Fatigue Behavior of Ceramic Matrix composites

Presented by

NITHIN K [email protected]
8 April 2013 1

Introduction

The fracture resistance of CMCs under cyclic conditions needs to be evaluated for design in a variety of potential structural applications. The density and penetration of matrix cracks was more under cyclic loading than under static loading conditions. Also, under static loading this CMC showed higher work of fracture than under cyclic loading .

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T.K.Sivakumar - 2010274014

Prewos Work
(the tensile fatigue behavior of Nicalon-type silicon carbide fiber reinforced lithium aluminosilicate (LAS) glass-ceramic composite)

They used two different types of LAS as the matrix materials: one showed a linear tensile stress- strain curve to failure (LAS-I) while the other showed a markedly nonlinear behavior due to extensive matrix cracking prior to ultimate failure(LAS - II). The residual tensile strength and elastic modulus of the LAS I composite after fatigue was the same as that of as-fabricated composite. In the LAS II composite, cycling below the proportional limit produced the same result. However, on cycling to stress levels higher than the proportional limit, a second linear stress-strain region having a modules less than the initial modules was observed . This change in behavior was due to the matrix micro-cracking at stress above the proportional limit.
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8 April 2013

Prewos Work
(the tensile fatigue behavior of Nicalon-type silicon carbide fiber reinforced lithium aluminosilicate (LAS) glass-ceramic composite)

Fatigue crack growth in variety of brittle solids in the compression, tension, and tension-compression fatigue shows that mechanical fatigue effects, i.e., due to cyclic loading, occur at room temperature in brittle solids as well. A variety of mechanisms such as micro cracking, dislocation plasticity , stress or strain- induced phase transformations, interfacial slip, and creep cavitation can promote an inelastic constitutive response in brittle solids of all kinds under compressive cycling.

8 April 2013

T.K.Sivakumar - 2010274014

Prewos Work
(the tensile fatigue behavior of Nicalon-type silicon carbide fiber reinforced lithium aluminosilicate (LAS) glass-ceramic composite)

8 April 2013

T.K.Sivakumar - 2010274014

Work by Suresh and coworkers

(Suresh et al., 1988,1991; Han and Suresh , 1989) on fatigue crack growth in variety of brittle solids)

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Fatigue in CMCs, the mechanisms of crack-tip deformation differ significantly under static and cyclic loading . They demonstrated that under pulsating compression, nucleation and growth of stable fatigue cracks occurred even at room temperature.

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Cyclic compressive loading caused mode I fatigue crack growth in SiC whiskers / Si3N4 matrix composites.
They also observed whiskers pullout and breakage after fatigue cycling. Such behavior is generally not observed under monotonic loading . This mode I fatigue crack growth under far-field cyclic compression occurs because a residual zone of tensile stress is generated at the crack tip on loading.
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8 April 2013

Work by Suresh and coworkers

(Suresh et al., 1988,1991; Han and Suresh , 1989) on fatigue crack growth in variety of brittle solids)

(a) Static deformation

(b) fatigue deformation leading to surface notch(Intrusion)

T.K.Sivakumar - 2010274014

(c) fatigue deformation leading to slip band extrusion

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8 April 2013

Work by Suresh and coworkers

(Suresh et al., 1988,1991; Han and Suresh , 1989) on fatigue crack growth in variety of brittle solids) (Continued .)

Wang et al (1991)investigated the behavior of a [0/90] carbon fiber reinforced silicon carbide composite under cyclic loading .

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They used tension-tension loading of smooth and notched sample and compression-compression loading .
Damage in pulsating tension consisted of cumulative micro cracking and spalling.

8 April 2013

T.K.Sivakumar - 2010274014

Work by Suresh and coworkers

(Suresh et al., 1988,1991; Han and Suresh , 1989) on fatigue crack growth in variety of brittle solids) (Continued .)

