Lecture 1
Lecture 1
BACKGROUND
• Insulation System of Transformer - Oil
Paper
• System Ages - Dielectric
Properties
deteriorate
• At end of Life - Insulation
system
completely
loses its
dielectric
properties
• Oil Ageing - Acids & Sludge formation
- Reversible (by processing)
• Paper Ageing - Tensile strength
- DP
- Furan formation
- Irreversible
1. Oil soluble
2. Extracted & analyzed
METHODOLOGY
HIGH PERFORMANCE LIQUID CHROMATOGRAPHY
Pump
Reference
UV
Inject Column Computer
Detector
Sample
Eluent
FURANS
1. 5-hydroxymethyl-2-furaldehyde
(5HMF)
2. 2-furfuryl alcohol (2FOL)
3. 2-furaldehyde (2FAL)
4. 2-acetylfuran (2ACF)
5. 5-methyl-2-furaldehyde (5MEF)
1
Chromatogram at 276 nm
mV 5
4
Standard
3
t (min)
Chromatogram at 220 nm
mV 1 Standard
5
4
3
t (min)
Condition of paper insulation of
transformer
Total furan, ppb Condition
0 - 100 Normal
101 - 250 Questionable
251 - 1000 Deteriorated
1001 - 2500 Low reliability
> 2500 Rewind / Replace paper insulation