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Standardization of KMnO4 Presentation

The presentation outlines an experiment to determine the strength of Potassium Permanganate (KMnO₄) using standard Sodium Oxalate solution through oxidation-reduction titration. It details the necessary equipment, chemicals, procedure, and calculations involved, ultimately concluding with a determined strength of 0.02M for KMnO₄. Precautions and potential questions are also provided to ensure accurate results and understanding of the experiment.

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antoradhikary169802
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31 views15 pages

Standardization of KMnO4 Presentation

The presentation outlines an experiment to determine the strength of Potassium Permanganate (KMnO₄) using standard Sodium Oxalate solution through oxidation-reduction titration. It details the necessary equipment, chemicals, procedure, and calculations involved, ultimately concluding with a determined strength of 0.02M for KMnO₄. Precautions and potential questions are also provided to ensure accurate results and understanding of the experiment.

Uploaded by

antoradhikary169802
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Download as PPTX, PDF, TXT or read online on Scribd
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WELLCOME

TO
OUR PRESANTATION

PRESENTED TO:

PRESENTED BY: DR. MD SHARIFUL ALAM


ASSOCIATE PROFESSOR
ANTOR ADHIKARY TEXTILE ENGINEERING
ID:242002174
:
Standardization of Potassium
Permanganate Solution
"Why are we doing this experiment? What is
our objective?"

• Determine the strength of


Potassium Permanganate with
standard Sodium Oxalate
solution.

• Study oxidation-reduction titration.


Learning Outcome
• - Determine the strength of KMnO₄ solution.
• - Observe the endpoint through color change.
Theory (Part 1)
• Redox Reaction:
• - Oxidation: Loss of electrons (increase in
oxidation number).
• - Reduction: Gain of electrons (decrease in
oxidation number).
Theory (Part 2)
• Reaction Details:
• - Reduction: MnO₄⁻ → Mn²⁺
• - Oxidation: Na₂C₂O₄ → CO₂
• - KMnO₄ serves as its own indicator (pink color
at endpoint).
"What equipment do we need to conduct
this experiment?"
Conical Flask Burette Pipette Volumetric Flask

Stand Funnel Wash bottle Beaker


"What chemicals do we need to conduct
this experiment?"
Sodium Oxalate Potassium Permanganate
Solution (Na₂C₂O₄) Solution (KMnO₄)

Sulfuric Acid (H₂SO₄) Distilled Water


solution (1M)
Procedure
Pipette out 10 ml of M/10
standard sodium oxalate
solution into a conical flask.

Add about 50 ml of
1M sulfuric acid
solution.

Heat the solution


to 60-70°C.
Titrate the solution
against KMnO₄ until a
light pink color appears.

Record the volume


of KMnO₄ used.
Observations
• Table:
• - Initial and final burette readings.
• - Volume of KMnO₄ used.
• - Average volume calculated from trials.
Calculations
• Strength of KMnO₄ (Sₖₘₙₒ₄):
• (Sₒₓ × Vₒₓ × nₖₘₙₒ₄) / (nₒₓ × Vₖₘₙₒ₄)
• Example:
• - Sₖₘₙₒ₄ = (0.05 × 10 × 2) / (5 × 10.2) = 0.02M
Result
• The determined strength of KMnO₄ is 0.02M.
Precautions
• - Rinse burette and pipette with respective
solutions.
• - Handle apparatus carefully.
• - Avoid parallax error while reading
measurements.
• - Heat solution evenly.
Questions & Answers
• Prepare to answer:
• - Why no indicator is needed?
• - Why is heating necessary?
• - Effect of temperature changes on reaction
rate.

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