Spalling (delamination) of surface due to corrosion of a reinforcement

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T.K.Sivakumar - 2010274014

Work by Suresh and coworkers

(Suresh et al., 1988,1991; Han and Suresh , 1989) on fatigue crack growth in variety of brittle solids) (Continued .)

An important problem in high-temperature behavior of polycrystalline ceramics is the presence of intergranular glassy phases. Sintering and other processing aids can form glassy phases at the boundaries , which can result subcritical crack growth. Such subcritical crack growth can become very important in ceramic matrix composites because fibers such as silicon carbide can undergo oxidation.

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Work by Suresh and coworkers

(Suresh et al., 1988,1991; Han and Suresh , 1989) on fatigue crack growth in variety of brittle solids) (Continued .)

Han and Suresh (1989) examined the tensile cyclic fatigue crack growth in a silicon carbide whisker (33 vol.%)/alumina composite at 1400 C. The composite showed subcritical fatigue crack growth at stress intensity values far below the fracture tough factor , stress ratio, and frequency. They examined the crack tip region by optical and transmission electron microscopy and found that the nucleation and growth of flaws at the interface was the main damage mechanism. Diffuse micro cracking in the wake of crack and crack deflection / branching were observed.
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Work by Suresh and coworkers

(Suresh et al., 1988,1991; Han and Suresh , 1989) on fatigue crack growth in variety of brittle solids) (Continued .)

An increase in the test temperature (or the cyclic stress intensity or a reduction in the loading rate) can cause a rather significant increase in the size of the damage zone at the crack tip.
Han and Suresh observed oxidation of silicon carbide whiskers to a silica-type glassy phase in the crack tip region at 1400 C, in air. The alumina matrix can react with the main oxidation product, viz.,SiO2, to form aluminosilicates, SiC-rich or stoichiometric mullite, and the like. Viscous flow of glass can result in interfacial debonding , followed that there is a difference in deformation and failure mechanism under static and cyclic loadings, even in CMCs.
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Work by Suresh and coworkers

(Suresh et al., 1988,1991; Han and Suresh , 1989) on fatigue crack growth in variety of brittle solids) (Continued .)

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Sorensen and Holmes (1995) Work

(on hysteretic heating in CMCs under cyclic loading conditions due to interfacial friction )

Sorensen and Holmes(1995) observed that a lubricating layer may be beneficial in improve fatigue life of Continuous fiber CMCs.

A thicker coating, which would be expected to provide greater protection to the fiber against abrasion damage, resulted in less frictional heating because of less wear of the fibers during fatigue of a chemical vapor infiltration (CVI) Nicalon/C/SiC composite (Chawla et al.,1997,1998). The composite with a thinner coating exhibited much higher frictional heating .

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Sorensen and Holmes (1995) Work

(on hysteretic heating in CMCs under cyclic loading conditions due to interfacial friction ) (Continued .)

At higher frequencies, more heating was observed since the energy dissipated per unit time also increased . Substantial damage in terms of modulus was observed in fatigue of Nicalon/C/SiC, with most of the damage occurring during the first cycle . At a constant stress, the level of damage was not significantly dependent on frequency.

At a given frequency , however, higher damage in both composites.

stress induced more

A recovery in modulus of these woven composites was observed due to stretching and alignment of the plain- weaves fabric during fatigue, creating a stiffer reinforcing architecture.
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Sorensen and Holmes (1995) Work

(on hysteretic heating in CMCs under cyclic loading conditions due to interfacial friction ) (Continued .)

The laminate stacking sequence can affect the highfrequency fatigue behavior of CMCs. In SCS-6/Si3N4 composites, frictional heating in angle ply laminates [45]was substantially higher than that in cross-ply laminates [0/90](Chawla,1997). Because the angle ply had a lower stiffness, matrix microcracking in this composite was more predominant . Temperature rise in the specimens correlated very well with stiffness loss as a functional of fatigue cycles in the composites.
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Thank you
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