,37.7
1,3,26 OCT 2020 09:51:22,Y,18.6,27.1,45.7
1,4,26 OCT 2020 09:57:22,Y,18.8,35.5,54.3
1,5,26 OCT 2020 10:03:22,Y,17.3,42.0,59.3
1,6,26 OCT 2020 10:09:22,Y,17.8,47.0,64.8
1,7,26 OCT 2020 10:15:22,Y,17.6,52.5,70.1
1,8,26 OCT 2020 10:21:22,N,18.4,57.0,75.4
1,9,26 OCT 2020 10:27:22,N,17.8,62.1,79.9
1,10,26 OCT 2020 10:33:22,N,18.1,66.5,84.6
2,1,26 OCT 2020 10:47:40,Y,504,28.4,532
2,2,26 OCT 2020 10:53:40,N,511,32.5,544
2,3,26 OCT 2020 10:59:40,N,514,37.5,552
2,4,26 OCT 2020 11:05:40,N,518,42.3,560
3,1,26 OCT 2020 11:19:55,Y,494,28.6,523
3,2,26 OCT 2020 11:25:55,N,499,32.2,531
3,3,26 OCT 2020 11:31:55,N,500,36.8,537
3,4,26 OCT 2020 11:37:55,N,501,41.6,543
4,1,26 OCT 2020 11:52:10,Y,507,25.8,533
4,2,26 OCT 2020 11:58:10,N,490,26.4,516
4,3,26 OCT 2020 12:04:10,N,493,29.5,523
4,4,26 OCT 2020 12:10:10,N,494,33.1,527

Blank(ppb),18.1
,Methanol,Nicotinamide,KHP
TOC,514 ppb,500 ppb,492 ppb
S.D.,3.51 ppb,1.00 ppb,2.08 ppb
R.S.D.,0.68 %,0.20 %,0.42 %
Percent Recovery,99.2 %,96.5 %,95.0 %

Specificity Pass/Fail,Pass

Result,11,002
Robustness Results
Run Date,23 OCT 2020 13:28
User ID,
Version,2.13,Rev,001

Vial Set Part Number,STD 74508

Robustness Set
Vial Set Lot Number,20254-5758
Expires,05 NOV 2020
Vial,Part#,Lot,Expiration Date
1,STD 74004,20254-5758,05 NOV 2020
2,STD 97701,20254-5758,05 NOV 2020
3,STD 97702,20254-5758,05 NOV 2020
4,STD 97703,20254-5758,05 NOV 2020

Vial,Rep,Time,Reject,TOC(ppb),IC(ppb),TC(ppb)
1,1,23 OCT 2020 13:45:09,Y,13.3,77.7,91.0
1,2,23 OCT 2020 13:51:09,Y,16.2,80.0,96.2
1,3,23 OCT 2020 13:57:09,Y,16.8,84.4,101
1,4,23 OCT 2020 14:03:09,Y,18.3,88.8,107
1,5,23 OCT 2020 14:09:09,Y,17.5,94.0,112
1,6,23 OCT 2020 14:15:09,N,19.0,99.1,118
1,7,23 OCT 2020 14:21:09,N,18.3,104,122
1,8,23 OCT 2020 14:27:09,N,18.4,108,126
2,1,23 OCT 2020 14:41:27,Y,489,52.9,542
2,2,23 OCT 2020 14:47:27,N,497,57.8,555
2,3,23 OCT 2020 14:53:27,N,500,63.4,563
2,4,23 OCT 2020 14:59:27,N,501,69.4,570
3,1,23 OCT 2020 15:13:42,Y,504,51.0,555
3,2,23 OCT 2020 15:19:42,N,509,55.9,565
3,3,23 OCT 2020 15:25:42,N,511,61.6,573
3,4,23 OCT 2020 15:31:42,N,512,68.0,580

Rw(ppb),18.6
Rs(ppb),499
Rss(ppb),511

Relative Recovery, 102%,Pass