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Introduction

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Introduction

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Usama Sultan
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SEPARATION PROCESSES-II

Ch.E-310
Lecture-1; Course Outlines and
Introduction to Separation Processes-II

Presented By
Dr. Khalid Mahmood
Introduction
Separation Processes-II
Course Code : CHE-310
Credit Hours: 2

Monday: 8-9 AM
Wednesday: 8-9 AM

Instructor: Dr. Khalid Mahmood


Course Evaluation
Evaluation type %age

Quizzes 30

Mid term 30

Final Exam 40
Course Objectives
*The objective of this course is to explain the fundamental
principles of packed and tray distillation columns.

*Analyze the basic concepts of distillation, estimation of


stage efficiencies from column performance data and
empirical correlations and stage efficiency and column
height.

*General design considerations for the distillation


columns.
BOOKS RECOMMENDED
1. Seader, J. D.; Henley, E. J.; Roper, D. K., Separation Process Principles: Chemical and
Biochemical Operations. 3rd Ed., John Wiley & Sons, Inc.: 2011. [Chapters 6–7, 9–11]
2. Benítez, J., Principles and Modern Applications of Mass Transfer Operations. 2nd Ed.,
John Wiley & Sons, Inc.: 2009.
3. Chhabra, R.; Shankar, V., Coulson and Richardson’s Chemical Engineering — Volume
1B: Heat and Mass Transfer: Fundamentals and Applications. 7th Ed., Butterworth-
Heinemann: 2017.
4. Górak, A.; Olujić, Ž., Distillation: Equipment and Processes. Academic Press: 2014
5. Górak, A.; Sorensen, E., Distillation: Fundamentals and Principles. Academic Press:
2014
6. Khoury, F. M., Multistage Separation Processes. 4th Ed., CRC Press: 2015
7. King, C. J., Separation Processes. 2nd Ed., Dover Publications, Inc.: 2013

8. McCabe, W. L.; Smith, J. C.; Harriott, P., Unit Operations of Chemical Engineering.
7th Ed., McGraw-Hill: 2005
COURSE OUTLINE
• (1)Equipment for vapor–liquid separations: (a) Packed columns (b)
Types of packing (c) Tray columns (d) Types of trays (e) Spray and bubble
columns

• (2)Absorption and stripping: (a) Graphical design method for tray


columns (b) Algebraic design method for tray columns (c) HETP design
method for packed columns (d) Stage efficiency and column height (e)
Estimation of stage efficiencies from column performance data and
empirical correlations (f) Flooding, pressure drop, and tray diameter (g)
Weeping, entrainment, and downcomer backup

• (3) General design considerations for binary distillation columns


COURSE OUTLINE
• (4) McCabe–Thiele method for design of trayed distillation columns: (a)
Operating lines; Minimum number of stages (b) Minimum reflux ratio (c)
Feed location (d) Pinch point (e) Effect of column pressure, condenser
type, reflux temperature, reboiler type, and feed preheating (f) Estimation
of condenser and reboiler duties (g) Design of distillation columns with
multiple feeds, side streams, and open steam

• (5)
Estimation of stage efficiencies from column performance data and
empirical correlations for distillation columns

• (6) HETP and HTU methods for design of packed distillation columns

• (7) Ponchon–Savarit method for design of trayed distillation columns


COURSE OUTLINE
• (8)Multicomponent distillation: (a) Fenske–Underwood– Gilliland
method (b) Bubble-point method (c) Sum-rates method (d) Inside-out
method

• (9) Advanced distillation processes (a) Distillation boundaries (b) Residue-


curve maps (c) Extractive distillation (d) Pressure-swing distillation (e)
Homogeneous and heterogeneous azeotropic distillation (f) Reactive
distillation.
Components of Packed Column
Advantages of Tray Column
Advantages of Packed Column
Design procedure
Packing Materials

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